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Determination of Titanium in Zinc ash by FAAS After Digested using Ultrasound-Assisted Extraction

Yıl 2021, Cilt: 7 Sayı: 1, 147 - 154, 30.06.2021

Fatma Kurşun , Buse Dağcı Cemile Özcan

https://doi.org/10.34186/klujes.941163
Cited By: 2

Öz

In this study, it is aimed to determine the amount of Ti (titanium) in waste ash samples taken from galvanizing factories by using flame atomic absorption (FAAS). Various time periods and different solvent mixtures were examined by using ultrasound-assisted extraction for digestion of zinch ash which taken from various processes of galvanizing metal sheet or pipe. The best solvent mixtures for Ti metal in galvanized waste was found HCl:HNO3:H2O2 (1:3:2) > HCl > HNO3:HCl (1:3) > HNO3 > HNO3:H2SO4 (3:1) > HNO3:H2SO4 (1:1) > HNO3:H2SO4 (3:2) > HNO3:H2SO4 (2:1), respectively.

Anahtar Kelimeler

Ultrasound-assisted extraction waste ash Titanium solvent mixtures

Destekleyen Kurum

-

Proje Numarası

-

Teşekkür

-

Kaynakça

  • [1] Dvorak, P., Jandova, J., Hydrometallurgical recovery of zinc from hot dip galvanizing ash. Hydrometallurgy, C 77, S 29-33, 2005.
  • [2] Ahmer, C., Maaß, P., Peißker, P., Handbook of Hot-dip Galvanization. WILLEY-VCH Verlag GmbH & Co, KGaA, Weinheim, 2011.
  • [3] Delvasto, P., Casal-Ramos, J. A., González-Jordán, O., Durán-Rodríguez, N. C., Domínguez-Vargas, J. R., Moncada, P., Caracterización de residuos sólidos procedentes de dos procesos distintos de galvanizado en caliente por inmersión, Revista De Metalurgia, C 48(1), S 33-44, 2012.
  • [4] Trpcevska, J., Holkova, B., Briancin, J., Koralova, K., Piroskova J., The pyrometallurgical recovery of zinc from the coarse-grained fraction of zinc ash by centrifugal force, Int. J. Miner. Process., C 143, S 25-33, 2015.
  • [5]Url4<https://webdosya.csb.gov.tr/db/cygm/editordosya/Galvaniz_Kaplama_Kilavuzu.pdf>, erişim tarihi 13.06.2020.
  • [6] Ogden, H. R., Clifford, A. H., Rare Metals. Handbook, Reinhold Publishing Corporation, Chapman&Hall Ltd., London, UK,, S 559-579, 1961.
  • [7] Url-1<https://www.britannica.com/technology/titanium-processing/The-metal-and-its-alloys>, erişim tarihi 31.03.2020.
  • [8] Burke, R. A., Hazardous Materials Chemistry for Emergency Responders, CRC Press, S 51-516, 2013.
  • [9] Petry, C. F., Capeletti, L. B., Stedile, F. C., dos Santos, J. H. Z., Pozebon, D., Determination of Titanium and Vanadium in Ziegler-Natta Catalysts by Inductively Coupled Plasma Atomic Emissin Spectrometry, Analytical, Sciences, The Japan Society for Analytical Chemistry, C 22, S 855-859, 2006.
  • [10] Mirzaei, M. Naeini A. K., Determination of Trace Amounts of Titanium by Flame Atomic Absorption Spectrometry after Cloud Point Extraction, Journal of Analytical Chemistry, C 68(7), S 595-599, 2013.
  • [11] Harris, D. C., Quantitative Chemical Analysis (8th edition) Translation Editor: Türker, A.R., Ankara, 2015.

DETERMINATION OF TITANIUM IN ZINC ASH BY FAAS AFTER DIGESTED USING ULTRASOUND-ASSISTED EXTRACTION

Yıl 2021, Cilt: 7 Sayı: 1, 147 - 154, 30.06.2021

Fatma Kurşun , Buse Dağcı Cemile Özcan

https://doi.org/10.34186/klujes.941163
Cited By: 2

Öz

Bu çalışmada, alevli atomik absorpsiyon (FAAS) kullanılarak galvaniz fabrikalarından alınan atık kül örneklerindeki Ti (titanyum) miktarının belirlenmesi amaçlanmıştır. Çeşitli galvanizleme sac veya boru proseslerinden elde edilen çinko külünün çözünürleştirilmesi için ses destekli ekstraksiyon kullanılarak çeşitli zaman periyotları ve farklı çözücü karışımları incelenmiştir. Galvanizli atıkta Ti metali için en iyi çözücü karışımları sırasıyla, HCl:HNO3:H2O2 (1:3:2) > HCl > HNO3:HCl (1:3) > HNO3 > HNO3:H2SO4 (3:1) > HNO3:H2SO4 (1:1) > HNO3:H2SO4 (3:2) > HNO3:H2SO4 (2:1) olarak bulunmuştur.

Anahtar Kelimeler

Ses destekli ekstraksiyon atık kül Titanyum çözücü karışımları

Proje Numarası

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Kaynakça

  • [1] Dvorak, P., Jandova, J., Hydrometallurgical recovery of zinc from hot dip galvanizing ash. Hydrometallurgy, C 77, S 29-33, 2005.
  • [2] Ahmer, C., Maaß, P., Peißker, P., Handbook of Hot-dip Galvanization. WILLEY-VCH Verlag GmbH & Co, KGaA, Weinheim, 2011.
  • [3] Delvasto, P., Casal-Ramos, J. A., González-Jordán, O., Durán-Rodríguez, N. C., Domínguez-Vargas, J. R., Moncada, P., Caracterización de residuos sólidos procedentes de dos procesos distintos de galvanizado en caliente por inmersión, Revista De Metalurgia, C 48(1), S 33-44, 2012.
  • [4] Trpcevska, J., Holkova, B., Briancin, J., Koralova, K., Piroskova J., The pyrometallurgical recovery of zinc from the coarse-grained fraction of zinc ash by centrifugal force, Int. J. Miner. Process., C 143, S 25-33, 2015.
  • [5]Url4<https://webdosya.csb.gov.tr/db/cygm/editordosya/Galvaniz_Kaplama_Kilavuzu.pdf>, erişim tarihi 13.06.2020.
  • [6] Ogden, H. R., Clifford, A. H., Rare Metals. Handbook, Reinhold Publishing Corporation, Chapman&Hall Ltd., London, UK,, S 559-579, 1961.
  • [7] Url-1<https://www.britannica.com/technology/titanium-processing/The-metal-and-its-alloys>, erişim tarihi 31.03.2020.
  • [8] Burke, R. A., Hazardous Materials Chemistry for Emergency Responders, CRC Press, S 51-516, 2013.
  • [9] Petry, C. F., Capeletti, L. B., Stedile, F. C., dos Santos, J. H. Z., Pozebon, D., Determination of Titanium and Vanadium in Ziegler-Natta Catalysts by Inductively Coupled Plasma Atomic Emissin Spectrometry, Analytical, Sciences, The Japan Society for Analytical Chemistry, C 22, S 855-859, 2006.
  • [10] Mirzaei, M. Naeini A. K., Determination of Trace Amounts of Titanium by Flame Atomic Absorption Spectrometry after Cloud Point Extraction, Journal of Analytical Chemistry, C 68(7), S 595-599, 2013.
  • [11] Harris, D. C., Quantitative Chemical Analysis (8th edition) Translation Editor: Türker, A.R., Ankara, 2015.
Toplam 11 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Mühendislik
Bölüm Sayı
Yazarlar

Fatma Kurşun 0000-0003-0212-0973

Buse Dağcı Bu kişi benim 0000-0001-9363-9951

Cemile Özcan 0000-0002-2954-0612

Proje Numarası -
Yayımlanma Tarihi 30 Haziran 2021
Yayımlandığı Sayı Yıl 2021 Cilt: 7 Sayı: 1

Kaynak Göster

APA Kurşun, F., Dağcı, B., & Özcan, C. (2021). Determination of Titanium in Zinc ash by FAAS After Digested using Ultrasound-Assisted Extraction. Kirklareli University Journal of Engineering and Science, 7(1), 147-154. https://doi.org/10.34186/klujes.941163

Cited By

Determination of lead and cadmium by magnetic solid-phase extraction (MSPE) using Co3O4@Fe3O4 nanoflowers and flame atomic absorption spectrometry (FAAS)
Chemical Papers
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Efficiency of Ag3PO4/TiO2 as a heterogeneous catalyst under solar and visible light for humic acid removal from aqueous solution
Heliyon
https://doi.org/10.1016/j.heliyon.2023.e15678