Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method

Ayça Kıyak Yıldırım

Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method

Abstract

Chemical bath deposition (CBD) method was used to deposit thin films of PbS. In the experiments, PbS was obtained at four temperatures which are 55, 65, 75 and 85 °C. The effects of relatively high temperature were investigated in detail. The structural properties of the PbS films were examined by using X-ray diffractometer (XRD). According to the XRD, it was found that when temperature was increased, the preferred orientation shifted from (111) plane to the (002) plane at a deposition temperature higher than 75 °C. Besides, crystallite sizes (cs), lattice constants (a), average stresses (S), micro strains (e) and dislocation densities (d) were obtained from the XRD results. Surface properties of the PbS thin films were researched by using scanning electron microscope (SEM). It was seen from the SEM images that there was crack on the surface of the films when the film was obtained at 55 °C. On the other hand, no cracks were observed in the SEM images of PbS films of 30000 magnifications produced at temperatures higher than 55 °C.

Keywords

Lead sulphide,Thin films; Chemical bath deposition; Temperature

References

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Details

Primary Language

Turkish

Subjects

-

Journal Section

-

Authors

Ayça Kıyak Yıldırım

Publication Date

October 5, 2018

Submission Date

May 23, 2018

Acceptance Date

-

Published in Issue

Year 2018 Volume: 22

IZ

https://izlik.org/JA28AJ95NM

Cite

RIS / Bibtex

APA

Kıyak Yıldırım, A. (2018). Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 22, 414-420. https://izlik.org/JA28AJ95NM

AMA

1.Kıyak Yıldırım A. Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. J. Nat. Appl. Sci. 2018;22:414-420. https://izlik.org/JA28AJ95NM

Chicago

Kıyak Yıldırım, Ayça. 2018. “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22 (October): 414-20. https://izlik.org/JA28AJ95NM.

EndNote

Kıyak Yıldırım A (October 1, 2018) Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22 414–420.

IEEE

[1]A. Kıyak Yıldırım, “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”, J. Nat. Appl. Sci., vol. 22, pp. 414–420, Oct. 2018, [Online]. Available: https://izlik.org/JA28AJ95NM

ISNAD

Kıyak Yıldırım, Ayça. “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22 (October 1, 2018): 414-420. https://izlik.org/JA28AJ95NM.

JAMA

1.Kıyak Yıldırım A. Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. J. Nat. Appl. Sci. 2018;22:414–420.

MLA

Kıyak Yıldırım, Ayça. “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, vol. 22, Oct. 2018, pp. 414-20, https://izlik.org/JA28AJ95NM.

Vancouver

1.Ayça Kıyak Yıldırım. Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. J. Nat. Appl. Sci. [Internet]. 2018 Oct. 1;22:414-20. Available from: https://izlik.org/JA28AJ95NM