Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method

Cilt: 22 5 Ekim 2018
PDF İndir

Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method

Öz

Chemical bath deposition (CBD) method was used to deposit thin films of PbS. In the experiments, PbS was obtained at four temperatures which are 55, 65, 75 and 85 °C. The effects of relatively high temperature were investigated in detail. The structural properties of the PbS films were examined by using X-ray diffractometer (XRD). According to the XRD, it was found that when temperature was increased, the preferred orientation shifted from (111) plane to the (002) plane at a deposition temperature higher than 75 °C. Besides, crystallite sizes (cs), lattice constants (a), average stresses (S), micro strains (e) and dislocation densities (d) were obtained from the XRD results. Surface properties of the PbS thin films were researched by using scanning electron microscope (SEM). It was seen from the SEM images that there was crack on the surface of the films when the film was obtained at 55 °C. On the other hand, no cracks were observed in the SEM images of PbS films of 30000 magnifications produced at temperatures higher than 55 °C.

Anahtar Kelimeler

Kaynakça

  1. [1] Tohidi, T., Jamshidi-Ghaleh, K., Namdar, A., Abdi-Ghaleh, R. 2014. Comparative studies on the structural, morphological, optical, and electrical properties of nanocrystalline PbS thin films grown by chemical bath deposition using two different bath compositions. Materials Science in Semiconductor Processing, 25, pp.197-206.
  2. [2] Yang, J., Walker, A. V., 2014. Morphological Control of PbS Grown on Functionalized Self Assembled Monolayers by Chemical Bath Deposition. Langmuir, 30, 6954−6962.
  3. [3] Soonmin, H., Kassim, A., Weetee, T., 2014. Chemical Bath Deposited Lead Sulphide Thin Films: Preparation and Characterization, World of Mechanics, 1 (1).
  4. [4] Pentia, E., Pintilie, L., Botila, T., Pintilie, I., Chaparro, A., Maffiotte, C. 2003. Bi influence on growth and physical properties of chemical deposited PbS films. Thin Solid Films, 434(1-2), pp.162-170.
  5. [5] Jana, S., Thapa, R., Maity, R., Chattopadhyay, K., 2008. Optical and dielectric properties of PVA capped nanocrystalline PbS thin films synthesized by chemical bath deposition. Physica E: Low-dimensional Systems and Nanostructures, 40(10), pp.3121-3126.
  6. [6] Raniero, L., Ferreira, C., Cruz, L., Pinto, A.,Alves, R., 2010. Photoconductivity activation in PbS thin films grown at room temperature by chemical bath deposition. Physica B: Condensed Matter, 405(5), pp.1283-1286.
  7. [7] Hussain, A., Begum, A., Rahman, A., 2012. Characterization of Nanocrystalline Lead Sulphide Thin Films Prepared by Chemical Bath Deposition Technique. Arabian Journal for Science and Engineering, 38(1), pp.169-174.
  8. [8] Yeon, D., Lee, S., Jo, Y., Moon, J., Cho, Y., 2014. Origin of the enhanced photovoltaic characteristics of PbS thin film solar cells processed at near room temperature. Journal of Materials Chemistry, 2(47), pp.20112-20117.

Ayrıntılar

Birincil Dil

Türkçe

Konular

-

Bölüm

-

Yayımlanma Tarihi

5 Ekim 2018

Gönderilme Tarihi

23 Mayıs 2018

Kabul Tarihi

-

Yayımlandığı Sayı

Yıl 2018 Cilt: 22

Kaynak Göster

APA
Kıyak Yıldırım, A. (2018). Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 22, 414-420. https://izlik.org/JA28AJ95NM
AMA
1.Kıyak Yıldırım A. Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. 2018;22:414-420. https://izlik.org/JA28AJ95NM
Chicago
Kıyak Yıldırım, Ayça. 2018. “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22 (Ekim): 414-20. https://izlik.org/JA28AJ95NM.
EndNote
Kıyak Yıldırım A (01 Ekim 2018) Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22 414–420.
IEEE
[1]A. Kıyak Yıldırım, “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”, Süleyman Demirel Üniv. Fen Bilim. Enst. Derg., c. 22, ss. 414–420, Eki. 2018, [çevrimiçi]. Erişim adresi: https://izlik.org/JA28AJ95NM
ISNAD
Kıyak Yıldırım, Ayça. “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22 (01 Ekim 2018): 414-420. https://izlik.org/JA28AJ95NM.
JAMA
1.Kıyak Yıldırım A. Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. 2018;22:414–420.
MLA
Kıyak Yıldırım, Ayça. “Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, c. 22, Ekim 2018, ss. 414-20, https://izlik.org/JA28AJ95NM.
Vancouver
1.Ayça Kıyak Yıldırım. Effects of Relatively High Temperature on Thin Films of PbS Fabricated by Chemical Bath Deposition Method. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. [Internet]. 01 Ekim 2018;22:414-20. Erişim adresi: https://izlik.org/JA28AJ95NM

e-ISSN :1308-6529
Linking ISSN (ISSN-L): 1300-7688

Dergide yayımlanan tüm makalelere ücretiz olarak erişilebilinir ve Creative Commons CC BY-NC Atıf-GayriTicari lisansı ile açık erişime sunulur. Tüm yazarlar ve diğer dergi kullanıcıları bu durumu kabul etmiş sayılırlar. CC BY-NC lisansı hakkında detaylı bilgiye erişmek için tıklayınız.