3D yazıcı rezinlerin renk stabilitesinin karşılaştırılması

Yıl 2025, Cilt: 8 Sayı: 6, 988 - 994, 25.10.2025

Bengisu Koca , Serdar Akarsu , Sultan Aktuğ Karademir , Samet Atasoy

https://doi.org/10.32322/jhsm.1754175

Öz

Amaç:
Bu çalışmanın amacı, kahve solüsyonuna daldırma sonrası iki farklı 3D baskı reçinesi, bir CAD/CAM reçine nano-seramik blok ve bir nanohibrit kompozit reçinenin uzun dönem renk stabilitelerini karşılaştırmaktı.

Gereç ve Yöntem:
Farklı üretim teknikleriyle üretilmiş dört farklı reçine esaslı materyalden örnekler hazırlandı: Eksiltmeli üretim (Cerasmart – Grup CS), Eklemeli üretim (VarseoSmile Crown Plus – Grup VS, Crowntec – Grup CT) ve geleneksel direkt kompozit yöntem (Clearfil Majesty Esthetic – Grup CME). Örnekler, 30 gün boyunca her gün 45 dakika kahve solüsyonuna daldırıldı ve günün kalan süresinde distile suda saklandı. Renk ölçümleri 1., 7., 14. ve 30. günlerde spektrofotometre ile yapıldı. Renk değişimleri (ΔE), CIEDE2000 formülü kullanılarak hesaplandı. Veriler tek yönlü ANOVA testi ile analiz edildi, anlamlı farklılıklar Tukey testi ile değerlendirildi. p<0.05 değeri istatistiksel olarak anlamlı kabul edildi.

Bulgular:
30 günün sonunda en düşük renk değişimi Grup VS’de (ΔE = 4.69), en yüksek renk değişimi ise Grup CS’de (ΔE = 5.60) gözlendi. Ancak gruplar arasındaki fark istatistiksel olarak anlamlı değildi (p = 0.69).

Sonuç:
3D baskı reçinelerinin renk değişimi, CAD/CAM reçine nano-seramik bloklar ve konvansiyonel kompozit reçinelerle karşılaştırılabilir düzeydeydi. Ancak tüm materyaller klinik olarak kabul edilebilir eşik değerin (ΔE > 1.8) üzerinde renk değişimi gösterdi. 3D baskı reçineleri ve eklemeli üretim tekniklerinin renk stabilitesini değerlendirmek için daha fazla çalışmaya ihtiyaç vardır.

Anahtar Kelimeler

3D YAZICI RESİN , KOMPOZİT REZİN , RENK STABİLİTESİ , CAD-CAM

Comparison of color stability of different 3-D printed resins

Öz

Aims: This study aimed to compare the long-term color stability of two different 3D-printed resins, one CAD/CAM resin nanoceramic block, and one nanohybrid composite resin after immersion in a coffee solution.
Methods: Specimens were prepared from four resin-based materials produced via different manufacturing techniques: subtractive manufacturing (Cerasmart-group CS), additive manufacturing (VarseoSmile Crown Plus-group VS, Crowntec-group CT), and conventional methods (Clearfil Majesty Esthetic-group CME). The samples were immersed in coffee for 45 minutes daily over 30 days and stored in distilled water for the rest of the day. Color measurements were taken using a spectrophotometer on days 1, 7, 14, and 30. Color changes (ΔE) were calculated using the CIEDE2000 formula. Data were analyzed using one-way ANOVA, and post hoc comparisons were performed using the Tukey test. A p-value <0.05 was considered statistically significant.
Results: There were significant differences among the groups on days 1, 7 and 14. At the end of 30 days, the lowest color change was observed in group VS (ΔE=4.69), while the highest was in group CS (ΔE=5.60). The differences among groups were not statistically significant (p=0.69).
Conclusion: The color change of 3D-printed resins was comparable to that of CAD/CAM nanoceramic blocks and conventional composite resins. However, all materials exhibited color changes above the clinically acceptable threshold (ΔE>1.8). Further studies are needed to evaluate the color stability of 3D printing resins and additive manufacturing techniques.

Anahtar Kelimeler

3D printing , CAD/CAM , composite resin , discoloration

Kaynakça

• Jockusch J, Özcan M. Additive manufacturing of dental polymers: an overview on processes, materials and applications. Dent Mater J. 2020; 39(3):345-354. doi:10.4012/dmj.2019-123
• Sasany R, Donmez MB, de Paula MS, et al. Stainability and translucency of potassium aluminum sulfate applied computer-aided design and computer-aided manufacturing materials after coffee thermocycling. J Esthet Restor Dent. 2024;36(3):477-483. doi:10.1111/jerd.13154
• Bae EJ, Jeong ID, Kim WC, Kim JH. A comparative study of additive and subtractive manufacturing for dental restorations. J Prosthet Dent. 2017; 118(2):187-193. doi:10.1016/j.prosdent.2016.11.004
• Lopes AJ, Lee IH, MacDonald E, Quintana R, Wicker R. Laser curing of silver-based conductive inks for in situ 3D structural electronics fabrication in stereolithography. J Mater Process Technol. 2014;214(9): 1935-1945. doi:10.1016/j.jmatprotec.2014.04.009
• Kim S, Chung SH, Kim RJY, Park YS. Investigating the role of chlorogenic acids and coffee type in coffee-induced teeth discoloration. Acta Odontol Scand. 2024;82(1):1-8. doi:10.1080/00016357.2023.2245880
• Peñate L, Mercade M, Arregui M, Roig M, Basilio J, Cedeño R. Color stability of CAD/CAM interim material for long-term fixed dental prostheses vs. conventional materials after immersion in different staining solutions. J Compos Sci. 2021;5(4):106. doi:10.3390/jcs5040106
• Paravina RD, Pérez MM, Ghinea R. Acceptability and perceptibility thresholds in dentistry: a comprehensive review of clinical and research applications. J Esthet Restor Dent. 2019;31(2):103-112. doi:10.1111/jerd. 12465
• Azmy E, Al-Kholy MRZ, Gad MM, Al-Thobity AM, Emam AM, Helal MA. Influence of different beverages on the color stability of nanocomposite denture base materials. Int J Dent. 2021;2021:5861848. doi:10.1155/2021/5861848
• Paravina RD, Ghinea R, Herrera LJ, et al. Color difference thresholds in dentistry. J Esthet Restor Dent. 2015;27(Suppl 1):S1-S9. doi:10.1111/jerd.12149
• Arocha MA, Mayoral JR, Lefever D, Mercade M, Basilio J, Roig M. Color stability of siloranes versus methacrylate-based composites after immersion in staining solutions. Clin Oral Investig. 2013;17(16):1481-1487. doi:10.1007/s00784-012-0837-7
• Aydın N, Karaoğlanoğlu S, Oktay EA, Kılıçarslan MA. Investigating the color changes on resin-based CAD/CAM blocks. J Esthet Restor Dent. 2020;32(2):251-256. doi:10.1111/jerd.12561
• Awad D, Stawarczyk B, Liebermann A, Ilie N. Translucency of esthetic dental restorative CAD/CAM materials and composite resins with respect to thickness and surface roughness. J Prosthet Dent. 2015;113(6): 534-540. doi:10.1016/j.prosdent.2014.12.003
• Pecho OE, Ghinea R, do Amaral EAN, Cardona JC, Della Bona A, Pérez MM. Relevant optical properties for direct restorative materials. Dent Mater. 2016;32(5):e105-e112. doi:10.1016/j.dental.2016.02.008
• Mudhaffer S, Althagafi R, Haider J, Satterthwaite J, Silikas N. Effects of printing orientation and artificial ageing on martens hardness and indentation modulus of 3D printed restorative resin materials. Dent Mater. 2024;40(7):1003-1014. doi:10.1016/j.dental.2024.05.005
• Vichi A, Balestra D, Scotti N, Louca C, Paolone G. Translucency of CAD/CAM and 3D printable composite materials for permanent dental restorations. Polymers (Basel). 2023;15(6):1443. doi:10.3390/polym15061 443
• Turker I, Yuzbasioglu E. Optical properties of CAD/CAM interpenetrating phase composites-an overview. Glass Ceram. 2024; 81(5):217-224.
• Lemon MT, Jones MS, Stansbury JW. Hydrogen bonding interactions in methacrylate monomers and polymers. J Biomed Mater Res A. 2007; 83(3):734-746. doi:10.1002/jbm.a.31448
• Umaña Alfaro G. Efecto del post curado en las propiedades físicas y mecánicas de resinas dentales de impresión 3D para restauraciones definitivas [master’s thesis]. Ciudad: Universidad; 2024.
• Bozoğulları HN, Temizci T. Evaluation of the color stability, stainability, and surface roughness of permanent composite-based milled and 3D printed CAD/CAM restorative materials after thermocycling. Appl Sci. 2023;13(21):11895. doi:10.3390/app132111895
• Shin JW, Kim JE, Choi YJ, et al. Evaluation of the color stability of 3D-printed crown and bridge materials against various sources of discoloration: an in vitro study. Materials (Basel). 2020;13(23):5359. doi: 10.3390/ma13235359
• Ellakany P, Fouda SM, AlGhamdi MA, Aly NM. Comparison of the color stability and surface roughness of 3-unit provisional fixed partial dentures fabricated by milling, conventional and different 3D printing fabrication techniques. J Dent. 2023;131:104458. doi:10.1016/j.jdent.2023.104458
• Krajangta N, Klaisiri A, Leelaponglit S, Intralawan N, Tiansuwan P, Pisethsalasai N. Color alteration of CAD/CAM 3D-printed, milled resin-ceramic hybrid material compared to enamel. Dent Mater J. 2024; 43(3):386-393. doi:10.4012/dmj.2023-275
• Puebla K, Arcaute K, Quintana R, Wicker RB. Effects of environmental conditions, aging, and build orientations on the mechanical properties of ASTM type I specimens manufactured via stereolithography. Rapid Prototyp J. 2012;18(5):374-388. doi:10.1108/13552541211250373
• Unkovskiy A, Bui PH, Schille C, Geis-Gerstorfer J, Huettig F, Spintzyk S. Objects build orientation, positioning, and curing influence dimensional accuracy and flexural properties of stereolithographically printed resin. Dent Mater. 2018;34(12):e324-e333. doi:10.1016/j.dental.2018.09.011
• Yadav RD, Raisingani D, Jindal D, Mathur R. A comparative analysis of different finishing and polishing devices on nanofilled, microfilled, and hybrid composite: a scanning electron microscopy and profilometric study. Int J Clin Pediatr Dent. 2016;9(3):201-206. doi:10.5005/jp-journals-10005-1364
• Monzón M, Ortega Z, Hernández A, Paz R, Ortega F. Anisotropy of photopolymer parts made by digital light processing. Materials (Basel). 2017;10(1):64. doi:10.3390/ma10010064
• Tahayeri A, Morgan M, Fugolin AP, et al. 3D printed versus conventionally cured provisional crown and bridge dental materials. Dent Mater. 2018;34(2):192-200. doi:10.1016/j.dental.2017.10.003
• Lee EH, Ahn JS, Lim YJ, Kwon HB, Kim MJ. Effect of post-curing time on the color stability and related properties of a tooth-colored 3D-printed resin material. J Mech Behav Biomed Mater. 2022;126:104993. doi:10. 1016/j.jmbbm.2021.104993
• Wada J, Wada K, Gibreel M, et al. Effect of surface polishing on physical properties of an occlusal splint material for additive manufacturing under protection gas post-curing condition. Polymers (Basel). 2023; 15(3):625. doi:10.3390/polym15030625
• Devlukia S, Hammond L, Malik K. Is surface roughness of direct resin composite restorations material and polisher-dependent? A systematic review. J Esthet Restor Dent. 2023;35(6):947-967. doi:10.1111/jerd.13102
• Erturk-Avunduk AT, Atılan-Yavuz S, Filiz H, Cengiz-Yanardag E. A comparative study of polishing systems on optical properties and surface roughness of additively manufactured and conventional resin based composites. Sci Rep. 2024;14(1):25658. doi:10.1038/s41598-024-77449-9
• Özer NE, Şahin Z, Çöl CY, Arık Ö, Kılıçarslan MA. The effect of different staining solutions on the color stability of permanent indirect composite resins produced by additive and subtractive techniques. Meandros Med Dent J. 2024;25(3):262-278. doi:10.69601/meandrosmdj.1533026
• Alshali RZ, Salim NA, Satterthwaite JD, Silikas N. Long-term sorption and solubility of bulk-fill and conventional resin-composites in water and artificial saliva. J Dent. 2015;43(12):1511-1518. doi:10.1016/j.jdent. 2015.10.001
• Johnston WM. Color measurement in dentistry. J Dent. 2009;37(Suppl 1): e2-e6. doi:10.1016/j.jdent.2009.03.011
• Nagai T, Alfaraj A, Chu TMG, Yang CC, Lin WS. Color stability of CAD-CAM hybrid ceramic materials following immersion in artificial saliva and wine. J Prosthodont. 2024;33(3):279-285. doi:10.1111/jopr.13868