Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights

Iqra Khalid; Abdullah Faheem; Akbar Ali

doi:10.56171/ojn.1778109

EN TR

Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights

Öz

A non-enzymatic choline biosensor was demonstrated with chitosan (CS) supported NiFe2O4 modified on a carbon paste electrode (CPE). NiFe2O4 is synthesized via the hydrothermal method to study the choline chloride (ChCl) behavior towards the distinctive performance of choline. The prepared sample with CPE. The synthesized NiFe2O4 was examined with different characterization techniques to confirm the formation of the specified material. X-ray diffraction (XRD), Fourier-Transmission Infrared spectroscopy (FTIR), and Raman Spectroscopy were used to optimize and evaluate the various properties of the prepared material. XRD confirmed the cubic inverse spinel crystal structure of NiFe2O4 with a crystallite size of 14nm, while FTIR spectra revealed the stretching and bending vibration over the IR frequency range, and modes confirmed through Raman spectra frequency range. The modified electrode of NiFe2O4/CS/CPE was used to perform electrochemical studies by voltammogram and evaluated through Cyclic voltammetry (CV). The CV curves taken at different working ranges (5-15μL) of potential 0.0- +1.0 V and the analyte signal of LoD (0.002μM), considering the S/N=3 across the current system, with the linear regression (R2) of 0.99. The prepared electrode showed a low (LoD) in the smaller range of the chloride choline and demonstrated a good response.

Anahtar Kelimeler

Nanomaterials, Ferrites, Chitosan, Biosensing, Electrochemical Sensors, Nanocomposites

Destekleyen Kurum

We are thankful to the Higher Education Commission of Pakistan for the grant of this project (NPRU-15417) titled ‘Ternary nano biocomposites for the fabrication of a novel electrode for the detection of chemical biomarkers,’ and to the Department of Physics, COMSATS University Islamabad, for its support in this research work.

Etik Beyan

No conflict of interest was declared by the authors.

Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights

Öz

A non-enzymatic choline biosensor was demonstrated with chitosan (CS) supported NiFe2O4 modified on a carbon paste electrode (CPE). NiFe2O4 is synthesized via the hydrothermal method to study the choline chloride (ChCl) behavior towards the distinctive performance of choline. The prepared sample with CPE. The synthesized NiFe2O4 was examined with different characterization techniques to confirm the formation of the specified material. X-ray diffraction (XRD), Fourier-Transmission Infrared spectroscopy (FTIR), and Raman Spectroscopy were used to optimize and evaluate the various properties of the prepared material. XRD confirmed the cubic inverse spinel crystal structure of NiFe2O4 with a crystallite size of 14nm, while FTIR spectra revealed the stretching and bending vibration over the IR frequency range, and modes confirmed through Raman spectra frequency range. The modified electrode of NiFe2O4/CS/CPE was used to perform electrochemical studies by voltammogram and evaluated through Cyclic voltammetry (CV). The CV curves taken at different working ranges (5-15μL) of potential 0.0- +1.0 V and the analyte signal of LoD (0.002μM), considering the S/N=3 across the current system, with the linear regression (R2) of 0.99. The prepared electrode showed a low (LoD) in the smaller range of the chloride choline and demonstrated a good response.

Anahtar Kelimeler

Nanomaterials, Nanocomposites, Ferrites, Chitosan, Biosensor, Electrochemical Sensor

Destekleyen Kurum

We are thankful to the Higher Education Commission of Pakistan for the grant of this project (NPRU-15417) titled ‘Ternary nano biocomposites for the fabrication of a novel electrode for the detection of chemical biomarkers,’ and to the Department of Physics, COMSATS University Islamabad, for its support in this research work.

Etik Beyan

No conflict of interest was declared by the authors.

Kaynakça

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Ayrıntılar

Birincil Dil

İngilizce

Konular

Malzeme Karekterizasyonu, Malzeme Mühendisliği (Diğer)

Bölüm

Araştırma Makalesi

Yazarlar

Iqra Khalid
0000-0002-5253-1837
Pakistan

Abdullah Faheem
0009-0009-6124-8943
Pakistan

Akbar Ali ^*
0000-0001-9934-680X
Pakistan

Erken Görünüm Tarihi

16 Aralık 2025

Yayımlanma Tarihi

29 Aralık 2025

Gönderilme Tarihi

14 Eylül 2025

Kabul Tarihi

21 Kasım 2025

Yayımlandığı Sayı

Yıl 2025 Cilt: 10 Sayı: 1/2

DOI

https://doi.org/10.56171/ojn.1778109

IZ

https://izlik.org/JA82AA76WA

APA

Khalid, I., Faheem, A., & Ali, A. (2025). Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights. Open Journal of Nano, 10(1/2), 14-26. https://doi.org/10.56171/ojn.1778109

AMA

1.Khalid I, Faheem A, Ali A. Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights. Open J. Nano. 2025;10(1/2):14-26. doi:10.56171/ojn.1778109

Chicago

Khalid, Iqra, Abdullah Faheem, ve Akbar Ali. 2025. “Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights”. Open Journal of Nano 10 (1/2): 14-26. https://doi.org/10.56171/ojn.1778109.

EndNote

Khalid I, Faheem A, Ali A (01 Aralık 2025) Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights. Open Journal of Nano 10 1/2 14–26.

IEEE

[1]I. Khalid, A. Faheem, ve A. Ali, “Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights”, Open J. Nano, c. 10, sy 1/2, ss. 14–26, Ara. 2025, doi: 10.56171/ojn.1778109.

ISNAD

Khalid, Iqra - Faheem, Abdullah - Ali, Akbar. “Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights”. Open Journal of Nano 10/1/2 (01 Aralık 2025): 14-26. https://doi.org/10.56171/ojn.1778109.

JAMA

1.Khalid I, Faheem A, Ali A. Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights. Open J. Nano. 2025;10:14–26.

MLA

Khalid, Iqra, vd. “Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights”. Open Journal of Nano, c. 10, sy 1/2, Aralık 2025, ss. 14-26, doi:10.56171/ojn.1778109.

Vancouver

1.Iqra Khalid, Abdullah Faheem, Akbar Ali. Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights. Open J. Nano. 01 Aralık 2025;10(1/2):14-26. doi:10.56171/ojn.1778109

Open Journal of Nano(OJN), dergisi molekülerden mikro boyuttaki yapılara kadar değişen fiziksel, kimyasal ve biyolojik olaylar ve süreçlerle ilgili (ancak bunlarla sınırlı olmayan) bilgilerle ilgilenir.
The Open Journal of Nano dergisinde yayınlanan tüm yayınlar Atıf-GayriTicari 4.0 Uluslararası (CC BY-NC 4.0) lisansı altında lisanlanmıştır.

Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights

Öz

Anahtar Kelimeler

Destekleyen Kurum

Etik Beyan

Ferrite-Based Hierarchical Nanostructures for Electrochemical Sensing: Synthesis, Interface Engineering, and Performance Insights

Öz

Anahtar Kelimeler

Destekleyen Kurum

Etik Beyan

Kaynakça

Ayrıntılar

Birincil Dil

Konular

Bölüm

Yazarlar

Erken Görünüm Tarihi

Yayımlanma Tarihi

Gönderilme Tarihi

Kabul Tarihi

Yayımlandığı Sayı

DOI

IZ

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