Araştırma Makalesi

Production and characterization of chitosan-based polymer particles with the precipitation collection method

Cilt: 1 Sayı: 2 8 Haziran 2022
  • Hülya Demırtaş
  • Şeyda Taşar *
  • Fatih Kaya
  • Ahmet Özer
PDF İndir

Production and characterization of chitosan-based polymer particles with the precipitation collection method

Öz

In this study, a chitosan-based polymer particle was produced to be used as a sorbent. Gel particle production was carried out using chitosan samples with different acetylation degrees and molecular weights. The produced particles were characterized. In the first phase of the study, chitosan samples were provided and structural analyses were performed. In the second stage, polymer particle production was carried out by the precipitation-collection method. The morphological, structural, and physicochemical properties of the produced gel particles were examined. In the last step, the sorption efficiency of the particles (distilled water, oleic acid) was investigated. As a result, it was measured that the polymer particle diameters were to be between 3.388 and 3.903 mm and the densities of the particles were to be 0.389-0.416 g/cm3. Distilled water holding capacity of the particle which was produced with an 85 % DDA chitosan sample, was calculated as 0.523 g/gparticles, and the oleic acid holding capacity was determined as 0.286 g/gparticles. These values are approximately 20 % lower than the values obtained with the 75 % DDA chitosan sample. Low molecular mass chitosan sample sorbed 0.556 g distilled water per gram particle and 0.193 g oleic acid per gram particle. These values were calculated as 0.170 g/gparticle and 0.381 g/gparticle for the particles produced using high molecular weight chitosan samples, respectively. EDX analysis performed on the selected region, it was determined that the chitosan-based polymer particle consisted of 43.58 % C, and 49.83 % O.

Anahtar Kelimeler

Kaynakça

  1. [1] Sharma S, Sudhakara P, Singh J, Ilyas RA, Asyraf MRM, Razman MR. “Critical review of biodegradable and bioactive polymer composites for bone tissue engineering and drug delivery applications”. Polymers, 13(16), 2623, 2021.
  2. [2] Fernandez-Kim SO. Physicochemical and Functional Properties of Crawfish Chitosan as Affected by Different Processing Protocols. MS dissertation, Louisiana State University, Baton Rouge, L.A., 2004.
  3. [3] Tajik H, Moradi M, Rohani SMR, Erfani AM, Jalali FSS. “Preparation of chitosan from brine shrimp (artemia urmiana) cyst shells and effects of different chemical processing sequences on the physicochemical and functional properties of the product”. Molecules, 13, 1263-1274, 2008.
  4. [4] Peker İ, Oktar F, Eroğlu M, Morkoç E. “Kerevit kabuklarından kitosan üretilmesi ve kesilmiş sütün suyundan laktoz izolasyonu işleminde kullanılması”. Tübitak MAG Project, Project number: 104M017, 88, 2006.
  5. [5] Rinaudo, M. “Chitin and chitosan: properties and applications”. Progress in Polymer Science, 31, 603-632, 2006.
  6. [6] Nemtsev SV, Gamzazade AI, Rogozhin SV, Bykova VM, Bykov VP. “Deacetylation of chitin under homogeneous conditions”. Applied Biochemistry and Microbiology, 38 (6), 521–526, 2002.
  7. [7] Paulino AT, Simionato JI, Garcia JC, Nozaki J. “Characterization of chitosan and chitin produced from silkworm crysalides”. Carbohydrate Polymers, 64, 98-103, 2006.
  8. [8] Hajji S, Younes I, Ghorbel-Bellaaj O, Hajji R, Rinaudo M, Nasri M, Jellouli K. “Structural differences between chitin and chitosan extracted from three different marine sources”. International Journal of Biological Macromolecules, 65, 298-306, 2014.

Ayrıntılar

Birincil Dil

İngilizce

Konular

Kimya Mühendisliği

Bölüm

Araştırma Makalesi

Yayımlanma Tarihi

8 Haziran 2022

Gönderilme Tarihi

21 Ocak 2022

Kabul Tarihi

9 Mayıs 2022

Yayımlandığı Sayı

Yıl 2022 Cilt: 1 Sayı: 2

Kaynak Göster

APA
Demırtaş, H., Taşar, Ş., Kaya, F., & Özer, A. (2022). Production and characterization of chitosan-based polymer particles with the precipitation collection method. Firat University Journal of Experimental and Computational Engineering, 1(2), 68-79. https://izlik.org/JA62GG22MY
AMA
1.Demırtaş H, Taşar Ş, Kaya F, Özer A. Production and characterization of chitosan-based polymer particles with the precipitation collection method. Firat University Journal of Experimental and Computational Engineering. 2022;1(2):68-79. https://izlik.org/JA62GG22MY
Chicago
Demırtaş, Hülya, Şeyda Taşar, Fatih Kaya, ve Ahmet Özer. 2022. “Production and characterization of chitosan-based polymer particles with the precipitation collection method”. Firat University Journal of Experimental and Computational Engineering 1 (2): 68-79. https://izlik.org/JA62GG22MY.
EndNote
Demırtaş H, Taşar Ş, Kaya F, Özer A (01 Haziran 2022) Production and characterization of chitosan-based polymer particles with the precipitation collection method. Firat University Journal of Experimental and Computational Engineering 1 2 68–79.
IEEE
[1]H. Demırtaş, Ş. Taşar, F. Kaya, ve A. Özer, “Production and characterization of chitosan-based polymer particles with the precipitation collection method”, Firat University Journal of Experimental and Computational Engineering, c. 1, sy 2, ss. 68–79, Haz. 2022, [çevrimiçi]. Erişim adresi: https://izlik.org/JA62GG22MY
ISNAD
Demırtaş, Hülya - Taşar, Şeyda - Kaya, Fatih - Özer, Ahmet. “Production and characterization of chitosan-based polymer particles with the precipitation collection method”. Firat University Journal of Experimental and Computational Engineering 1/2 (01 Haziran 2022): 68-79. https://izlik.org/JA62GG22MY.
JAMA
1.Demırtaş H, Taşar Ş, Kaya F, Özer A. Production and characterization of chitosan-based polymer particles with the precipitation collection method. Firat University Journal of Experimental and Computational Engineering. 2022;1:68–79.
MLA
Demırtaş, Hülya, vd. “Production and characterization of chitosan-based polymer particles with the precipitation collection method”. Firat University Journal of Experimental and Computational Engineering, c. 1, sy 2, Haziran 2022, ss. 68-79, https://izlik.org/JA62GG22MY.
Vancouver
1.Hülya Demırtaş, Şeyda Taşar, Fatih Kaya, Ahmet Özer. Production and characterization of chitosan-based polymer particles with the precipitation collection method. Firat University Journal of Experimental and Computational Engineering [Internet]. 01 Haziran 2022;1(2):68-79. Erişim adresi: https://izlik.org/JA62GG22MY