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The Effect Of Thin Film CrC Coating On Microstructure And Microhardness Properties Of Manganese Steel Surface

Yıl 2024, Cilt: 14 Sayı: 2, 160 - 163

Öz

In this study, the microstructure and microhardness properties of manganese steel coated with chromium carbide (CrC) using Thermo Reactive Diffusion (TRD) method at 900℃ and 1100℃ for 4 hours were investigated. The surface morphology of the coating was characterized by scanning electron microscopy (SEM), elemental distribution, X-ray spectroscopy (EDS). Microhardness properties were determined using the Vickers method. Microstructural properties and microhardness results were characterized. The microstructure results showed that the coating process at 1100℃ was metallurgically more uniform. The minimum coating thickness was 14.95 μm at 900℃ and the maximum thickness was 24.1 μm at 1100℃. In EDS measurements, while CrC was dense in the coating region, Fe density increased towards the substrate. In the microhardness measurements, the highest value was measured as 2371 HV0.5 in the sample coated at 1100℃. Based on these results, it is thought that CrC coating forms a better coating layer especially at high temperatures.

Kaynakça

  • [1] Ş. Ertürk, F. Erzincanlı, "Investigation of Coating Properties and Machining Capability of Boron and Titanium Coated AISI D2 Cutting Tools by Thermochemical Method." DUBITED 8.1: 1095-1109, 2020.
  • [2] S. Özel, "Yüzey Kaplama İşlemlerinde Kullanılan Isıl Püskürtme Yöntemleri." Bitlis Eren University Journal of Science 2.1: 88-97, 2013.
  • [3] Ç. Dindar, M. Altay, & H. Aydın, " Laser Cladding Process and Process Parameters: A Review Uludağ University Journal of The Faculty of Engineering 26.2: 723-736, 2021
  • [4] M. Kilic, A Imak, & I. Kirik, "Surface modification of AISI 304 stainless steel with NiBSi-SiC composite by TIG method." JMEPEG 30.2: 1411-1419, 2021.
  • [5] M. Akkaş, "The mechanical and corrosion properties of WCCo–Al coatings formed on AA2024 using the HVOF method." Materials Research Express(MRX) 7.7: 076515, 2020.
  • [6] H. Durmuş, M. Türkmen, & U. Çalıgülü, "Wear Resistances of X6Cr17 Ferritic Stainless Steel Surfaces Coated with Al2O3 Powders Using Thermal Spray Method." DUJE 11.3: 1167-1173, 2020.
  • [7] A. Aytaç, & U. Malayoğlu, "Comparison of PVD and JVD / DVD Thin Film Coatings by Physical Vapor Deposition Methods and a Conceptual, Academic and Theoretical Analysis on Industrial Applications of DVD Coating Technology." Journal of Defense Sciences 17.1: 131-164, 2018.
  • [8] M. Kılıç, & E. Korkmaz, " Effect of Parameters on Coating Thickness." Batman University Journal of Life Sciences 13.2: 28-35, 2024.
  • [9] B. Kurt, Y. Küçük, and M.S. Gök, Microabrasion wear behavior of VC and CrC coatings deposited by thermo-reactive diffusion technique, Tribol. Trans., 57, No. 2, pp. 345, 2014.
  • [10] A. Toru, "Thermoreactive deposition/diffusion process for surface hardening of steels." Steel Heat Treating Fundamentals and Processes. ASM International, 725-740, 2013.
  • [11] M. Kilic, (2020). "TiC coatings on an alloyed steel produced by thermal diffusion". Materials Testing, 62(9), 909-912, 2020.
  • [12] Çelik, Y. H., Ertem, M., Gür, A. K., Kurt, B., Caligulu, U., Özay, Ç., & Yildiz, T. (2021). Investıgatıon Of Mıcrostructure Propertıes Of Nbc–B Coated Hardox 400 Steel By Trd Method And Evaluatıon Of Wear Behavıor By Taguchı Method. Surface Review and Letters, 28(12), 2150115.
  • [13] S. Buytoz, B. Yılmaz, " Investigation of microstrucutural properties of TiC coating obtained by termoreactive diffusion process on AISI4140 steel." Fırat University Journal of Engineering Sciences 31.2: 473-480, 2019.
  • [14] B. Kurt, Y. Küçük, & M.S. Gök, "Microabrasion wear behavior of VC and CrC coatings deposited by thermoreactive diffusion technique." Tribology Transactions 57.2: 345-352, 2014.
  • [15] Y. Karaca, "Investigation of VC Coatability Of 1.2344 Hot Work Tool Steel With Box Cementation Method." Nevşehir Journal of Science and Technology 106-110, 2019.
  • [16] M. Kilic, "TiC coatings on an alloyed steel produced by thermal diffusion." Materials Testing 62.9: 909-912, 2020.
  • [17] F. E. Castillejo, D. M. Marulanda, J. J. Olaya& J. E. Alfonso, "Wear and corrosion resistance of niobium–chromium carbide coatings on AISI D2 produced through TRD." Surface and Coatings Technology 254: 104-111, 2014.
  • [18] A. Ghadi, H.Ebrahimnezhad-Khaljiri, & R. Gholizadeh, "A comprehensive review on the carbide-base coatings produced by thermo-reactive diffusion: microstructure and properties viewpoints." Journal of Alloys and Compounds, 171839, 2023.
  • [19] S. Özel, " Microstructure and hardness investigation of fe matrix carbide layers alloyed by TIG welding method." KSU Journal of Engineering Sciences 27.2: 311-324, 2024.
  • [20] A. V. Khvan, B.Hallstedt, & C. Broeckmann, "A thermodynamic evaluation of the Fe–Cr–C system." Calphad 46: 24-33, 2014.
  • [21] M. R. Najari, S. A. Sajjadi, & O. Ganji, " Microstructural evolution and wear properties of chromium carbide coating formed by thermo-reactive diffusion (TRD) process on a cold-work tool steel " Results in Surfaces and Interfaces 8: 100059, 2022.
  • [22] O. Ganji, S. A. Sajjadi, Z. G.Yang, M. Mirjalili, & M. R. Najari, "On the formation and properties of chromium carbide and vanadium carbide coatings produced on W1 tool steel through thermal reactive diffusion (TRD)" Ceramics International 46.16: 25320-25329, .
Yıl 2024, Cilt: 14 Sayı: 2, 160 - 163

Öz

Kaynakça

  • [1] Ş. Ertürk, F. Erzincanlı, "Investigation of Coating Properties and Machining Capability of Boron and Titanium Coated AISI D2 Cutting Tools by Thermochemical Method." DUBITED 8.1: 1095-1109, 2020.
  • [2] S. Özel, "Yüzey Kaplama İşlemlerinde Kullanılan Isıl Püskürtme Yöntemleri." Bitlis Eren University Journal of Science 2.1: 88-97, 2013.
  • [3] Ç. Dindar, M. Altay, & H. Aydın, " Laser Cladding Process and Process Parameters: A Review Uludağ University Journal of The Faculty of Engineering 26.2: 723-736, 2021
  • [4] M. Kilic, A Imak, & I. Kirik, "Surface modification of AISI 304 stainless steel with NiBSi-SiC composite by TIG method." JMEPEG 30.2: 1411-1419, 2021.
  • [5] M. Akkaş, "The mechanical and corrosion properties of WCCo–Al coatings formed on AA2024 using the HVOF method." Materials Research Express(MRX) 7.7: 076515, 2020.
  • [6] H. Durmuş, M. Türkmen, & U. Çalıgülü, "Wear Resistances of X6Cr17 Ferritic Stainless Steel Surfaces Coated with Al2O3 Powders Using Thermal Spray Method." DUJE 11.3: 1167-1173, 2020.
  • [7] A. Aytaç, & U. Malayoğlu, "Comparison of PVD and JVD / DVD Thin Film Coatings by Physical Vapor Deposition Methods and a Conceptual, Academic and Theoretical Analysis on Industrial Applications of DVD Coating Technology." Journal of Defense Sciences 17.1: 131-164, 2018.
  • [8] M. Kılıç, & E. Korkmaz, " Effect of Parameters on Coating Thickness." Batman University Journal of Life Sciences 13.2: 28-35, 2024.
  • [9] B. Kurt, Y. Küçük, and M.S. Gök, Microabrasion wear behavior of VC and CrC coatings deposited by thermo-reactive diffusion technique, Tribol. Trans., 57, No. 2, pp. 345, 2014.
  • [10] A. Toru, "Thermoreactive deposition/diffusion process for surface hardening of steels." Steel Heat Treating Fundamentals and Processes. ASM International, 725-740, 2013.
  • [11] M. Kilic, (2020). "TiC coatings on an alloyed steel produced by thermal diffusion". Materials Testing, 62(9), 909-912, 2020.
  • [12] Çelik, Y. H., Ertem, M., Gür, A. K., Kurt, B., Caligulu, U., Özay, Ç., & Yildiz, T. (2021). Investıgatıon Of Mıcrostructure Propertıes Of Nbc–B Coated Hardox 400 Steel By Trd Method And Evaluatıon Of Wear Behavıor By Taguchı Method. Surface Review and Letters, 28(12), 2150115.
  • [13] S. Buytoz, B. Yılmaz, " Investigation of microstrucutural properties of TiC coating obtained by termoreactive diffusion process on AISI4140 steel." Fırat University Journal of Engineering Sciences 31.2: 473-480, 2019.
  • [14] B. Kurt, Y. Küçük, & M.S. Gök, "Microabrasion wear behavior of VC and CrC coatings deposited by thermoreactive diffusion technique." Tribology Transactions 57.2: 345-352, 2014.
  • [15] Y. Karaca, "Investigation of VC Coatability Of 1.2344 Hot Work Tool Steel With Box Cementation Method." Nevşehir Journal of Science and Technology 106-110, 2019.
  • [16] M. Kilic, "TiC coatings on an alloyed steel produced by thermal diffusion." Materials Testing 62.9: 909-912, 2020.
  • [17] F. E. Castillejo, D. M. Marulanda, J. J. Olaya& J. E. Alfonso, "Wear and corrosion resistance of niobium–chromium carbide coatings on AISI D2 produced through TRD." Surface and Coatings Technology 254: 104-111, 2014.
  • [18] A. Ghadi, H.Ebrahimnezhad-Khaljiri, & R. Gholizadeh, "A comprehensive review on the carbide-base coatings produced by thermo-reactive diffusion: microstructure and properties viewpoints." Journal of Alloys and Compounds, 171839, 2023.
  • [19] S. Özel, " Microstructure and hardness investigation of fe matrix carbide layers alloyed by TIG welding method." KSU Journal of Engineering Sciences 27.2: 311-324, 2024.
  • [20] A. V. Khvan, B.Hallstedt, & C. Broeckmann, "A thermodynamic evaluation of the Fe–Cr–C system." Calphad 46: 24-33, 2014.
  • [21] M. R. Najari, S. A. Sajjadi, & O. Ganji, " Microstructural evolution and wear properties of chromium carbide coating formed by thermo-reactive diffusion (TRD) process on a cold-work tool steel " Results in Surfaces and Interfaces 8: 100059, 2022.
  • [22] O. Ganji, S. A. Sajjadi, Z. G.Yang, M. Mirjalili, & M. R. Najari, "On the formation and properties of chromium carbide and vanadium carbide coatings produced on W1 tool steel through thermal reactive diffusion (TRD)" Ceramics International 46.16: 25320-25329, .
Toplam 22 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Malzeme Üretim Teknolojileri
Bölüm Araştırma Makalesi
Yazarlar

Musa Kılıç 0000-0001-5808-6917

Erken Görünüm Tarihi 13 Ocak 2025
Yayımlanma Tarihi
Gönderilme Tarihi 8 Temmuz 2024
Kabul Tarihi 3 Eylül 2024
Yayımlandığı Sayı Yıl 2024 Cilt: 14 Sayı: 2

Kaynak Göster

APA Kılıç, M. (2025). The Effect Of Thin Film CrC Coating On Microstructure And Microhardness Properties Of Manganese Steel Surface. European Journal of Technique (EJT), 14(2), 160-163. https://doi.org/10.36222/ejt.1512398

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