Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini

Abdulkadir Levent

doi:10.19113/sdufbed.20660

Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini

Abstract

Bu çalışmada, Naftalin bor katkılı elmas elektrot yüzeyindeki elektrokimyasal özellikleri, değişik çözelti ortamları ve geniş bir pH aralığında incelenmiştir. İlk olarak çalışma elektrotun performansını etkileyen değişkenler (destek elektrolitinin seçimi, elektrot temizleme yöntemi, iyon şiddeti ve pH, biriktirme/ölçüm çözeltisinin bileşimi, biriktirme gerilimi/süresi, voltametrik dalga formu değişkenleri); voltametri ve/ya da sıyırma voltametrisi teknikleri kullanılarak ayrıntılı olarak araştırılmıştır. Daha sonra önerilen yöntemlerin elde edilen optimum koşullarda Naftalin için doğrusallık (0.9-4.5 µM), saptama sınırı (LOD; 0.225 µM) ve kesinlik (% BSS 2.26) açısından validasyonu gerçekleştirilmiştir. Geliştirilen KD-ASV yöntemi, çeşme suyunda naftalinin analizi için standart katma yöntemi kullanılarak başarılı bir şekilde uygulanmıştır.

Keywords

PAH,Naftalin; Voltametri; Bor katkılı elmas elektrot

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Details

Primary Language

Turkish

Subjects

-

Journal Section

-

Authors

Abdulkadir Levent

Publication Date

April 28, 2017

Submission Date

January 19, 2017

Acceptance Date

-

Published in Issue

Year 2017 Volume: 21 Number: 3

DOI

https://doi.org/10.19113/sdufbed.20660

IZ

https://izlik.org/JA73AP85ML

Cite

RIS / Bibtex

APA

Levent, A. (2017). Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 21(3), 948-955. https://doi.org/10.19113/sdufbed.20660

AMA

1.Levent A. Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. J. Nat. Appl. Sci. 2017;21(3):948-955. doi:10.19113/sdufbed.20660

Chicago

Levent, Abdulkadir. 2017. “Bor Katkılı Elmas Elektrot Ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi Ile Miktar Tayini”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21 (3): 948-55. https://doi.org/10.19113/sdufbed.20660.

EndNote

Levent A (December 1, 2017) Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21 3 948–955.

IEEE

[1]A. Levent, “Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini”, J. Nat. Appl. Sci., vol. 21, no. 3, pp. 948–955, Dec. 2017, doi: 10.19113/sdufbed.20660.

ISNAD

Levent, Abdulkadir. “Bor Katkılı Elmas Elektrot Ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi Ile Miktar Tayini”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21/3 (December 1, 2017): 948-955. https://doi.org/10.19113/sdufbed.20660.

JAMA

1.Levent A. Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. J. Nat. Appl. Sci. 2017;21:948–955.

MLA

Levent, Abdulkadir. “Bor Katkılı Elmas Elektrot Ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi Ile Miktar Tayini”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, vol. 21, no. 3, Dec. 2017, pp. 948-55, doi:10.19113/sdufbed.20660.

Vancouver

1.Abdulkadir Levent. Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. J. Nat. Appl. Sci. 2017 Dec. 1;21(3):948-55. doi:10.19113/sdufbed.20660

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Katyonik Surfaktan Varlığında Kalem Grafit Elektrot Yüzeyinde Epirubisin’in Sıyırma Voltametrisi ile Miktar Tayini

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https://doi.org/10.35414/akufemubid.621530