Yıl 2019, Cilt 19 , Sayı 2, Sayfalar 286 - 291 2019-09-17

The Structural and Optical Properties of Sb2S3 Thin Films
Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri

Şilan BATURAY [1] , Derya BATIBAY [2] , Yusuf Selim OCAK [3]


The Antimony thiorea thin films which are the subject of this study were prepared by ultrasonic spray pyrolysis technique. The Antimony thiorea thin films were investigated depending on the substrate temperature. The optical and structural characteristics of these films were determined using UV–vis spectrophotometry and XRD analysis, respectively. By changing the substrate temperature, it was possible to control the optical and structural characteristic of the films. The optical properties films were analysed by energy band gap measurements using UV–vis spectrophotometry. While the band gaps of as grown films found to be 2.36, 2.47 ve 1.84eV, the band gaps of the films at annealing 500°C found to be 1.73, 1.76 ve 1.77eV.  XRD analysis was used to determine the microstrain (e), lattice spacing phase (d), crystallite size (D) and dislocation density (δ) for all orientations.

Bu çalışmaya konu olan antimon sülfür ince filmler ultrasonik sprey piroliz tekniği kullanılarak hazırlanmıştır. Farklı alttaş sıcaklığına bağlı olarak hazırlanan antimon sülfür ince filmlerin optik ve yapısal özellikleri sırasıyla UV-vis spektrofotometri ve XRD analizi kullanılarak incelenmiştir. Bu şekilde alttaş sıcaklığını değiştirerek optik ve yapısal özelikleri kontrol etmek mümkün olmuştur. Filmlerin optik özellikleri, UV-vis spektrometresi kullanılarak enerji bant aralığı ölçümleri ile analiz edildi. 275, 300 ve 325 °C’ de yapılan ve tavlanmamış filmler için enerji bant değerleri sırasıyla 2.36, 2.47 ve 1.84 eV olarak bulunurken, 500 °C’de sülfür ortamında tavlanan filmler için enerji bant değerleri sırasıyla 1.73, 1.76 ve 1.77eV olarak bulundu. Bütün yönelimler için mikro yapı (e), düzlemler arası mesafe (d), kristal büyüklüğü (D) ve dislokasyon yoğunluk (δ) XRD analizi kullanılarak belirlendi.
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Birincil Dil tr
Konular Mühendislik
Bölüm Makaleler
Yazarlar

Orcid: 0000-0002-8122-6671
Yazar: Şilan BATURAY (Sorumlu Yazar)
Kurum: DİCLE ÜNİVERSİTESİ, FEN FAKÜLTESİ
Ülke: Turkey


Orcid: 0000-0002-1012-6702
Yazar: Derya BATIBAY
Kurum: DİCLE ÜNİVERSİTESİ
Ülke: Turkey


Orcid: 0000-0001-8754-1720
Yazar: Yusuf Selim OCAK
Kurum: DİCLE ÜNİVERSİTESİ
Ülke: Turkey


Tarihler

Başvuru Tarihi : 31 Mayıs 2018
Yayımlanma Tarihi : 17 Eylül 2019

Bibtex @araştırma makalesi { akufemubid429200, journal = {Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi}, issn = {}, eissn = {2149-3367}, address = {}, publisher = {Afyon Kocatepe Üniversitesi}, year = {2019}, volume = {19}, pages = {286 - 291}, doi = {}, title = {Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri}, key = {cite}, author = {BATURAY, Şilan and BATIBAY, Derya and OCAK, Yusuf Selim} }
APA BATURAY, Ş , BATIBAY, D , OCAK, Y . (2019). Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri. Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi , 19 (2) , 286-291 . Retrieved from https://dergipark.org.tr/tr/pub/akufemubid/issue/48783/429200
MLA BATURAY, Ş , BATIBAY, D , OCAK, Y . "Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri". Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi 19 (2019 ): 286-291 <https://dergipark.org.tr/tr/pub/akufemubid/issue/48783/429200>
Chicago BATURAY, Ş , BATIBAY, D , OCAK, Y . "Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri". Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi 19 (2019 ): 286-291
RIS TY - JOUR T1 - Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri AU - Şilan BATURAY , Derya BATIBAY , Yusuf Selim OCAK Y1 - 2019 PY - 2019 N1 - DO - T2 - Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi JF - Journal JO - JOR SP - 286 EP - 291 VL - 19 IS - 2 SN - -2149-3367 M3 - UR - Y2 - 2019 ER -
EndNote %0 Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri %A Şilan BATURAY , Derya BATIBAY , Yusuf Selim OCAK %T Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri %D 2019 %J Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi %P -2149-3367 %V 19 %N 2 %R %U
ISNAD BATURAY, Şilan , BATIBAY, Derya , OCAK, Yusuf Selim . "Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri". Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi 19 / 2 (Eylül 2019): 286-291 .
AMA BATURAY Ş , BATIBAY D , OCAK Y . Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri. Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi. 2019; 19(2): 286-291.
Vancouver BATURAY Ş , BATIBAY D , OCAK Y . Sb2S3 İnce Filmlerinin Yapısal ve Optik Özellikleri. Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi. 2019; 19(2): 291-286.