Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini

Abdulkadir Levent

doi:10.19113/sdufbed.20660

Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini

Öz

Bu çalışmada, Naftalin bor katkılı elmas elektrot yüzeyindeki elektrokimyasal özellikleri, değişik çözelti ortamları ve geniş bir pH aralığında incelenmiştir. İlk olarak çalışma elektrotun performansını etkileyen değişkenler (destek elektrolitinin seçimi, elektrot temizleme yöntemi, iyon şiddeti ve pH, biriktirme/ölçüm çözeltisinin bileşimi, biriktirme gerilimi/süresi, voltametrik dalga formu değişkenleri); voltametri ve/ya da sıyırma voltametrisi teknikleri kullanılarak ayrıntılı olarak araştırılmıştır. Daha sonra önerilen yöntemlerin elde edilen optimum koşullarda Naftalin için doğrusallık (0.9-4.5 µM), saptama sınırı (LOD; 0.225 µM) ve kesinlik (% BSS 2.26) açısından validasyonu gerçekleştirilmiştir. Geliştirilen KD-ASV yöntemi, çeşme suyunda naftalinin analizi için standart katma yöntemi kullanılarak başarılı bir şekilde uygulanmıştır.

Anahtar Kelimeler

PAH,Naftalin; Voltametri; Bor katkılı elmas elektrot

Kaynakça

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Ayrıntılar

Birincil Dil

Türkçe

Konular

-

Bölüm

-

Yazarlar

Abdulkadir Levent

Yayımlanma Tarihi

28 Nisan 2017

Gönderilme Tarihi

19 Ocak 2017

Kabul Tarihi

-

Yayımlandığı Sayı

Yıl 2017 Cilt: 21 Sayı: 3

DOI

https://doi.org/10.19113/sdufbed.20660

IZ

https://izlik.org/JA73AP85ML

Kaynak Göster

RIS / Bibtex

APA

Levent, A. (2017). Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 21(3), 948-955. https://doi.org/10.19113/sdufbed.20660

AMA

1.Levent A. Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. 2017;21(3):948-955. doi:10.19113/sdufbed.20660

Chicago

Levent, Abdulkadir. 2017. “Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21 (3): 948-55. https://doi.org/10.19113/sdufbed.20660.

EndNote

Levent A (01 Aralık 2017) Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21 3 948–955.

IEEE

[1]A. Levent, “Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini”, Süleyman Demirel Üniv. Fen Bilim. Enst. Derg., c. 21, sy 3, ss. 948–955, Ara. 2017, doi: 10.19113/sdufbed.20660.

ISNAD

Levent, Abdulkadir. “Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21/3 (01 Aralık 2017): 948-955. https://doi.org/10.19113/sdufbed.20660.

JAMA

1.Levent A. Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. 2017;21:948–955.

MLA

Levent, Abdulkadir. “Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, c. 21, sy 3, Aralık 2017, ss. 948-55, doi:10.19113/sdufbed.20660.

Vancouver

1.Abdulkadir Levent. Bor Katkılı Elmas Elektrot ile Naftalin’in Voltametrik Davranışı: Kare Dalga Anodik Sıyırma Voltametrisi ile Miktar Tayini. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. 01 Aralık 2017;21(3):948-55. doi:10.19113/sdufbed.20660

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https://doi.org/10.35414/akufemubid.621530