Sayın Editör, Metin içindeki birimler ve farklı gösterimler düzeltilmiştir. Referanlar dergi kurallarına göre tekrar revize edilmiştir. Metin içinde verilen cümlelerde aralarında birden fazla boşluk olan yerler kontrol edilmiştir. Makale içinde geçen figur ve tablolar, referanslardan sonra verilmiştir. Ayrıca bütün şekillerin çöznürlüğü 300 dpi olarak yeniden ayrı ayrı yüklenmiştir. Bütün makalenin taranarak yazım hatalarının kontrol edilmesi gerekmeltedir. Gerekli gördüğünüz tüm düzeltmeler yapılmıştır. saygılar sunuyorum
This study describes the residual mercury levels in canned fish marketed in Turkey. In total, 375 fish samples were analyzed by Inductive Coupled Plasma Optical Emission Spectrometry (ICP OES) for mercury residues. The quantification limit (LOQ) from the validation data ranged from 0.008 to 0.043 mg kg-1. Accuracy and precision were evaluated by means of recovery experiments at two concentration levels (30, and 50 μg L−1), obtaining recoveries between 87.5% and 109.3% and coefficient of variation below 10%. Also, the relative standard deviation (RSD) ranged from 0.2% to 9%. The expanded measurement uncertainty for mercury ranged from 11.1% to 19.2%. In investigated samples, 4.8% were detected at a detectable level of mercury, but these levels were below the legal limits. With regard to hg level were no significant correlations (p < 0.05) between species. According to Turkey's legislation, none of for example the maximum limit of 1.0 mg g-1 did not exceed the level, but 1.3% exceeded the limit recommended by the Food and Agriculture Organization/World Health Organization (0.5 ug g-1). The reproducibility limits obtained as a result of the validation study were found to be appropriate in accordance with both the NMKL 170 method and the Turkish Food Codex (Communiqué No: 2014/2), as well as the EU Commission Decision 2002/657/EC.
Birincil Dil | İngilizce |
---|---|
Konular | Mühendislik |
Bölüm | Articles |
Yazarlar | |
Erken Görünüm Tarihi | 30 Aralık 2021 |
Yayımlanma Tarihi | 5 Ocak 2022 |
Kabul Tarihi | 24 Mayıs 2021 |
Yayımlandığı Sayı | Yıl 2022 Cilt: 50 Sayı: 1 |
HACETTEPE JOURNAL OF BIOLOGY AND CHEMİSTRY
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