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Gamma Spectrometric Method Validation for the Measurements of <sup>40</sup>K and <sup>137</sup>Cs in the Milk Powder

Year 2018, Volume: 22 Issue: 2, 493 - 498, 15.08.2018

Yusuf Ağuş

Abstract

In this study, gamma spectrometric method validation of the 40K and 137Cs in the milk powder was investigated. Each component of the method validation is evaluated and quantified. For this purpose, HpGe detectors with 20% efficiency n-type and 150% efficiency p-type were used.

Keywords

Gamma spectrometry Method validation; Milk powder; 40K; 137Cs

References

  • [1] Eurachem Guide. The Fitness for Purpose of Analytical Methods. A Laboratory Guide to Method Validation and Related Topics. Second edition. 2014
  • [2] EURACHEM / CITAC GUIDE CG4. Quantifying Uncertainty in Analytical Measurement. 2nd Edition. 2000.
  • [3] Gilmore, Gordon R., 2008. Practical Gamma-Ray Spectrometry-2nd Edition.
  • [4] Lepy, M., C, Pearce A, Sima, O., 2015. Uncertainties in gamma-ray spectrometry. Metrologia, 52(2015), pp. S123-S145.
  • [5] International Atomic Energy Agency (IAEA), 2004. Guide Quantifying Uncertainty in Nuclear Analytical Measurements, Vienna, 103-126, IAEA-TECDOC- 1401.
  • [6] ISO. Guide to the Expression of Uncertainty in Measurement, ISO, 1995.
  • [7] Currie, L.A., 1968. Limits for qualitative detection and quantitative determination, application to radioactivity. Anal. Chem., 40 (3), 586–593.
  • [8] NIST National Institute of Standards and Technology. Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results, Technical Note 1297, 1994 Edition.

Year 2018, Volume: 22 Issue: 2, 493 - 498, 15.08.2018

Yusuf Ağuş

Abstract

References

  • [1] Eurachem Guide. The Fitness for Purpose of Analytical Methods. A Laboratory Guide to Method Validation and Related Topics. Second edition. 2014
  • [2] EURACHEM / CITAC GUIDE CG4. Quantifying Uncertainty in Analytical Measurement. 2nd Edition. 2000.
  • [3] Gilmore, Gordon R., 2008. Practical Gamma-Ray Spectrometry-2nd Edition.
  • [4] Lepy, M., C, Pearce A, Sima, O., 2015. Uncertainties in gamma-ray spectrometry. Metrologia, 52(2015), pp. S123-S145.
  • [5] International Atomic Energy Agency (IAEA), 2004. Guide Quantifying Uncertainty in Nuclear Analytical Measurements, Vienna, 103-126, IAEA-TECDOC- 1401.
  • [6] ISO. Guide to the Expression of Uncertainty in Measurement, ISO, 1995.
  • [7] Currie, L.A., 1968. Limits for qualitative detection and quantitative determination, application to radioactivity. Anal. Chem., 40 (3), 586–593.
  • [8] NIST National Institute of Standards and Technology. Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results, Technical Note 1297, 1994 Edition.
There are 8 citations in total.

Details

Journal Section Articles
Authors

Yusuf Ağuş

Publication Date August 15, 2018
Published in Issue Year 2018 Volume: 22 Issue: 2

Cite

APA Ağuş, Y. (2018). Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 22(2), 493-498.
AMA Ağuş Y. Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder. SDÜ Fen Bil Enst Der. August 2018;22(2):493-498.
Chicago Ağuş, Yusuf. “Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22, no. 2 (August 2018): 493-98.
EndNote Ağuş Y (August 1, 2018) Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22 2 493–498.
IEEE Y. Ağuş, “Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder”, SDÜ Fen Bil Enst Der, vol. 22, no. 2, pp. 493–498, 2018.
ISNAD Ağuş, Yusuf. “Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 22/2 (August 2018), 493-498.
JAMA Ağuş Y. Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder. SDÜ Fen Bil Enst Der. 2018;22:493–498.
MLA Ağuş, Yusuf. “Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, vol. 22, no. 2, 2018, pp. 493-8.
Vancouver Ağuş Y. Gamma Spectrometric Method Validation for the Measurements of 40K and 137Cs in the Milk Powder. SDÜ Fen Bil Enst Der. 2018;22(2):493-8.
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