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Endüstriyel Borlama Uygulamaları için AISI D2 Soğuk İş Takım Çeliğinin Optimum Yüzey Pürüzlülüğünün Belirlenmesi

Yıl 2025, Cilt: 8 Sayı: 5, 2094 - 2110, 15.12.2025
https://doi.org/10.47495/okufbed.1639938

Öz

Borlama işlemi sırasında, malzemenin yüzeyinde çok ince ve son derece sert bir seramik tabaka oluşur. Bu işlem, aşınma ve korozyona karşı yüksek direnç gerektiren bileşenlerde yaygın olarak uygulanmaktadır. Borlanmış parçalar üstün özellikler kazansa da işlem sırasında kullanılan yüksek sıcaklıklar, parçanın son boyutlarını ve yüzey pürüzlülüğünü değiştirebildiğinden önemli bir zorluk oluşturmaktadır. Bu durum, yüksek boyutsal hassasiyet ve yüzey kalitesi gerektiren ancak işlevleri nedeniyle hızla aşınan zımbalar gibi hassas kesici takımlar için özellikle kritiktir. Bu çalışmada, hassas kalıp parçalarında yaygın olarak kullanılan AISI D2 (1.2379, X153CrMoV12) soğuk iş takım çeliğinin borlama sonrası yüzey pürüzlülüğündeki değişim incelenmiştir. Farklı başlangıç yüzey pürüzlülüğüne sahip numuneler, 900 °C ve 950 °C sıcaklıklarda, 6 ve 8 saat süreyle Ekabor® II katı ortamında borlanmıştır. İşlem öncesi nihai boyutlandırma ve yüzey durumları, tel erozyon ve hassas tornalama işlemleriyle hazırlanmıştır. Sonuçlar, başlangıç Ra değeri < 1 µm olan numunelerde yüzey pürüzlülüğünde %143’e kadar artış olduğunu, Ra > 2 µm olan bazı numunelerde ise %26’ya varan azalma sergilediğini göstermiştir. Artan sıcaklık ve süre, bu etkileri daha da yoğunlaştırmıştır. Bulgular, başlangıç yüzey pürüzlülüğünün borlama sonrası yüzey morfolojisi üzerinde kritik bir rol oynadığını ve hassas uygulamalarda dikkatle kontrol edilmesi gerektiğini vurgulamaktadır.

Teşekkür

Bu çalışma 19-21 Ağustos 2024 tarihleri arasında 18. Uluslararası İstanbul Yaşam, Mühendislik, Mimarlık ve Matematik Bilimleri Bilimsel Araştırma Kongresi'nde sözlü bildiri olarak sunulmuştur.

Kaynakça

  • Armagan E., Kaplan Y., Onar V., Ulukoy A. Wear behavior of boronized AISI D2 tool steel. 16th International Materials Symposium, 12-14 October 2016, pp: 353-358, Denizli, Türkiye.
  • American Society for Testing and Materials (ASTM). ASTM A681 Standard specification for tool steels alloy, 2018.
  • Bahrami A., Anijdan S., Golozar M., Shamanian M. Effects of conventional heat treatment on wear resistance of AISI H13 tool steel. Wear 2005; 258(5-6): 846–851.
  • Basir MHM., Abdullah B., Alias SK., Jumadin MH., Ismail MH. Analysis on microstructure, hardness and surface roughness of shot blasted-paste boronized 316 austenitic stainless steel. Jurnal Teknologi 2015; 76(3): 75–79.
  • Bastidas DM. Corrosion and protection of metals. Metals 2020; 10(4): 458.
  • Belaid M., Fares ML., Assalla O., Boukari F. Surface characterization of a modified cold work tool steel treated by powder-pack boronizing. Materialwissenschaft Und Werkstofftechnik 2022; 53(1): 15–38.
  • BorTec. Improve wear protection by boronizing. https://bortec-group.com/services/boronizing/. Accession date: 15.02.2025.
  • Çalık A. Effect of powder particle size on the mechanical properties of boronized EN H320 LA steel sheets. ISIJ International 2013; 53(1): 160–164.
  • Çakir MV. A comparative study on tribocorrosion wear behavior of boride and vanadium carbide coatings produced by TRD on AISI D2 steel. Protection of Metals and Physical Chemistry of Surfaces 2022; 58(3): 562-573.
  • Çetin M., Günen A., Kalkandelen M., Karakaş MS. Microstructural, wear and corrosion characteristics of boronized AISI 904L superaustenitic stainless steel. Vacuum 2021; 187: 110145.
  • de Mendonça Ferreira ST., Bacco ALK., do Nascimento EM., Lepienski CM. Mechanical characterization and micro-wear of FeB-Fe2B layers on boriding AISI D2 and AISI 4340 steels. Materials Sciences and Applications 2021; 12(7): 330-344.
  • Gürcan Y., Işıtan A., Kutlubay RÇ. Determination of microstructure and microhardness properties of boronized Vanadis 4 steel. 4th International Conference on Engineering Technology and Applied Sciences (ICETAS), 24-28 April 2019, pp:277-281, Kiev, Ukraine.
  • Holmberg K., Erdemir A. Influence of tribology on global energy consumption, costs and emissions. Friction 2017; 5: 263-284.
  • Hunan Fushun Metal Co. DIN 1.2379 cold work mould steel bars with ANSI D2 steel grade. https://www.fushunspecialsteel.com/1-2379-cold-work-mould-steel-bars-with-ansi-d2-steel-grade/. Accession date: 15.02.2025.
  • Işıtan A. Boronizing: In the industrial applications in Turkey, why not find the place it deserves?. International Symposium on Boron, 17-19 April 2019, pp:287-292, Nevşehir, Türkiye.
  • Işıtan A. Sondaj makinasında kullanılan ve üzerinde keçe çalışan araparçanın aşınma performansının ve kullanım ömrünün arttırılması. Mühendis ve Makine 2018; 59(693): 47–53.
  • Jain V., Sundararajan G. Influence of the pack thickness of the boronizing mixture on the boronizing of steel. Surface and Coatings Technology 2002; 149(1): 21–26.
  • Kantoríková E., Moravec J., Biňasová V. The effect of borides on the mechanical properties of tool steels and sintered carbides. Transportation Research Procedia 2023; 74: 522-529.
  • Krelling AP., Milan JCG., De Costa CE. Tribological behaviour of borided H13 steel with different boronizing agents. Surface Engineering 2015; 31(8): 581-587.
  • Kutlubay RÇ., Işıtan A., Gürcan Y. Borlama işleminin Vanadis 4 çeliğinin aşınma direnci üzerine etkisi. 4th International Conference on Engineering Technology and Applied Sciences (ICETAS), 24-28 April 2019, pp:282-285, Kiev, Ukraine.
  • Lampman S. Introduction to surface hardening of steels. In: Davis, JR. (ed.) ASM Handbook Volume 4 Heat Treating. ASM International 1991; 259–267.
  • Matuschka AG Von. Boronizing. Oxford England: The Alden Pres; 1980.
  • Nair F., Zafar HMN., Cerit AA., Karamış MB. Analyzing the influence of simultaneously austenitization and multi-directional boriding on the surface and subsurface of H13 tool steel. Journal of Materials Engineering and Performance 2022; 31(12): 9791-9801.
  • Özbek I. The improvement of surface performance of (AISI M50, AISI M2) high speed steels and AISI W1 steel by boronizing treatment. Sakarya University Graduate School of Natural and Applied Sciences PhD Thesis, Sakarya, Türkiye, 2001.
  • Peng C. The effect of boronizing on hardness, wear and corrosion properties of AISI 1018 and AISI 316L steels. University of Saskatchewan College of Graduate and Postdoctoral Studies PhD Thesis, Metis, Canada, 2020.
  • Pereira R., Mariani F., Lombardi AN., Totten GE., Casteletti L. Characterization of layers produced by boronizing and boronizing-PVD on AISI D2 tool steel. Materials Performance and Characterization 2016; 5(4): 406–413.
  • Precision Punch and Tooling. Technical reference. https://ppunch.com/technical-reference/. Accession date: 15.02.2025.
  • Qamar SZ. Effect of heat treatment on mechanical properties of H11 tool steel. Journal of Achievements in Materials and Manufacturing Engineering 2009; 35(2): 115-120.
  • Reséndiz-Calderón CD., Cao-Romero-Gallegos JA., Farfan-Cabrera LI., Campos-Silva I., Soriano-Vargas O. Influence of boronizing on the tribological behavior of AISI D2 tool steel for dry deep drawing of stainless steel and aluminum. Surface and Coatings Technology 2024; 484: 130832.
  • Sinha AK. Boronizing. In: Davis, JR. (ed.) ASM Handbook Volume 4 Heat Treating. ASM International 1991; 437.
  • Sista V., Kahvecioglu O., Eryilmaz OL., Erdemir A., Timur S. Electrochemical boronizing and characterization of AISI D2 tool steel. Thin Solid Films 2011; 520(5): 1582–1588.
  • Şahin S. Effects of boronizing process on the surface roughness and dimensions of AISI 1020, AISI 1040 and AISI 2714. Journal of Materials Processing Technology 2009; 209(4): 1736–1741.
  • Thyssenkrupp Steel. 2379 tool steel. https://thyssenkruppsteel.wordpress.com/tag/aisi-d2/. Accession date: 15.02.2025
  • Türkmen İ., Yalamaç E. Effect of alternative boronizing mixtures on boride layer and tribological behaviour of boronized SAE 1020 steel. Metals and Materials International 2022; 28(5): 1114–1128.
  • Ulukoy A., Can AC., Ozmen Y., Tasgetiren S. Borocarburizing of decarburized gears made from 21NiCrMo2 (AISI 8620) steel. Proceedings of the Institution of Mechanical Engineers Part L: Journal of Materials: Design and Applications 2013; 229(3): 226–235.
  • Uluköy A., Can AÇ. Çeliklerin borlanması. Pamukkale University Journal of Engineering Sciences 2006; 12(2): 189–198.
  • VillaVelázquez-Mendoza CI., Rodriguez-Mendoza JL., Ibarra-Galván V., Hodgkins RP., López-Valdivieso A., Serrato-Palacios LL., Leal-Cruz AL., Ibarra-Junquera V. Effect of substrate roughness, time and temperature on the processing of iron boride coatings: Experimental and statistical approaches. International Journal of Surface Science and Engineering 2014; 8(1): 71–91.
  • Woydt M. The importance of tribology for reducing CO2 emissions and for sustainability. Wear 2021; 474: 203768.
  • Yu L., Chen X., Khor K., Sundararajan G. FeB/Fe2B phase transformation during SPS pack-boronizing: Boride layer growth kinetics. Acta Materialia 2005; 53(8): 2361–2368.

Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications

Yıl 2025, Cilt: 8 Sayı: 5, 2094 - 2110, 15.12.2025
https://doi.org/10.47495/okufbed.1639938

Öz

During the boronizing process, a very thin and extremely hard ceramic layer forms on the surface of the material. This procedure is commonly applied to components requiring high resistance to wear and corrosion. Although boronized parts acquire superior properties, a key challenge is the elevated temperatures used during the process, which can alter the final dimensions and surface roughness of the part. This issue is particularly critical for precision cutting tools such as punches, which require high dimensional accuracy and surface quality but often suffer from rapid wear due to their function. In this study, the surface roughness evolution of AISI D2 (1.2379, X153CrMoV12) cold work tool steel—widely used in precision mold parts—was investigated after boronizing. Specimens with different initial surface roughness values were boronized in a solid Ekabor® II medium at 900 °C and 950 °C for 6 and 8 hours. Final dimensions and surface conditions were prepared via wire erosion and fine turning before treatment. The results showed that samples with Ra < 1 µm experienced up to 143% increase in surface roughness, while some Ra > 2 µm samples exhibited reductions of up to 26%. Increased temperature and duration intensified these effects. The findings emphasize that the initial surface roughness plays a critical role in the post-boronizing surface morphology and must be carefully controlled in precision applications.

Teşekkür

This study was presented as an oral presentation at the 18th International Istanbul Scientific Research Congress on Life, Engineering, Architecture and Mathematical Sciences between August 19-21, 2024.

Kaynakça

  • Armagan E., Kaplan Y., Onar V., Ulukoy A. Wear behavior of boronized AISI D2 tool steel. 16th International Materials Symposium, 12-14 October 2016, pp: 353-358, Denizli, Türkiye.
  • American Society for Testing and Materials (ASTM). ASTM A681 Standard specification for tool steels alloy, 2018.
  • Bahrami A., Anijdan S., Golozar M., Shamanian M. Effects of conventional heat treatment on wear resistance of AISI H13 tool steel. Wear 2005; 258(5-6): 846–851.
  • Basir MHM., Abdullah B., Alias SK., Jumadin MH., Ismail MH. Analysis on microstructure, hardness and surface roughness of shot blasted-paste boronized 316 austenitic stainless steel. Jurnal Teknologi 2015; 76(3): 75–79.
  • Bastidas DM. Corrosion and protection of metals. Metals 2020; 10(4): 458.
  • Belaid M., Fares ML., Assalla O., Boukari F. Surface characterization of a modified cold work tool steel treated by powder-pack boronizing. Materialwissenschaft Und Werkstofftechnik 2022; 53(1): 15–38.
  • BorTec. Improve wear protection by boronizing. https://bortec-group.com/services/boronizing/. Accession date: 15.02.2025.
  • Çalık A. Effect of powder particle size on the mechanical properties of boronized EN H320 LA steel sheets. ISIJ International 2013; 53(1): 160–164.
  • Çakir MV. A comparative study on tribocorrosion wear behavior of boride and vanadium carbide coatings produced by TRD on AISI D2 steel. Protection of Metals and Physical Chemistry of Surfaces 2022; 58(3): 562-573.
  • Çetin M., Günen A., Kalkandelen M., Karakaş MS. Microstructural, wear and corrosion characteristics of boronized AISI 904L superaustenitic stainless steel. Vacuum 2021; 187: 110145.
  • de Mendonça Ferreira ST., Bacco ALK., do Nascimento EM., Lepienski CM. Mechanical characterization and micro-wear of FeB-Fe2B layers on boriding AISI D2 and AISI 4340 steels. Materials Sciences and Applications 2021; 12(7): 330-344.
  • Gürcan Y., Işıtan A., Kutlubay RÇ. Determination of microstructure and microhardness properties of boronized Vanadis 4 steel. 4th International Conference on Engineering Technology and Applied Sciences (ICETAS), 24-28 April 2019, pp:277-281, Kiev, Ukraine.
  • Holmberg K., Erdemir A. Influence of tribology on global energy consumption, costs and emissions. Friction 2017; 5: 263-284.
  • Hunan Fushun Metal Co. DIN 1.2379 cold work mould steel bars with ANSI D2 steel grade. https://www.fushunspecialsteel.com/1-2379-cold-work-mould-steel-bars-with-ansi-d2-steel-grade/. Accession date: 15.02.2025.
  • Işıtan A. Boronizing: In the industrial applications in Turkey, why not find the place it deserves?. International Symposium on Boron, 17-19 April 2019, pp:287-292, Nevşehir, Türkiye.
  • Işıtan A. Sondaj makinasında kullanılan ve üzerinde keçe çalışan araparçanın aşınma performansının ve kullanım ömrünün arttırılması. Mühendis ve Makine 2018; 59(693): 47–53.
  • Jain V., Sundararajan G. Influence of the pack thickness of the boronizing mixture on the boronizing of steel. Surface and Coatings Technology 2002; 149(1): 21–26.
  • Kantoríková E., Moravec J., Biňasová V. The effect of borides on the mechanical properties of tool steels and sintered carbides. Transportation Research Procedia 2023; 74: 522-529.
  • Krelling AP., Milan JCG., De Costa CE. Tribological behaviour of borided H13 steel with different boronizing agents. Surface Engineering 2015; 31(8): 581-587.
  • Kutlubay RÇ., Işıtan A., Gürcan Y. Borlama işleminin Vanadis 4 çeliğinin aşınma direnci üzerine etkisi. 4th International Conference on Engineering Technology and Applied Sciences (ICETAS), 24-28 April 2019, pp:282-285, Kiev, Ukraine.
  • Lampman S. Introduction to surface hardening of steels. In: Davis, JR. (ed.) ASM Handbook Volume 4 Heat Treating. ASM International 1991; 259–267.
  • Matuschka AG Von. Boronizing. Oxford England: The Alden Pres; 1980.
  • Nair F., Zafar HMN., Cerit AA., Karamış MB. Analyzing the influence of simultaneously austenitization and multi-directional boriding on the surface and subsurface of H13 tool steel. Journal of Materials Engineering and Performance 2022; 31(12): 9791-9801.
  • Özbek I. The improvement of surface performance of (AISI M50, AISI M2) high speed steels and AISI W1 steel by boronizing treatment. Sakarya University Graduate School of Natural and Applied Sciences PhD Thesis, Sakarya, Türkiye, 2001.
  • Peng C. The effect of boronizing on hardness, wear and corrosion properties of AISI 1018 and AISI 316L steels. University of Saskatchewan College of Graduate and Postdoctoral Studies PhD Thesis, Metis, Canada, 2020.
  • Pereira R., Mariani F., Lombardi AN., Totten GE., Casteletti L. Characterization of layers produced by boronizing and boronizing-PVD on AISI D2 tool steel. Materials Performance and Characterization 2016; 5(4): 406–413.
  • Precision Punch and Tooling. Technical reference. https://ppunch.com/technical-reference/. Accession date: 15.02.2025.
  • Qamar SZ. Effect of heat treatment on mechanical properties of H11 tool steel. Journal of Achievements in Materials and Manufacturing Engineering 2009; 35(2): 115-120.
  • Reséndiz-Calderón CD., Cao-Romero-Gallegos JA., Farfan-Cabrera LI., Campos-Silva I., Soriano-Vargas O. Influence of boronizing on the tribological behavior of AISI D2 tool steel for dry deep drawing of stainless steel and aluminum. Surface and Coatings Technology 2024; 484: 130832.
  • Sinha AK. Boronizing. In: Davis, JR. (ed.) ASM Handbook Volume 4 Heat Treating. ASM International 1991; 437.
  • Sista V., Kahvecioglu O., Eryilmaz OL., Erdemir A., Timur S. Electrochemical boronizing and characterization of AISI D2 tool steel. Thin Solid Films 2011; 520(5): 1582–1588.
  • Şahin S. Effects of boronizing process on the surface roughness and dimensions of AISI 1020, AISI 1040 and AISI 2714. Journal of Materials Processing Technology 2009; 209(4): 1736–1741.
  • Thyssenkrupp Steel. 2379 tool steel. https://thyssenkruppsteel.wordpress.com/tag/aisi-d2/. Accession date: 15.02.2025
  • Türkmen İ., Yalamaç E. Effect of alternative boronizing mixtures on boride layer and tribological behaviour of boronized SAE 1020 steel. Metals and Materials International 2022; 28(5): 1114–1128.
  • Ulukoy A., Can AC., Ozmen Y., Tasgetiren S. Borocarburizing of decarburized gears made from 21NiCrMo2 (AISI 8620) steel. Proceedings of the Institution of Mechanical Engineers Part L: Journal of Materials: Design and Applications 2013; 229(3): 226–235.
  • Uluköy A., Can AÇ. Çeliklerin borlanması. Pamukkale University Journal of Engineering Sciences 2006; 12(2): 189–198.
  • VillaVelázquez-Mendoza CI., Rodriguez-Mendoza JL., Ibarra-Galván V., Hodgkins RP., López-Valdivieso A., Serrato-Palacios LL., Leal-Cruz AL., Ibarra-Junquera V. Effect of substrate roughness, time and temperature on the processing of iron boride coatings: Experimental and statistical approaches. International Journal of Surface Science and Engineering 2014; 8(1): 71–91.
  • Woydt M. The importance of tribology for reducing CO2 emissions and for sustainability. Wear 2021; 474: 203768.
  • Yu L., Chen X., Khor K., Sundararajan G. FeB/Fe2B phase transformation during SPS pack-boronizing: Boride layer growth kinetics. Acta Materialia 2005; 53(8): 2361–2368.
Toplam 39 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular İmalat Süreçleri ve Teknolojileri
Bölüm Araştırma Makalesi
Yazarlar

Yasin Gürcan

Arzum Işıtan 0000-0002-5228-9788

Gönderilme Tarihi 15 Şubat 2025
Kabul Tarihi 12 Mayıs 2025
Yayımlanma Tarihi 15 Aralık 2025
Yayımlandığı Sayı Yıl 2025 Cilt: 8 Sayı: 5

Kaynak Göster

APA Gürcan, Y., & Işıtan, A. (2025). Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 8(5), 2094-2110. https://doi.org/10.47495/okufbed.1639938
AMA Gürcan Y, Işıtan A. Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi. Aralık 2025;8(5):2094-2110. doi:10.47495/okufbed.1639938
Chicago Gürcan, Yasin, ve Arzum Işıtan. “Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications”. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi 8, sy. 5 (Aralık 2025): 2094-2110. https://doi.org/10.47495/okufbed.1639938.
EndNote Gürcan Y, Işıtan A (01 Aralık 2025) Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi 8 5 2094–2110.
IEEE Y. Gürcan ve A. Işıtan, “Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications”, Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi, c. 8, sy. 5, ss. 2094–2110, 2025, doi: 10.47495/okufbed.1639938.
ISNAD Gürcan, Yasin - Işıtan, Arzum. “Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications”. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi 8/5 (Aralık2025), 2094-2110. https://doi.org/10.47495/okufbed.1639938.
JAMA Gürcan Y, Işıtan A. Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2025;8:2094–2110.
MLA Gürcan, Yasin ve Arzum Işıtan. “Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications”. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi, c. 8, sy. 5, 2025, ss. 2094-10, doi:10.47495/okufbed.1639938.
Vancouver Gürcan Y, Işıtan A. Determination of The Optimum Surface Roughness of AISI D2 Cold Work Tool Steel for Industrial Boronizing Applications. Osmaniye Korkut Ata Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2025;8(5):2094-110.

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