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Sol-gel synthesis and characterization of TiO2 powder

Cilt: 1 Sayı: 2 12 Aralık 2017
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Sol-gel synthesis and characterization of TiO2 powder

Abstract

In the present study, TiO2 powder having the tetragonal crystal without any impurity was easily synthesized by sol-gel method, and its characterization was done by X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray (EDX) spectroscopy. The crystallinity degree was found to be of 89.0%. A flaky morphology was observed.

Keywords

Sol-gel synthesis,TiO2,X-ray diffraction (XRD)

Kaynakça

  1. Chimupala Y, Hyett G, Simpson R, Mitchell R, Douthwaite R, Milne SJ, Brydson RD. Synthesis and characterization of mixed phase anatase TiO2 and sodium-doped TiO2(B) thin films by low pressure chemical vapour deposition (LPCVD). RSC Adv 2014;4:48507-15.
  2. Viana MM, Soares VF, Mohallem NDS. Synthesis and characterization of TiO2 nanoparticles. Ceram Int 2010;36:2047-53.
  3. Dadkhah M, Salavati-Niasari M, Mir N. Synthesis and characterization of TiO2 nanoparticles by using new shape controllers and its application in dye sensitized solar cells. J Ind Eng Chem 2014;20:4039-44.
  4. Paunović P, Grozdanov A, Češnovar A, Makreski P, Gentile G, Ranguelov B, Fidančevska E. Characterization of nanoscaled TiO2 produced by simplified sol–gel method using organometallic precursor. J Eng Mater Technol 2015;137:021003 1-5.
  5. Byranvand MM, Kharat AN, Fatholahi L, Beiranvand ZM. A review on synthesis of nano-TiO2 via different methods. J Nanostruct 2013;3:1-9.
  6. Li Z, Kawashita M, Doi M. Sol–gel synthesis and characterization of magnetic TiO2 microspheres. J Ceram Soc Jpn 2010;118:467-73.
  7. Chen X, Mao SS. Titanium dioxide nanomaterials: Synthesis, properties, modifications, and applications. Chem Rev 2007;107:2891-959.
  8. Phonkhokkong T, Thongtem T, Thongtem S, Phuruangrat A, Promnopas W. Synthesis and characterization of TiO2 nanopowders for fabrication of dye sensitized solar cells. Dig J Nanomater Biostruct 2016;11:81-9.
  9. Sharma A, Karn RK, Pandiyan SK. Synthesis of TiO2 nanoparticles by sol-gel method and their characterization. J Basic and Appl Eng Res 2014;1:1-5.
  10. Toyoda M, Nanbu Y, Nakazawa Y, Hirano M, Inagaki M. Effect of crystallinity of anatase on photoactivity for methyleneblue decomposition in water. Appl Catal B 2004;49: 227-32.

Kaynak Göster

APA
Kaygili, O., Bulut, N., Tatar, C., Ates, T., & İnce, T. (2017). Sol-gel synthesis and characterization of TiO2 powder. International Journal of Innovative Engineering Applications, 1(2), 38-40. https://izlik.org/JA57HS55WJ
AMA
1.Kaygili O, Bulut N, Tatar C, Ates T, İnce T. Sol-gel synthesis and characterization of TiO2 powder. ijiea, IJIEA. 2017;1(2):38-40. https://izlik.org/JA57HS55WJ
Chicago
Kaygili, Omer, Niyazi Bulut, Cengiz Tatar, Tankut Ates, ve Turan İnce. 2017. “Sol-gel synthesis and characterization of TiO2 powder”. International Journal of Innovative Engineering Applications 1 (2): 38-40. https://izlik.org/JA57HS55WJ.
EndNote
Kaygili O, Bulut N, Tatar C, Ates T, İnce T (01 Aralık 2017) Sol-gel synthesis and characterization of TiO2 powder. International Journal of Innovative Engineering Applications 1 2 38–40.
IEEE
[1]O. Kaygili, N. Bulut, C. Tatar, T. Ates, ve T. İnce, “Sol-gel synthesis and characterization of TiO2 powder”, ijiea, IJIEA, c. 1, sy 2, ss. 38–40, Ara. 2017, [çevrimiçi]. Erişim adresi: https://izlik.org/JA57HS55WJ
ISNAD
Kaygili, Omer - Bulut, Niyazi - Tatar, Cengiz - Ates, Tankut - İnce, Turan. “Sol-gel synthesis and characterization of TiO2 powder”. International Journal of Innovative Engineering Applications 1/2 (01 Aralık 2017): 38-40. https://izlik.org/JA57HS55WJ.
JAMA
1.Kaygili O, Bulut N, Tatar C, Ates T, İnce T. Sol-gel synthesis and characterization of TiO2 powder. ijiea, IJIEA. 2017;1:38–40.
MLA
Kaygili, Omer, vd. “Sol-gel synthesis and characterization of TiO2 powder”. International Journal of Innovative Engineering Applications, c. 1, sy 2, Aralık 2017, ss. 38-40, https://izlik.org/JA57HS55WJ.
Vancouver
1.Omer Kaygili, Niyazi Bulut, Cengiz Tatar, Tankut Ates, Turan İnce. Sol-gel synthesis and characterization of TiO2 powder. ijiea, IJIEA [Internet]. 01 Aralık 2017;1(2):38-40. Erişim adresi: https://izlik.org/JA57HS55WJ