Elektrokimyasal Olarak Çöktürülmüş Metal Oksit Takviyelendirilmiş Ni Nanokompozit Kaplamaların Korozyon Performansı

Öz

Geleneksel nikel kaplamaların özellikleri, elektrokimyasal çöktürme yöntemi kullanılarak üretilen metal oksit nanopartiküller ile güçlendirilmiş Ni nanokompozit kaplamalar hazırlanarak geliştirilmiştir. Uygulanan akım yoğunluğunun etkisi, SiO 2 nanopartikül konsantrasyonu değiştirilerek incelenmiştir. Nanokompozit kaplamaların faz yapısı çalışması ve morfolojik incelemeleri sırasıyla XIşını Difraktometre ve Taramalı Elektron Mikroskobu ile yapılmıştır. Elde edilen nanokompozit kaplamaların mekanik özelliklerini belirlemek için Vickers indentasyon yöntemi kullanılmıştır. Nanokompozit kaplamaların elektrokimyasal davranışını değerlendirmek için potansiyodinamik polarizasyon tekniği uygulanmıştır. Sonuç olarak, Ni matrisine SiO 2 nanopartiküllerinin ilavesi, üretilen nanokompozit kaplamaların hem mekanik hem de elektrokimyasal özelliklerini iyileştirmektedir.

Anahtar Kelimeler

• Nanokompozit Kaplamalar
• SiO 2Nanopartikül
• Elektrokimyasal Çöktürme
• Mikrosertlik
• Korozyon

Corrosion Performance of Electrodeposited Ni Nanocomposite Coatings Reinforced with Metal Oxide Particles

Öz

The properties of traditional nickel coatings were enhanced by preparing Ni nanocomposite coatings reinforced with metal oxide nanoparticles by using electrodeposition technique. The impact of applied current density was investigated by changing SiO2 nanoparticle concentration. Phase structure study and morphological investigation of the samples were performed by X-Ray Diffractometer and Scanning Electron Microscopy, respectively. Vickers indentation method was utilized to determine the mechanical properties of obtained nanocomposite coatings. Potentiodynamic polarization technique was performed to evaluate electrochemical behavior of nanocomposite coatings. As a result, introducing SiO 2 nanoparticles to Ni matrix improves both mechanical and electrochemical properties of produced nanocomposite coatings.

Anahtar Kelimeler

• Nanocomposite Coatings
• SiO 2Nanoparticle
• Electrodeposition
• Microhardness
• Corrosion

Kaynakça

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