İletken poli(o-anisidin)/ talk kompozitinin sentezi ve karakterizasyonu
Yıl 2018,
Cilt: 33 Sayı: 2, 403 - 412, 06.04.2018
Duygu Anaklı
,
Sevil Çetinkaya
,
Meral Karakisla
,
Mehmet Sacak
Öz
İletken poli(o-anisidin)(POA)/talk kompoziti talk partikülleri varlığında amonyum persülfat (APS) yükseltgeni kullanarak o-anisidinin kimyasal polimerizasyonu ile hazırlandı. (POA)/talk kompozitinin içerdiği POA miktarı ve iletkenliğinin APS/o-anisidin mol oranı, o-anisidin ve HCI derişimleri gibi polimerizasyon parametreleri ile değişimi incelendi. Talkın mikrosertlik özelliğinin yapıya katılan iletken polimer ile arttığı mikro indentasyon analizi ile belirlendi. Kompozitin yapısal, fiziksel, morfolojik ve ısıl analizleri FTIR, XRD, BET, SEM ve TGA teknikleri ile incelendi.
Kaynakça
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