The Effect of Dıfferent Prımer and Unıversal Adhesıve on Shear Bond Strength Between Zırconıa and Self Adhesıve Resın Cement

Year 2024, , 10 - 16, 26.04.2024

Necla Demir , Sema Nur Öztürk , Çiğdem Çebi Tüysüz Meryem Gülce Subaşı

https://doi.org/10.15311/selcukdentj.1341590

Abstract

Background:The aim of this study was to evaluate the effect of different primers and universal adhesive used after sandblasting with aluminum oxide particles on the shear bond strength between zirconia and self-adhesive resin cement after thermal aging.
Material and Methods:Twenty rectangular samples were prepared from CAD/CAM zirconia blocks with dimensions of 2 mm x 11 mm x 11 mm. Surface roughening of 50 µm Al2O3 particles was applied to the surface of all samples. Prepared samples were divided into 4 subgroups according to different primer and adhesive applications (n=5). Control: No primer or universal adhesive was applied. Kerr Silane Primer (Negative Control): Ceramic primer without MDP content was applied. Ceramica-S and Nova Compo-B Plus: Ceramica-S primer and Nova Compo-B Plus universal adhesive were mixed and applied. Clearfil Ceramic Primer Plus: Clearfil Ceramic Primer Plus has been applied. Following the surface treatments, the self-adhesive resin cement was polymerized on the ceramic surfaces. Then, the samples were subjected to 5000 cycles of thermal cycling. Shear bond strength test was applied to the samples in a universal testing device. One-Way Analysis of Variance was used to compare the Fmax (N) and Mpa values according to the surface treatments.
Results:According to the use of different primers and adhesives, the mean Fmax (N) values showed a statistically significant difference (p<0,001). The value obtained with Ceramica S and Nova Compo-B Plus differed from all other primer groups and was higher (p<0,001). The value obtained with Clearfil Ceramic Primer Plus also differed from the other groups (p<0,001). The Fmax (N) values obtained in the control group and Kerr Silane Primer groups were similar (p<0,001).
Conclusions: Within the current limitations, it can be concluded that the application of self-adhesive resin cement without any primer or a primer without MDP is not sufficient to improve the bond strength to the zirconia ceramic surface. Primers or adhesives containing MDP and applied after sandblasting appear to be an ideal option for bonding to zirconia.
Keywords: Primer, Universal Adhesive, Zirconia

Keywords

primer, universal adhesive, zirconia

Ethical Statement

This article is not the version of a presentation. This article has not been prepared on the basis of a master’s/ doctoral thesis. It is declared that during the preparation process of this study, scientific and ethical principles were followed and all the studies benefited are stated in the bibliography.

Farklı Primerlerin ve Universal Adezivin, Zirkonya ve Self Adeziv Rezin Siman Arasındaki Makaslama Bağlanma Dayanımı Üzerine Etkisi

Abstract

Amaç: Bu çalışmanın amacı, alüminyum oksit partikülleriyle kumlama sonrası kullanılan farklı primerlerin ve universal adezivin, termal yaşlandırma sonrasında zirkonya ile self adeziv rezin siman arasındaki makaslama bağlanma dayanımı üzerindeki etkisini değerlendirmektir.
Gereç ve Yöntem: Çalışmamızda CAD/CAM zirkonya bloklardan boyutları 2 mm x 11 mm x 11 mm olacak şekilde 20 adet dörtgen örnek hazırlanmıştır. Tüm örneklerin yüzeyine 50 µm Al2O3 partikülleri yüzey pürüzlendirme işlemi uygulanmıştır. Hazırlanan örnekler farklı primer ve adeziv uygulamalarına göre 4 alt gruba ayrılmıştır (n=5). Kontrol: Herhangi bir primer veya universal adeziv uygulanmamıştır. Kerr Silane Primer (Negatif Kontrol): MDP içeriği bulunmayan seramik primeri uygulanmıştır. Ceramica-S ve Nova Compo-B Plus: Ceramica-S primer ve Nova Compo-B Plus universal adeziv karıştırılarak uygulanmıştır. Clearfil Ceramic Primer Plus: Clearfil Ceramic Primer Plus uygulanmıştır. Yüzey uygulamalarını takiben self adeziv rezin siman seramik yüzeylerine polimerize edilmiştir. Ardından örnekler 5000 devir termal döngü işlemine tabi tutulmuştur. Örneklere universal test cihazında makaslama bağlanma dayanımı testi uygulanmıştır. Yüzey işlemlerine göre Fmax (N) ve Mpa değerlerinin karşılaştırılmasında Tek Yönlü Varyans Analizi kullanılmıştır.
Bulgular: Farklı primer ve adeziv kullanımına göre Fmax (N) ortalama değerleri istatistiksel olarak anlamlı bir farklılık göstermiştir (p<0,001. Ceramica S ve Nova Compo-B Plus ile elde edilen değer diğer tüm primer gruplarından farklılık göstermiştir ve daha yüksektir (p<0,001). Clearfil Ceramic Primer Plus ile elde edilen değer de diğer gruplardan farklılık göstermiştir (p<0,001). Kontrol grubu ve Kerr Silane Primer gruplarında elde edilen Fmax (N) değerleri benzerlik göstermektedir (p>0,001).
Sonuç: Mevcut limitasyonlar dahilinde, self adeziv rezin simanın herhangi bir primer uygulaması olmaksızın veya MDP içermeyen bir primer uygulanmasının, zirkonya seramik yüzeyine bağlanma gücünü artırmak için yeterli olmadığı sonucuna varılabilir. MDP içeren ve kumlama sonrası uygulanan primerler veya adezivler, zirkonyaya bağlanma için ideal bir seçenek olarak görünmektedir.
Anahtar Kelimeler: Primer, Universal adeziv, Zirkonya

Keywords

primer, universal adeziv, zirkonya

Ethical Statement

Bu makale, sempozyum ya da kongrede sunulan bir tebliğin içeriği geliştirilerek ve kısmen değiştirilerek üretilmemiştir. Bu çalışma, yüksek lisans ya da doktora tezi esas alınarak hazırlanmamıştır. Bu çalışmanın hazırlanma sürecinde bilimsel ve etik ilkelere uyulduğu ve yararlanılan tüm çalışmaların kaynakçada belirtildiği beyan olunur.

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