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Germanyum piramit dizisinin etkin yüzey silanizasyonu ve floresan etiketlenmesi: Optimizasyon ve karakterizasyon

Yıl 2024, Cilt: 13 Sayı: 4, 1127 - 1138, 15.10.2024
https://doi.org/10.28948/ngumuh.1449020

Öz

Günümüzde homojen germanyum (Ge) piramit dizileri güneş hücreleri, fotodedektörler ve yeni nesil yarı iletken lazerler gibi pek çok uygulama alanında karşımıza çıkmaktadır. Germanyum piramit yüzeylerin kullanım alanlarının daha çok geliştirilebilmesi kimyasal ve biyolojik sensör gibi uygulamalarda da aktif olarak kullanılabilmesi için bu yüzeylerin biyolojik moleküllere hızlı cevap verecek şekilde modifiye edilmesi gerekmektedir. Bu çalışmada germanyum piramit yüzeylerinin 3-aminopropiltrietoksisilan (APTES) ile modifiye edilerek biyolojik molekülere açık olacak şekilde işlevselleştirilmesi için basit ve düşük maliyetli bir yöntem araştırılmıştır. APTES'in germanyum yüzeylerinde varlığını belirlemek için APTES ile modifiye edilmiş germanyum yüzeyler floresan BODIPY molekülleri ile etiketlenmiştir. Silanizasyon süreci boyunca, reaksiyon süresi ve reaksiyon sıcaklığının yığınsal germanyum ve piramit dizisine yerleşen APTES molekülleri üzerindeki etkileri araştırılmıştır. Farklı reaksiyonlarla üretilen numuneler, fotolüminesans spektroskopisi (PL) ve floresan yaşam ömrü görüntüleme mikroskobu (FLIM) ile karakterize edilmiştir. APTES moleküllerinin oldukça iyi bir yüzey tutunması sağlayabilmesi için optimum reaksiyon süresi ve işlem sıcaklığı sırasıyla 24 saat ve 60 0C olarak belirlenmiştir. FLIM mikroskobu ile görüntülenen piramitler üzerinde BODIPY moleküllerinin yaşam ömrü 2,4 ns olarak ölçülmüştür. APTES uygulaması elektronik açıdan önemli yarı iletken yüzeylerde çeşitli molekülleri hareketsiz hale getirmek ve yüksek performanslı yeni optoelektronik cihazlar üretmek için sağlam ve güvenilir bir yol sunabilir.

Proje Numarası

114F451 ve 16-M-15

Kaynakça

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Efficient surface silanization and fluorescent labelling of germanium pyramid array: Optimization and characterization

Yıl 2024, Cilt: 13 Sayı: 4, 1127 - 1138, 15.10.2024
https://doi.org/10.28948/ngumuh.1449020

Öz

Nowadays homogeneous germanium (Ge) pyramid arrays are emerging in many application areas such as solar cells, photodetectors and next-generation semiconductor lasers. To enhance the application areas of germanium pyramid surfaces, particularly in chemical and biological sensors, these surfaces need to be modified to rapidly respond to biological molecules. In this work, a simple and cost-effective method was investigated to modify germanium pyramid surfaces with 3-aminopropyltriethoxysilane (APTES), enabling them to be functionalized for interaction with biological molecules. In order to establish the presence of APTES on germanium surfaces, APTES modified surfaces were labeled with fluorescent BODIPY molecules. During the silanization process, the effects of reaction time and reaction temperature were studied for the attachment of APTES on bulk germanium and pyramid array. The products of different reactions were characterized using photoluminescence spectroscopy (PL) and fluorescence lifetime imaging microscopy (FLIM). The optimum reaction time and processing temperature for a reasonably good surface coverage by APTES molecules were determined as 24 hour and 60 0C, respectively. The fluorescence lifetime of BODIPY molecules on pyramids monitored with FLIM microscope was measured as 2.4 ns. APTES treatment can offer a robust and reliable pathway to immobilize various molecules on electronically important semiconductor surfaces and fabricate new optoelectronic devices with high performance.

Proje Numarası

114F451 ve 16-M-15

Kaynakça

  • S. Suresh, Semiconductor Nanomaterials, Methods and Applications: A Review. Nanoscience and Nanotechnology, 3(3), 62, 2013. http://article.sapub.org/10.5923.j.nn.20130303.06.html
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  • A.K. Katiyar, A.K. Sinha, S. Manna and S.K. Ray, Fabrication of Si/ZnS radial nanowire heterojunction arrays for white light emitting devices on Si substrates. ACS Applied Materials and Interfaces, 6(17), 15007, 2014. https://doi.org/10.1021/am5028605.
  • S. Kato, Y. Kurokawa, K. Gotoh and T. Soga, Silicon nanowire heterojunction solar cells with an Al2O3 passivation film fabricated by atomic layer deposition. nanoscale research letters, 14(99), 1, 2019. https://doi.org/10.1186/s11671-019-2930-1
  • S. Jeong, E.C. Garnett, S. Wang, Z. Yu, S. Fan, M.L. Brongersma, M.D. McGehee and Y. Cui, Hybrid silicon nanocone–polymer solar cells. nano letters, 12(6), 2971, 2012. https://doi.org/10.1021/nl300713x.
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  • A.Razzaq, V. Depauw, J. Cho, H.S. Radhakrishnan, I. Gordon, J. Szlufcik, Y. Abdulraheem and J.Poortmans, Periodic inverse nanopyramid gratings for light management in silicon heterojunction devices and comparison with random pyramid texturing. Solar Energy Materials and Solar Cells, 206, 110263, 2020. https://doi.org/10.1016/j.solmat.2019.110263.
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  • H. Hafeez, D. K. Choi, C. M. Lee, P. J. Jesuraj, D. H. Kim, A. Song, K. B. Chung, M. Song, J. F. Ma, C.-S. Kim and S.Y. Ryu, Replacement of n-type layers with a non-toxic APTES interfacial layer to improve the performance of amorphous Si thin-film solar cells. RSC Advances, 9, 7536, 2019. https://doi.org/ 10.1039/C8RA07409G.
  • N. Aissaoui, L. Bergaoui, J. Landoulsi, J.-F. Lambert and S. Boujday, Silane Layers on Silicon Surfaces: Mechanism of Interaction, Stability and Influence on Protein Adsorption. Langmuir, 28, 656, 2012. https://doi.org/10.1021/la2036778.
  • P. Saengdee, W. Chaisriratanakul, W. Bunjongpru, W. Sripumkhai, A. Srisuwan, W. Jeamsaksiri, C. Hruanun, A. Poyai and C. Promptmas, Surface modification of silicon dioxide, silicon nitride and titanium oxynitride for lactate dehydrogenase immobilization. Biosensors and Bioelectronics, 67, 134, 2015. http://dx.doi.org/10.1016/j.bios.2014.07.057.
  • N. Majoul, S. Aouida and B. Bessaïs, Progress of porous silicon APTES-functionalization by FTIR investigations. Applied Surface Science, 331, 388, 2015. https://doi.org/10.1016/j.apsusc.2015.01.107.
  • M. Hiraoui, M. Guendouz, N. Lorrain, A. Moadhen, L. Haji and M. Oueslati, Spectroscopy studies of functionalized oxidized porous silicon surface for biosensing applications. Materials Chemistry and Physics, 128, 151, 2011. https://doi.org/10.1016/ j.matchemphys.2011.02.052.
  • E. Makila, L.M. Bimbo, M. Kaasalainen, B. Herranz, A.J. Airaksinen, M. Heinonen, E. Kukk, J. Hirvonen, H.A. Santos and J. Salonen, Amine modification of thermally carbonized porous silicon with silane coupling chemistry. Langmuir 28, 14045, 2012. https://doi.org/10.1021/la303091k.
  • S.G. Coombs, S. Khodjaniyazova and F.V. Bright, Exploiting the 3-Aminopropyltriethoxysilane (APTES) autocatalytic nature to create bioconjugated microarrays on hydrogen-passivated porous silicon. Talanta, 177, 26, 2018. https://doi.org/10.1016/ j.talanta.2017.09.038.
  • L. De Stefano, G. Oliviero, J. Amato, N. Borbone, G. Piccialli, L. Mayol, I. Rendina, M. Terracciano and I. Rea, Aminosilane functionalizations of mesoporous oxidized silicon for oligonucleotide synthesis and detection. J R Soc Interface, 10, 20130160, 2013. http://dx.doi.org/10.1098/rsif.2013.0160.
  • B. Qiao, T.J. Wang, H. Gao and Y. Jin, High density silanization of nano-silica particles using γ-aminopropyltriethoxysilane (APTES). Applied Surface Science, 351, 646, 2015. https://doi.org/10.1016/ j.apsusc.2015.05.174.
  • A. Miranda, L. Martínez and P. A. Beule, Facile synthesis of an aminopropylsilane layer on Si/SiO2 substrates using ethanol as APTES solvent. MethodsX, 7, 100931, 2020. https://doi.org/10.1016/ j.mex.2020.100931.
  • E.J. Cueto-Diaz, A. Castro-Muniz, F. Suarez-Garcia, S. Galvez-Martinez, M.C. Torquemada-Vico, M.P. Valles-Gonzalez and E. Mateo-Marti, APTES-based silica nanoparticles as a potential modifier for the selective sequestration of CO2 gas molecules. Nanomaterials, 11, 2893, 2021. https://doi.org/10.3390/nano11112893.
  • S. Ahoulou, E. Perret and J.-M. Nedelec, Functionalization and characterization of silicon nanowires for sensing applications: A review. Nanomaterials, 11, 999, 2021. https://doi.org/10.3390/nano11040999.
  • Y. Liang, J. Huang, P. Zang, J. Kim and W. Hu, Molecular layer deposition of APTES on silicon nanowire biosensors: Surface characterization, stability and pH response. Applied Surface Science, 322, 202, 2014. https://doi.org/10.1016/j.apsusc.2014.10.097.
  • S. Mirsian, A.Khodadadian, M. Hedayati, A.Manzour-ol-Ajdad, R. Kalantarinejad and C. Heitzinger, A new method for selective functionalization of silicon nanowire sensors and Bayesian inversion for its parameters. Biosensors and Bioelectronics, 142, 111527, 2019. https://doi.org/10.1016/ j.bios.2019.111527.
  • S. Laumier, T. Farrow, H.Zalinge, L.Seravalli, M. Bosi and I. Sandall, Selection and functionalization of germanium nanowires for bio-sensing. ACS Omega,7(39), 35288, 2022. https://doi.org/ 10.1021/acsomega.2c04775.
  • Q. Han, Y. Fu, L.Jin, J. Zhao, Z. Xu, F. Fang, J. Gao, W. Yu, Germanium nanopyramid arrays showing near-100% absorption in the visible regime. Nano Res. 8, 2216, 2015. https://doi.org/10.1007/s12274-015-0731-0K.
  • Y. Kim, N. Lam, K. Kim, W. Park, J. Lee, Ge nanopillar solar cells epitaxially grown by metalorganic chemical vapor deposition. Sci. Rep. 7, 42693, 2017. https://doi.org/10.1038/srep42693.
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  • Açıkgöz ve H. Yungevis, GaAs yarı iletken yüzeyinde mikro yarıkların üretilmesi ve FLIM tekniği ile yüzey karakterizasyonu. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, 11(3), 826, 2022. https://doi.org/10.28948/ngumuh.1082122.
  • V. Rozyyev, J.G. Murphy, E. Barry, A.U. Mane, S.J. Sibener, J.W. Elam, Vapor-phase grafting of a model aminosilane compound to Al2O3, ZnO, and TiO2 surfaces prepared by atomic layer deposition. Applied Surface Science, 562, 149996, 2021. https://doi.org/10.1016/j.apsusc.2021.149996.
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  • Z. Xu, Q. Liu and J.A. Finch, Silanation and stability of 3-aminopropyl triethoxy silane on nanosized superparamagnetic particles:I. Direct silanation. Applied Surface Science, 120, 269, 1997. https://doi.org/10.1016/S0169-4332(97)00234-1.
  • M. Terracciano, I. Rea, J. Politi, L. De Stefano, Optical characterization of aminosilane-modified silicon dioxide surface for biosensing. J. Europ. Opt. Soc. Rap. Public. 8, 13075, 2013. http://dx.doi.org/ 10.2971/jeos.2013.13075.
  • P. Saengdee, C. Promptmas, S. Thanapitak, A. Srisuwan, A. Pankiew, N. Thornyanadacha, W. Chaisriratanakul, E. Chaowicharat, W. Jeamsaksiri, Optimization of 3-aminopropyltriethoxysilane functionalization on silicon nitride surface for biomolecule immobilization. Talanta 207, 120305, 2020. https://doi.org/10.1016/j.talanta.2019.120305.
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Toplam 65 adet kaynakça vardır.

Ayrıntılar

Birincil Dil Türkçe
Konular Elektronik,Optik ve Manyetik Malzemeler, Malzeme Karekterizasyonu
Bölüm Araştırma Makaleleri
Yazarlar

Sabriye Açıkgöz 0000-0002-2020-7565

Hasan Yüngeviş 0000-0001-5451-3379

Ayşegül Şahin 0000-0002-3238-6409

Emin Özünal 0000-0002-3389-9062

Proje Numarası 114F451 ve 16-M-15
Erken Görünüm Tarihi 4 Eylül 2024
Yayımlanma Tarihi 15 Ekim 2024
Gönderilme Tarihi 12 Mart 2024
Kabul Tarihi 15 Temmuz 2024
Yayımlandığı Sayı Yıl 2024 Cilt: 13 Sayı: 4

Kaynak Göster

APA Açıkgöz, S., Yüngeviş, H., Şahin, A., Özünal, E. (2024). Germanyum piramit dizisinin etkin yüzey silanizasyonu ve floresan etiketlenmesi: Optimizasyon ve karakterizasyon. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, 13(4), 1127-1138. https://doi.org/10.28948/ngumuh.1449020
AMA Açıkgöz S, Yüngeviş H, Şahin A, Özünal E. Germanyum piramit dizisinin etkin yüzey silanizasyonu ve floresan etiketlenmesi: Optimizasyon ve karakterizasyon. NÖHÜ Müh. Bilim. Derg. Ekim 2024;13(4):1127-1138. doi:10.28948/ngumuh.1449020
Chicago Açıkgöz, Sabriye, Hasan Yüngeviş, Ayşegül Şahin, ve Emin Özünal. “Germanyum Piramit Dizisinin Etkin yüzey Silanizasyonu Ve Floresan Etiketlenmesi: Optimizasyon Ve Karakterizasyon”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 13, sy. 4 (Ekim 2024): 1127-38. https://doi.org/10.28948/ngumuh.1449020.
EndNote Açıkgöz S, Yüngeviş H, Şahin A, Özünal E (01 Ekim 2024) Germanyum piramit dizisinin etkin yüzey silanizasyonu ve floresan etiketlenmesi: Optimizasyon ve karakterizasyon. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 13 4 1127–1138.
IEEE S. Açıkgöz, H. Yüngeviş, A. Şahin, ve E. Özünal, “Germanyum piramit dizisinin etkin yüzey silanizasyonu ve floresan etiketlenmesi: Optimizasyon ve karakterizasyon”, NÖHÜ Müh. Bilim. Derg., c. 13, sy. 4, ss. 1127–1138, 2024, doi: 10.28948/ngumuh.1449020.
ISNAD Açıkgöz, Sabriye vd. “Germanyum Piramit Dizisinin Etkin yüzey Silanizasyonu Ve Floresan Etiketlenmesi: Optimizasyon Ve Karakterizasyon”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 13/4 (Ekim 2024), 1127-1138. https://doi.org/10.28948/ngumuh.1449020.
JAMA Açıkgöz S, Yüngeviş H, Şahin A, Özünal E. Germanyum piramit dizisinin etkin yüzey silanizasyonu ve floresan etiketlenmesi: Optimizasyon ve karakterizasyon. NÖHÜ Müh. Bilim. Derg. 2024;13:1127–1138.
MLA Açıkgöz, Sabriye vd. “Germanyum Piramit Dizisinin Etkin yüzey Silanizasyonu Ve Floresan Etiketlenmesi: Optimizasyon Ve Karakterizasyon”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, c. 13, sy. 4, 2024, ss. 1127-38, doi:10.28948/ngumuh.1449020.
Vancouver Açıkgöz S, Yüngeviş H, Şahin A, Özünal E. Germanyum piramit dizisinin etkin yüzey silanizasyonu ve floresan etiketlenmesi: Optimizasyon ve karakterizasyon. NÖHÜ Müh. Bilim. Derg. 2024;13(4):1127-38.

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