316L/HA Kompozitlerinin Farklı Fizyolojik Sıvılardaki Korozyon ve Biyoaktivite Davranışının Araştırılması

Yıl 2024, Cilt: 27 Sayı: 5, 1913 - 1921, 02.10.2024

Özlem Canpolat , Aykut Çanakçı

https://doi.org/10.2339/politeknik.1312685

Öz

Bu çalışmada, biyomedikal uygulamalar için toz metalurjisi yöntemi ile SS316L/HA kompozitleri üretilmiş; yoğunluğu, mikroyapısı, sertliği, korozyon direnci ve biyoaktivite özellikleri incelenmiştir. 316L matrisine ağırlıkça %3, %5 ve %7 oranında hidroksiapatit (HA) takviye edilmiştir. HA oranının artışı ile birlikte yoğunluk ve sertlik azalmış, porozite ise artmıştır. XRD analizlerinde 316L ve HA piklerinin yanı sıra CaCr2O4 fazının pikleri de görülmüştür. Korozyon deneyleri Ringer ve Hank's fizyolojik sıvılarında gerçekleştirilerek kompozitler içinde %5 takviyeli olan numunenin korozyon hızı en düşük çıkmıştır. Biyoaktivite testleri simüle edilmiş vücut sıvısında (SBF) 7 ve 14 gün bekletilerek gerçekleştirilmiş ve her iki sürenin sonunda numune yüzeylerinde küresel kristalitlerden oluşan apatit tabakası gözlenmiştir

Anahtar Kelimeler

316L, Hidroksiapatit, Toz metalurjisi, Biyomalzeme

Destekleyen Kurum

Karadeniz Teknik Üniversitesi Bilimsel Araştırma Projeleri Birimi

Proje Numarası

FDK-2019-8440

Investigation of Corrosion and Bioactivity Behavior of 316L/HA Composites in Different Physiological Fluids

Öz

In this study, SS316L/HA composites were produced by powder metallurgy method for biomedical applications; density, microstructure, hardness, corrosion resistance and bioactivity properties were investigated. 3%, 5% and 7% by weight of hydroxyapatite (HA) were added to the 316L matrix. With the increase of HA ratio, density and hardness decreased, while porosity increased. In XRD analysis, in addition to 316L and HA peaks, CaCr2O4 phase peaks were also observed. Corrosion tests were carried out in Ringer and Hank's physiological fluids, and the corrosion rate of the sample with 5% reinforcement was the lowest among composites. Bioactivity tests were carried out in simulated body fluid (SBF) for 7 and 14 days, and at the end of both periods, apatite layer consisting of spherical crystallites was observed on the sample surfaces.

Anahtar Kelimeler

316L, Hydroxyapatite, Powder metallurgy, Biomaterial

Proje Numarası

FDK-2019-8440

Kaynakça

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