The role of tempering conditions and Cr content on the microstructure and mechanical performance of 0.16C-5.5Mn steel
Yıl 2026,
Cilt: 15 Sayı: 1
,
1
-
16
,
30.03.2026
Fatih Demir
,
Mehmet Eroğlu
Öz
In this paper, the role of tempering conditions and Cr content on the microstructure and mechanical performance of 0.16C-5.5Mn medium manganese steel is discussed. For this purpose, various analyses were applied to 0.16C-5.5Mn steels with 0% Cr and 1.2% Cr content for microstructural characterization. The results obtained showed that the tempering process produced a microstructure consisting of ferrite and fine acicular carbides dispersed in the tempered martensite matrix in 0.16C-5.5Mn steel. It was also observed that the retained austenite phase persisted in the microstructure after tempering. In addition, the Cr content in 0.16C-5.5Mn steel improved the stability of the retained austenite phase after tempering. When all these results were correlated with the data obtained from mechanical tests, it was observed that tempering treatment at low temperatures and Cr content in the steel composition significantly improved the combination of tensile strength and total elongation (TS×TE) of 0.16C-5.5Mn medium manganese steel.
Kaynakça
-
Kwiatkowski da Silva A, Inden G, Kumar A, Ponge D, Gault B, Raabe D. Competition between formation of carbides and reversed austenite during tempering of a medium-manganese steel studied by thermodynamic-kinetic simulations and atom probe tomography. Acta Mater. 2018;147:165-175. doi:10.1016/j.actamat.2018.01.022
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Arlazarov A, Hazotte A, Bouaziz O, Gouné M, Kegel F. Characterization of microstructure formation and mechanical behaviour of an advanced Medium-Mn steel, in Conf. Proc. Materials Science & Technology (). Pittsburgh: MS&T; 2012. p. 1124–1131.
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Arlazarov A, Gouné M, Bouaziz O, Hazotte A, Petitgand G, Barges P. Evolution of microstructure and mechanical properties of medium Mn steels during double annealing. Mater Sci Eng A. 2012;542:31-39. doi:10.1016/j.msea.2012.02.024
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Lee YK, Han J. Current opinion in medium manganese steel. Mater Sci Technol (United Kingdom). 2015;31(7):843-856. doi:10.1179/1743284714Y.0000000722
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Rana R. Special issue on ‘Medium manganese steels.’ Mater Sci Technol (United Kingdom). 2019;35(17):2039-2044. doi:10.1080/02670836.2019.1673971
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Tsukataimi I, Hashimoto S, Inoue T. Effects of Silicon and Manganese Addition on Mechanical Properties of High-strength Hot-rolled Sheet Steel Containing Retained Austenite. ISIJ Int. 1991;31(9):992-1000. doi:10.2355/isijinternational.31.992
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Hashimoto S, Ikeda S, Sugimoto KI, Miyake S. Effects of Nb and Mo addition to 0.2%C-1.5%Si-1.5%Mn steel on mechanical properties of hot rolled TRIP-aided steel sheets. ISIJ Int. 2004;44(9):1590-1598. doi:10.2355/isijinternational.44.1590
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Cao WQ, Wang C, Shi J, Wang MQ, Hui WJ, Dong H. Microstructure and mechanical properties of Fe-0.2C-5Mn steel processed by ART-annealing. Mater Sci Eng A. 2011;528(22-23):6661-6666. doi:10.1016/j.msea.2011.05.039
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Cai M, Li Z, Chao Q, Hodgson PD. A Novel Mo and Nb Microalloyed Medium Mn TRIP Steel with Maximal Ultimate Strength and Moderate Ductility. Metall Mater Trans A Phys Metall Mater Sci. 2014;45(12):5624-5634. doi:10.1007/s11661-014-2504-x
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Siciliano F, Poliak EI. Modeling of the Resistance to Hot Deformation and the Effects of Microalloying in High-Al Steels under Industrial Conditions. Mater Sci Forum. 2005;500-501:195-202. doi:10.4028/www.scientific.net/msf.500-501.195
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Gibbs PJ, De Moor E, Merwin MJ, Clausen B, Speer JG, Matlock DK. Austenite stability effects on tensile behavior of manganese-enriched- austenite
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Yang F, Luo H, Hu C, Pu E, Dong H. Effects of intercritical annealing process on microstructures and tensile properties of cold-rolled 7Mn steel. Mater Sci Eng A. 2017;685(November 2016):115-122. doi:10.1016/j.msea.2016.12.119
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Bai Y, Matsui Y, Shibata A, Tsuji N. Effect of thermomechanical processing at α + γ two-phase temperatures on microstructure and mechanical property of 5Mn-0.1C-2Si medium-manganese steel. Mater Sci Eng A. 2019;743(August 2018):57-66. doi:10.1016/j.msea.2018.11.061
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Xu HF, Zhao J, Cao WQ, et al. Heat treatment effects on the microstructure and mechanical properties of a medium manganese steel (0.2C-5Mn). Mater Sci Eng A. 2012;532:435-442. doi:10.1016/j.msea.2011.11.009
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Xu YB, Zou Y, Hu ZP, Han DT, Chen SQ, Misra RDK. Correlation between deformation behavior and austenite characteristics in a Mn-Al type TRIP steel. Mater Sci Eng A. 2017;698(11):126-135. doi:10.1016/j.msea.2017.05.058
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Grajcar A, Kuziak R, Zalecki W. Third generation of AHSS with increased fraction of retained austenite for the automotive industry. Arch Civ Mech Eng. 2012;12(3):334-341. doi:10.1016/j.acme.2012.06.011
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Zhao X, Zhang Y, Shao C, Hui W, Dong H. Thermal stability of retained austenite and mechanical properties of medium-Mn steel during tempering treatment. J. Iron Steel Res. Int. 2017;24:830–837. doi:10.1016/s1006-706x(17)30123-1
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Yan S, Liu X, Liu WJ, Lan H, Wu H. Comparison on mechanical properties and microstructure of a C-Mn-Si steel treated by quenching and partitioning (Q&P) and quenching and tempering (Q&T) processes. Mater Sci Eng A. 2015;620:58-66. doi:10.1016/j.msea.2014.09.047
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Temperleme koşullarının ve Cr içeriğinin 0.16C-5.5Mn çeliğinin mikroyapısı ve mekanik performansındaki rolü
Yıl 2026,
Cilt: 15 Sayı: 1
,
1
-
16
,
30.03.2026
Fatih Demir
,
Mehmet Eroğlu
Öz
Bu makalede, temperleme koşullarının ve Cr içeriğinin 0.16C-5.5Mn orta manganlı çeliğinin mikroyapısı ve mekanik performansındaki rolü ele alınmıştır. Bu amaçla imal edilen %0 Cr ve %1.2 Cr içerikli 0.16C-5.5Mn çeliklerine mikroyapı karakterizasyonu amacıyla çeşitli analizler uygulanmıştır. Elde edilen sonuçlar temperleme işleminin 0.16C-5.5Mn çeliğinde temperlenmiş martenzit matrisinde dağılmış ferrit ve ince iğnemsi karbürlerden oluşan bir mikroyapı meydana getirdiğini göstermiştir. Ayrıca, kalıntı östenit fazının temperleme sonrasında da mikroyapıda varlığını sürdürdüğü görülmüştür. Ek olarak, 0.16C-5.5Mn çeliğindeki Cr içeriği kalıntı östenit fazının temperleme sonrasındaki kararlılığını geliştirmiştir. Tüm bu sonuçlar mekanik testlerden elde edilen veriler ile ilişkilendirildiğinde, düşük sıcaklıklardaki temperleme işleminin ve çelik bileşimindeki Cr içeriğinin 0.16C-5.5Mn orta manganlı çeliğinin çekme mukavemeti ile toplam uzama (TS×TE) kombinasyonunu belirgin bir şekilde geliştirdiği gözlemlenmiştir.
Kaynakça
-
Kwiatkowski da Silva A, Inden G, Kumar A, Ponge D, Gault B, Raabe D. Competition between formation of carbides and reversed austenite during tempering of a medium-manganese steel studied by thermodynamic-kinetic simulations and atom probe tomography. Acta Mater. 2018;147:165-175. doi:10.1016/j.actamat.2018.01.022
-
Arlazarov A, Hazotte A, Bouaziz O, Gouné M, Kegel F. Characterization of microstructure formation and mechanical behaviour of an advanced Medium-Mn steel, in Conf. Proc. Materials Science & Technology (). Pittsburgh: MS&T; 2012. p. 1124–1131.
-
Arlazarov A, Gouné M, Bouaziz O, Hazotte A, Petitgand G, Barges P. Evolution of microstructure and mechanical properties of medium Mn steels during double annealing. Mater Sci Eng A. 2012;542:31-39. doi:10.1016/j.msea.2012.02.024
-
Lee YK, Han J. Current opinion in medium manganese steel. Mater Sci Technol (United Kingdom). 2015;31(7):843-856. doi:10.1179/1743284714Y.0000000722
-
Rana R. Special issue on ‘Medium manganese steels.’ Mater Sci Technol (United Kingdom). 2019;35(17):2039-2044. doi:10.1080/02670836.2019.1673971
-
Tsukataimi I, Hashimoto S, Inoue T. Effects of Silicon and Manganese Addition on Mechanical Properties of High-strength Hot-rolled Sheet Steel Containing Retained Austenite. ISIJ Int. 1991;31(9):992-1000. doi:10.2355/isijinternational.31.992
-
Hashimoto S, Ikeda S, Sugimoto KI, Miyake S. Effects of Nb and Mo addition to 0.2%C-1.5%Si-1.5%Mn steel on mechanical properties of hot rolled TRIP-aided steel sheets. ISIJ Int. 2004;44(9):1590-1598. doi:10.2355/isijinternational.44.1590
-
Cao WQ, Wang C, Shi J, Wang MQ, Hui WJ, Dong H. Microstructure and mechanical properties of Fe-0.2C-5Mn steel processed by ART-annealing. Mater Sci Eng A. 2011;528(22-23):6661-6666. doi:10.1016/j.msea.2011.05.039
-
Cai M, Li Z, Chao Q, Hodgson PD. A Novel Mo and Nb Microalloyed Medium Mn TRIP Steel with Maximal Ultimate Strength and Moderate Ductility. Metall Mater Trans A Phys Metall Mater Sci. 2014;45(12):5624-5634. doi:10.1007/s11661-014-2504-x
-
Cai MH, Zhu WJ, Stanford N, Pan LB, Chao Q, Hodgson PD. Dependence of deformation behavior on grain size and strain rate in an ultrahigh strength-ductile Mn-based TRIP alloy. Mater Sci Eng A. 2016;653:35-42. doi:10.1016/j.msea.2015.11.103
-
Siciliano F, Poliak EI. Modeling of the Resistance to Hot Deformation and the Effects of Microalloying in High-Al Steels under Industrial Conditions. Mater Sci Forum. 2005;500-501:195-202. doi:10.4028/www.scientific.net/msf.500-501.195
-
Gibbs PJ, De Moor E, Merwin MJ, Clausen B, Speer JG, Matlock DK. Austenite stability effects on tensile behavior of manganese-enriched- austenite
transformation-induced plasticity steel. Metall Mater Trans A Phys Metall Mater Sci. 2011;42(12):3691-3702. doi:10.1007/s11661-011-0687-y
-
Dong H. High performance steels: Initiative and practice. Sci China Technol Sci. 2012;55(7):1774-1790. doi:10.1007/s11431-012-4911-9
-
Zhao C, Cao WQ, Zhang C, Yang ZG, Dong H, Weng YQ. Effect of annealing temperature and time on microstructure evolution of 0*2C-5Mn steel during intercritical annealing process. Mater Sci Technol (United Kingdom). 2014;30(7):791-799. doi:10.1179/1743284713Y.0000000416
-
Kong L, Liu Y, Liu J, et al. The influence of chromium on the pearlite-austenite transformation kinetics of the Fe-Cr-C ternary steels. J Alloys Compd. 2015;648:494-499. doi:10.1016/j.jallcom.2015.06.259
-
Zhang H, Pradeep KG, Mandal S, Ponge D, Raabe D. New insights into the austenitization process of low-alloyed hypereutectoid steels: Nucleation analysis of strain-induced austenite formation. Acta Mater. 2014;80:296-308. doi:10.1016/j.actamat.2014.07.073
-
Yang F, Luo H, Hu C, Pu E, Dong H. Effects of intercritical annealing process on microstructures and tensile properties of cold-rolled 7Mn steel. Mater Sci Eng A. 2017;685(November 2016):115-122. doi:10.1016/j.msea.2016.12.119
-
Bai Y, Matsui Y, Shibata A, Tsuji N. Effect of thermomechanical processing at α + γ two-phase temperatures on microstructure and mechanical property of 5Mn-0.1C-2Si medium-manganese steel. Mater Sci Eng A. 2019;743(August 2018):57-66. doi:10.1016/j.msea.2018.11.061
-
Xu HF, Zhao J, Cao WQ, et al. Heat treatment effects on the microstructure and mechanical properties of a medium manganese steel (0.2C-5Mn). Mater Sci Eng A. 2012;532:435-442. doi:10.1016/j.msea.2011.11.009
-
Xu YB, Zou Y, Hu ZP, Han DT, Chen SQ, Misra RDK. Correlation between deformation behavior and austenite characteristics in a Mn-Al type TRIP steel. Mater Sci Eng A. 2017;698(11):126-135. doi:10.1016/j.msea.2017.05.058
-
Huang H, Matsumura O, Furukawa T. Retained austenite in. 1994;10(July):621-626.
-
Grajcar A, Kuziak R, Zalecki W. Third generation of AHSS with increased fraction of retained austenite for the automotive industry. Arch Civ Mech Eng. 2012;12(3):334-341. doi:10.1016/j.acme.2012.06.011
-
Zhao X, Zhang Y, Shao C, Hui W, Dong H. Thermal stability of retained austenite and mechanical properties of medium-Mn steel during tempering treatment. J. Iron Steel Res. Int. 2017;24:830–837. doi:10.1016/s1006-706x(17)30123-1
-
Lee SJ, Matlock DK, Van Tyne CJ. An empirical model for carbon diffusion in austenite incorporating alloying element effects. ISIJ Int. 2011;51(11):1903-1911. doi:10.2355/isijinternational.51.1903
-
Yan S, Liu X, Liu WJ, Lan H, Wu H. Comparison on mechanical properties and microstructure of a C-Mn-Si steel treated by quenching and partitioning (Q&P) and quenching and tempering (Q&T) processes. Mater Sci Eng A. 2015;620:58-66. doi:10.1016/j.msea.2014.09.047
-
Technologies M, Campus C, Kelimeler A. Effect of Tempering Heat Treatment on Medium Manganese Steels Temperleme Isıl İşleminin Orta Manganlı Çelikler Üzerindeki Etkisi. 2023;4(1):31-36.
-
Pierce DT, Coughlin DR, Clarke KD, et al. Microstructural evolution during quenching and partitioning of 0.2C-1.5Mn-1.3Si steels with Cr or Ni additions. Acta Mater. 2018;151:454-469. doi:10.1016/j.actamat.2018.03.007
-
Han F, Hwang B, Suh DW, Wang Z, Lee DL, Kim SJ. Effect of molybdenum and chromium on hardenability of low-carbon boron-added steels. Met Mater Int. 2008;14(6):667-672. doi:10.3365/met.mat.2008.12.667
-
Beswick JM. The effect of chromium in high carbon bearing steels. Metall Trans A. 1987;18(11):1897-1906. doi:10.1007/bf02647019
-
Pelton AD, Koukkari P, Pajarre R, Eriksson G. Para-equilibrium phase diagrams. J Chem Thermodyn. 2014;72:16-22. doi:10.1016/j.jct.2013.12.023
-
Suzuki T, Ono Y, Miyamoto G, Furuhara T. Effects of Si and Cr on bainite microstructure of medium carbon steels. Tetsu-To-Hagane/Journal Iron Steel Inst Japan. 2010;96(6):392-399. doi:10.2355/tetsutohagane.96.392
-
Kirchner G, Nishizawa T, Uhrenius B. The distribution of chromium between ferrite and austenite and the thermodynamics of the α/γ equilibrium in the Fe-Cr and Fe-Mn Systems. Metall Trans. 1973;4(1):167-174. doi:10.1007/BF02649616
-
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