Araştırma Makalesi
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İndüktif Eşleşmiş Plazma Optik Emisyon Spektroskopisi ile Patates, Elma ve Mısırda Ağır Metal Tayini

Yıl 2017, Cilt: 8 Sayı: 2, 196 - 201, 11.09.2017

Öz

Bu çalışmada, Burdur bölgesinde yetiştirilen ve
Burdur Merkez yerel pazarından satın alınan patates, elma ve mısır örneklerinde
bazı ağır metallerin (As, Bi, Cd, Co, Cu, Mn, Mo, Ni, Pb, Sb, V, Zn) tayini
indüktif eşleşmiş plazma optik emisyon spektroskopisi (ICPOES) ile
gerçekleştirilmiştir. Patates ve elma örnekleri kuru yakma, mısır örnekleri ise
yaş yakma tekniği kullanarak çözünür hale getirilmiştir. ICPOES tekniği ile
örneklerin kantitatif analizinde kalibrasyon yöntemi kullanılmış ve sonuçlar
%95 güven seviyesinde verilmiştir.

Kaynakça

  • Algül, I., Kara, D. (2014). Determination and chemometric evaluation of total aflatoxin, aflatoxin B1, ochratoxin A and heavy metals content in corn flours from Turkey. Food Chemistry 157: 70–76.
  • Altundağ , H., Tüzen, M. (2011). Comparison of dry, wet and microwave digestion methods for the multi element determination in some dried fruit samples by ICP-OES. Food and Chemical Toxicology 49: 2800–2807.
  • Amorello, D., Barreca, S., Bruno, M., Milia, A., Orecchio, S., Pettignano, A. (2016). Chemical characterization of ancient liturgical vestment (chasuble) by Inductively Coupled Plasma–Optical Emission Spectrometry (ICP–OES). Microchemical Journal 129: 305–309.
  • Asaduzzaman, K., Khandaker, M.U., Baharudin, N.A.B., Amin, Y. B.M., Farook, M. S., Bradley, D.A., Mahmoud, O. (2017). Heavy metals in human teeth dentine: A bio-indicator of metals exposure and environmental pollution. Chemosphere 176: 221-230.
  • Bressy, F.C., Brito, G. B., Barbosa, I.S., Teixeira, L.S.G., Korn, M.G.A. (2013). Determination of trace element concentrations in tomato samples at different stages of maturation by ICP OES and ICP-MS following microwave-assisted digestion. Microchemical Journal 109: 145–149.
  • Chen, L., Wu, C., Du, P., Feng, X., Wu, P., Cai, C. (2017). Electrolyzing synthesis of boron-doped graphene quantum dots for fluorescence determination of Fe3+ ions in water samples. Talanta 164:100–109.
  • Cindric´, I.J., Krizman, I., Zeiner , M., Kampic´, Š, Medunic´, G., Stingeder, G. (2012). ICP-AES determination of minor and major elements in apples after microwave assisted digestion. Food Chemistry 135: 2675–2680.
  • Dahaghin, Z., Mousavi, H.Z., Sajjadi, S.M. (2017). Trace amounts of Cd(II), Cu(II) and Pb(II) ions monitoring using Fe3O4@ graphene oxide nanocomposite modified via 2-mercaptobenzothiazole as a novel and efficient nanosorbent. Journal of Molecular Liquids 231: 386–395.
  • Duran, A., Tüzen, M., Soylak, M. (2008). Trace element levels in some dried fruit samples from Turkey. International Journal of Food Sciences and Nutrition 59(7-8): 581-589.
  • Fan, W., Qiao, J., Guan, X. (2017). Multi-wavelength spectrophotometric determination of Cr(VI) in water with ABTS. Chemosphere 171: 460-467.
  • Hashmi, D. R., Khan, F. A., Shaikh, G. H., Usmani, T. H. (2005). Determination of trace metals in the vegetables procured from local markets of Karachi City by atomic absorption spectrophometry. Journal of the Chemical Society of Pakistan 27(4): 353-357.
  • Altundağ, H., Tüzen, M. (2011). Comparison of dry, wet and microwave digestion methods for the multi element determination in some dried fruit samples by ICP-OES. Food and Chemical Toxicology 49: 2800–2807.
  • Karadaş, C., Kara, D. (2017). Dispersive liquid–liquid microextraction based on solidification of floating organic drop for preconcentration and determination of trace amounts of copper by flame atomic absorption spectrometry. Food Chemistry 220: 242–248.
  • Koduru , J.R., Lee, K.D. (2014). Evaluation of thiosemicarbazone derivative as chelating agent for the simultaneous removal and trace determination of Cd(II) and Pb(II) in food and water samples. Food Chemistry 150: 1–8.
  • Nan, Z., Cheng, G. (2001). Copper and zinc uptake by Spring Wheat (Triticum aestivum L.) and Corn (Zea mays L.) Grown in Baiyin Region. Bulletin of Environmental Contamination and Toxicology 67: 83–90.
  • Öztürk, E., Atsan, E., Polat, T., Kara, K. (2011). Variation in heavy metal concentrations of potato (Solanum Tuberosum L.) Cultivars. The Journal of Animal & Plant Sciences, 21(2): 235-239.
  • Radwan, M.A., Salama, A.K. (2006). Market basket survey for some heavy metals in Egyptian fruits and vegetables. Food and Chemical Toxicology 44: 1273–1278.
  • Ragi, A.S., Leena, P.P., Cheriyan, E., Nair, S.M. (2017). Heavy metal concentrations in some gastropods and bivalves collected from the fishing zone of South India. Marine Pollution Bulletin 118: 452–458.
  • Rasouli, Z., Hassanzadeh,Z., Ghavami, R. (2016). Application of a new version of GA-RBF neural network for simultaneous spectrophotometric determination of Zn(II), Fe(II), Co(II) and Cu(II) in rea lsamples: An explorator study of their complexation abilities toward MTB. Talanta160: 86–98.
  • Tokalıoğlu, Ş., Papak, A., Kartal, Ş. (2017). Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry. Arabian Journal of Chemistry 10: 9–23.
  • Tüzen, M., Soylak, M. (2007). Evaluation of trace element contents in canned foods marketed from Türkey. Food Chemistry 102: 1089–1095.
  • Vareda, J.P., Valente, A.J.M., Durães, L. (2016). Heavy metals in Iberian soils: Removal by current adsorbents/ amendments and prospective for aerogels. Advances in Colloid and Interface Science 237: 28–42.
  • Zinoubi, K., Majdoub, H., Barhoumi, H., Boufi, S., Jaffrezic-Renault, N. (2017). Determination of trace heavy metal ions by anodic stripping voltammetry using nanofibrillated cellulose modified electrode. Journal of Electroanalytical Chemistry 799: 70–77.

Determination of Some Heavy Metals in Patato, Apple and Corn by Inductively Coupled Plasma Optical Emission Spectroscopy

Yıl 2017, Cilt: 8 Sayı: 2, 196 - 201, 11.09.2017

Öz

In this study, the heavy
metals (As, Bi, Cd, Co, Cu, Mn, Mo, Ni, Pb, Sb, V, Zn) in the patato, apple and
corn samples grown in Burdur Region and obtained from Burdur Center local
bazaar were determined by Inductively Coupled Plasma Optical Emission
Spectroscopy (ICPOES). Potato and apple samples were solubilized using dry
ashing, while corn samples were solubilized using wet ashing technique. The
calibration method was applied for the quantitative analysis of the samples and
the results are given at 95% of confidence level.

Kaynakça

  • Algül, I., Kara, D. (2014). Determination and chemometric evaluation of total aflatoxin, aflatoxin B1, ochratoxin A and heavy metals content in corn flours from Turkey. Food Chemistry 157: 70–76.
  • Altundağ , H., Tüzen, M. (2011). Comparison of dry, wet and microwave digestion methods for the multi element determination in some dried fruit samples by ICP-OES. Food and Chemical Toxicology 49: 2800–2807.
  • Amorello, D., Barreca, S., Bruno, M., Milia, A., Orecchio, S., Pettignano, A. (2016). Chemical characterization of ancient liturgical vestment (chasuble) by Inductively Coupled Plasma–Optical Emission Spectrometry (ICP–OES). Microchemical Journal 129: 305–309.
  • Asaduzzaman, K., Khandaker, M.U., Baharudin, N.A.B., Amin, Y. B.M., Farook, M. S., Bradley, D.A., Mahmoud, O. (2017). Heavy metals in human teeth dentine: A bio-indicator of metals exposure and environmental pollution. Chemosphere 176: 221-230.
  • Bressy, F.C., Brito, G. B., Barbosa, I.S., Teixeira, L.S.G., Korn, M.G.A. (2013). Determination of trace element concentrations in tomato samples at different stages of maturation by ICP OES and ICP-MS following microwave-assisted digestion. Microchemical Journal 109: 145–149.
  • Chen, L., Wu, C., Du, P., Feng, X., Wu, P., Cai, C. (2017). Electrolyzing synthesis of boron-doped graphene quantum dots for fluorescence determination of Fe3+ ions in water samples. Talanta 164:100–109.
  • Cindric´, I.J., Krizman, I., Zeiner , M., Kampic´, Š, Medunic´, G., Stingeder, G. (2012). ICP-AES determination of minor and major elements in apples after microwave assisted digestion. Food Chemistry 135: 2675–2680.
  • Dahaghin, Z., Mousavi, H.Z., Sajjadi, S.M. (2017). Trace amounts of Cd(II), Cu(II) and Pb(II) ions monitoring using Fe3O4@ graphene oxide nanocomposite modified via 2-mercaptobenzothiazole as a novel and efficient nanosorbent. Journal of Molecular Liquids 231: 386–395.
  • Duran, A., Tüzen, M., Soylak, M. (2008). Trace element levels in some dried fruit samples from Turkey. International Journal of Food Sciences and Nutrition 59(7-8): 581-589.
  • Fan, W., Qiao, J., Guan, X. (2017). Multi-wavelength spectrophotometric determination of Cr(VI) in water with ABTS. Chemosphere 171: 460-467.
  • Hashmi, D. R., Khan, F. A., Shaikh, G. H., Usmani, T. H. (2005). Determination of trace metals in the vegetables procured from local markets of Karachi City by atomic absorption spectrophometry. Journal of the Chemical Society of Pakistan 27(4): 353-357.
  • Altundağ, H., Tüzen, M. (2011). Comparison of dry, wet and microwave digestion methods for the multi element determination in some dried fruit samples by ICP-OES. Food and Chemical Toxicology 49: 2800–2807.
  • Karadaş, C., Kara, D. (2017). Dispersive liquid–liquid microextraction based on solidification of floating organic drop for preconcentration and determination of trace amounts of copper by flame atomic absorption spectrometry. Food Chemistry 220: 242–248.
  • Koduru , J.R., Lee, K.D. (2014). Evaluation of thiosemicarbazone derivative as chelating agent for the simultaneous removal and trace determination of Cd(II) and Pb(II) in food and water samples. Food Chemistry 150: 1–8.
  • Nan, Z., Cheng, G. (2001). Copper and zinc uptake by Spring Wheat (Triticum aestivum L.) and Corn (Zea mays L.) Grown in Baiyin Region. Bulletin of Environmental Contamination and Toxicology 67: 83–90.
  • Öztürk, E., Atsan, E., Polat, T., Kara, K. (2011). Variation in heavy metal concentrations of potato (Solanum Tuberosum L.) Cultivars. The Journal of Animal & Plant Sciences, 21(2): 235-239.
  • Radwan, M.A., Salama, A.K. (2006). Market basket survey for some heavy metals in Egyptian fruits and vegetables. Food and Chemical Toxicology 44: 1273–1278.
  • Ragi, A.S., Leena, P.P., Cheriyan, E., Nair, S.M. (2017). Heavy metal concentrations in some gastropods and bivalves collected from the fishing zone of South India. Marine Pollution Bulletin 118: 452–458.
  • Rasouli, Z., Hassanzadeh,Z., Ghavami, R. (2016). Application of a new version of GA-RBF neural network for simultaneous spectrophotometric determination of Zn(II), Fe(II), Co(II) and Cu(II) in rea lsamples: An explorator study of their complexation abilities toward MTB. Talanta160: 86–98.
  • Tokalıoğlu, Ş., Papak, A., Kartal, Ş. (2017). Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry. Arabian Journal of Chemistry 10: 9–23.
  • Tüzen, M., Soylak, M. (2007). Evaluation of trace element contents in canned foods marketed from Türkey. Food Chemistry 102: 1089–1095.
  • Vareda, J.P., Valente, A.J.M., Durães, L. (2016). Heavy metals in Iberian soils: Removal by current adsorbents/ amendments and prospective for aerogels. Advances in Colloid and Interface Science 237: 28–42.
  • Zinoubi, K., Majdoub, H., Barhoumi, H., Boufi, S., Jaffrezic-Renault, N. (2017). Determination of trace heavy metal ions by anodic stripping voltammetry using nanofibrillated cellulose modified electrode. Journal of Electroanalytical Chemistry 799: 70–77.
Toplam 23 adet kaynakça vardır.

Ayrıntılar

Bölüm Araştırma Makalesi
Yazarlar

Yasin Arslan

Diğdem Trak Bu kişi benim

Fatma Tomul

Erdal Kendüzler

Yayımlanma Tarihi 11 Eylül 2017
Kabul Tarihi 12 Eylül 2017
Yayımlandığı Sayı Yıl 2017 Cilt: 8 Sayı: 2

Kaynak Göster

APA Arslan, Y., Trak, D., Tomul, F., Kendüzler, E. (2017). İndüktif Eşleşmiş Plazma Optik Emisyon Spektroskopisi ile Patates, Elma ve Mısırda Ağır Metal Tayini. Mehmet Akif Ersoy Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 8(2), 196-201.