The Effect of Cu doping on Fatigue Properties of TiZrNbN Coatings

Öz

The fatigue properties are very important for cutting tools due to service life. To improve fatigue properties of cutting tools, transition metal nitrides with soft metal (Cu, Ni etc.) have been coated on cutting tool materials. To investigate Cu effect on fatigue properties, TiZrNbN and Cu doped TiZrNbN coatings were deposited on M2 high speed steel using reactive closed field unbalanced magnetron sputtering (CFUBMS) in bias voltage of -80V, coating pressure of 0.33 Pa and Cu target current of 0.6 A. Microstructure properties of the coatings were determined by X-Ray Diffraction (XRD), Scanning Electron Microscope (SEM) and Energy Dispersive Spectroscopy (EDS). Mechanical properties of the coatings were examined with microhardness tester and scratch tester. Fatigue properties of the coatings were examined using multi-pass scratch tester. According to the results, the microhardness of Cu doped TiZrNbN is better than TiZrNbN. On the other hand, the adhesion and fatigue properties of TiZrNbN are the highest.

Anahtar Kelimeler

• CFUBMS,multi-pass scratch,TiZrNbN,fatigue,Cu

Cu ilavesinin TiZrNbN Kaplamaların Yorulma Özelliklerine Etkisi

Öz

Yorulma özellikleri, kullanım ömrü nedeniyle kesme aletleri için çok önemlidir. Kesici takımların yorulma özelliklerini iyileştirmek için kesici takım malzemeleri üzerine yumuşak metalle (Cu, Ni vb.) Geçiş metali nitrürleri kaplanmıştır. Yorulma özellikleri üzerindeki Cu etkisini araştırmak için, TiZrNbN ve Cu katkılı TiZrNbN kaplamalar, -80V'luk ön gerilim voltajında, 0.33 Pa'lık kaplama basıncı ve Cu hedef akımında 0.6 A değerinde reaktif kapalı alan dengesiz manyetik alanda sıçratma (CFUBMS) kullanılarak M2 yüksek hızlı çelik üzerinde biriktirildi. Kaplamaların mikro yapı özellikleri X-Ray Difraktometri (XRD), Taramalı Elektron Mikroskop (SEM) ve Enerji Dağıtıcı Spektroskopi (EDS) ile belirlenmiştir. Kaplamaların mekanik özellikleri microhardness test cihazı ve çizik test cihazı ile incelenmiştir. Kaplamaların yorulma özellikleri çok geçişli çizik test cihazı kullanılarak incelenmiştir. Sonuçlara göre, Cu katkılı TiZrNbN'nin mikro sertliği TiZrNbN'den daha iyidir. Öte yandan, TiZrNbN'nin yapışma ve yorulma özellikleri en yüksektir

Anahtar Kelimeler

• CFUBMS,çoklu geçişli çizik,TiZrNbN,yorulma,Cu

Kaynakça

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