Araştırma Makalesi
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Sinkrotron Işınımı: Depolama Halkasından Sert X-ışını Demet Hattına

Yıl 2019, , 75 - 88, 31.12.2019
https://doi.org/10.17482/uumfd.534761

Öz

Bu çalışmada, elektronların bir elektron kaynağından salınması ile başlayıp sinkrotron ışınımı elde
edilmesine kadarki birbirini izleyen adımları kapsayan genel bir bakış sunulmuştur. Üçüncü nesil ışınım
kaynaklarının ana karakteristikleri ve temel bileşenleri ile farklı eklenti aygıtlarının ışınım
karakteristikleri de tartışılmıştır. Tipik bir sert X-ışını sinkrotron demet hattının kısaca tasvirinden sonra,
rezonans olmayan inelastik sert X-ışını tekniği olan, sinkrotron ışınımına dayalı X-ışını Raman saçılma
spektroskopisi açıklanmıştır. Son olarak, DESY-PETRA III sinkrotronundaki X-ışını Raman
spektrometresi kullanılarak, 10 keV enerjide 0.8 eV çözünürlükle kaydedilen sıvı fazdaki suyun oksijen
K-soğurma sınırı spektrumu sunulmuş ve literatürde geleneksel X-ışını soğurma spektroskobisi ile
ölçülen spektrum ile karşılaştırılmıştır. 

Kaynakça

  • Ascone, I. et al. (2004) PETRA III: A Low Emittance Synchrotron Radiation Source, Technical Design Report, EDMS ID: D00000000822371,A,1,1
  • Balerna, A. and Mobilio, S. (2015) Introduction to synchrotron radiation, Springer-Verlag Berlin Heidelberg. doi: 10.1007/978-3-642-55315-8_1
  • Basile, F. et al. (2010) Combined Use of Synchrotron‐Radiation‐Based Imaging Techniques for the Characterization of Structured Catalysts, Advanced Functional Materials, 20, 4117–4126. doi: 10.1002/ADFM.201001004
  • Bergmann, U. et al. (2002a) Bulk-sensitive XAS characterization of light elements: From X-ray Raman scattering to X-ray Raman spectroscopy, Microchemical Journal, 71, 221–230. doi: 10.1016/S0026-265X(02)00014-0
  • Bergmann, U. et al. (2002b) X-ray Raman spectroscopy at the oxygen K edge of water and ice: Implications on local structure models, Physical Review B, 66, 092107. doi: 10.1103/PhysRevB.66.092107
  • Braun, A. et al. (2015) Hard X-rays in–soft X-rays out: An operando piggyback view deep into a charging lithium ion battery with X-ray Raman spectroscopy. Journal of Electron Spectroscopy and Related Phenomena, 200, 257-263. doi: 10.1016/j.elspec.2015.03.005
  • Brown, G.E. and Sturchio, N.C. (2002) An Overview of Synchrotron Radiation Applications to Low Temperature Geochemistry and Environmental Science, Reviews in Mineralogy and Geochemistry, 49 (1) , 1-115. doi: 10.2138/gsrmg.49.1.1
  • Cai Y. Q. et al. (2005) Ordering of hydrogen bonds in high-pressure low-temperature H2O, Physical Reiew Letters, 94, 025502. doi: 10.1103/PhysRevLett.94.025502
  • Cotte, M. et al. (2010) Synchrotron-Based X-ray Absorption Spectroscopy for Art Conservation: Looking Back and Looking Forward, Accounts of Chemical Research, 43 (6),705–714. doi: 10.1021/ar900199m
  • Fukui, H. et al. (2007) Oxygen K-edge fine structures of water by x-ray Raman scattering spectroscopy under pressure conditions, Journal of Chemical Physics, 127, 134502. doi: 10.1063/1.2774988
  • Gomez, A. et al. (2018) The high-energy x-ray diffraction and scattering beamline at the Canadian Light Source, Review of Scientific Instruments, 89, 063301. doi: 10.1063/1.5017613
  • Gueriau, P. et al. (2017) Noninvasive Synchrotron-Based X-ray Raman Scattering Discriminates Carbonaceous Compounds in Ancient and Historical Materials. Analytical Chemistry, 89 (20), 10819-10826. doi: 10.1021/acs.analchem.7b02202
  • Hämäläinen, K. and Manninen, S. (2001) Resonant and non-resonant inelastic x-ray scattering, Journal of Physics-Condensed Matter, 13 (34), 7539–7555. doi: 10.1088/0953-8984/13/34/306
  • Huotari, S. et al. (2010) Direct tomography with chemical-bond contrast, Nature Materials, 10 (7), 489–493. doi: 10.1038/nmat3031
  • Iwamoto, H. (2018) Synchrotron Radiation X-ray Diffraction Techniques Applied to Insect Flight Muscle, International Journal of Molecular Sciences, 19 (6), 1748. doi: 10.3390/ijms19061748
  • Iitaka T. et al. (2015) Pressure-induced dissociation of water molecules in ice VII, Scientific Reports, 5, 12551. doi: 10.1038/srep12551
  • Jonas A. et al. (2014) Comparison of x-ray absorption spectra between water and ice: New ice data with low pre-edge absorption cross-section, Journal of Chemical Physics, 141, 034507. doi: 10.1063/1.4890035
  • Lee, S. K. et al. (2014) Probing of pressure-induced bonding transitions in crystalline and amorphous earth materials: insights from X-ray Raman scattering at high pressure, Reviews in Mineralogy and Geochemistry, 78 (1), 139-174. doi: 10.2138/rmg.2014.78.4
  • Lindegaard-Andersen, A. and Gerward, L. (1995) Röntgen centenary-100 years of X-rays, Radiation Physics and Chemistry, 46 (3), 299–302. doi: 10.1016/0969-806X(95)00063-4
  • Lutzenkirchen-Hecht, D. et al. (2014) The multi-purpose hard X-ay beamline BL10 at the DELTA storage ring, Journal of Synchrotron Radiation, 21, 819-826. doi: 10.1107/S1600577514006705
  • Mao W. L. et al. (2006) X-ray-induced dissociation of H2O and formation of an H2O2 alloy at high pressure, Science, 314, 636–638. doi: 10.1126/science.1132884
  • McCarthy, A. A. et al. (2018) ID30B–a versatile beamline for macromolecular crystallography experiments at the ESRF, Journal of Synchrotron Radiation, 25, 1249–1260 doi: 10.1107/S1600577518007166
  • Moffat, K. and Ren, Z. (1997) Synchrotron radiation applications to macromolecular crystallography, Current Opinion in Structural Biology, 7 (5), 689-696. doi: 10.1016/S0959-440X(97)80079-6
  • Myneni, S. et al. (2002) Spectroscopic probing of local hydrogen-bonding structures in liquid water, Journal of Physics Condensed Matter, 14 (8), L213. doi: 10.1088/0953-8984/14/8/106
  • Näslund, L. Å. et al. (2005) X-ray absorption spectroscopy measurements of liquid water, Journal of Physical Chemistry B, 109 (28), 13835-13839. doi: 10.1021/jp052046q
  • Nilsson, A. et al. (2010) X-ray absorption spectroscopy and x-ray Raman scattering of water and ice: an experimental view, Journal of Electron Spectroscopy and Related Phenomena, 177 (2-3), 99–129. doi: 10.1016/j.elspec.2010.02.005
  • Parent, P. et al. (2002) Structure of the water ice surface studied by x-ray absorption spectroscopy at the O K-edge, Journal of Chemical Physics, 117, 10842–10851. doi: 10.1063/1.1519256
  • Richard, F. et al. (2001) TESLA Technical Design Report Part I Executive Summary, ISBN: 3-935702-00-0, ISSN: 0418-9833
  • Sahle C. J. et al. (2013) Microscopic structure of water at elevated pressures and temperatures, Proceedings of the National Academy of Sciences, 110, 6301–6306. doi: 10.1073/pnas.1220301110
  • Sahle, C. J. et al. (2015) Planning, performing and analyzing X-ray Raman scattering experiments, Journal of Synchrotron Radiation, 22, 400-409. doi: 10.1107/S1600577514027581
  • Sahle, C. J. et al. (2016). In situ characterization of the decomposition behavior of Mg (BH4)2 by X-ray Raman scattering spectroscopy. Physical Chemistry Chemical Physics, 18 (7), 5397-5403. doi: 10.1039/C5CP06571B
  • Smith, J. D. et al. (2006) Probing the local structure of liquid water by x-ray absorption spectroscopy, Journal of Physical Chemistry B, 110 (40), 20038–20045. doi: 10.1021/jp063661c
  • Tse, J. S. et al. (2008) X-ray Raman spectroscopic study of water in the condensed phases, Physical Reiew Letters, 100, 095502. doi: 10.1103/PhysRevLett.100.095502
  • Yano, J. and Yachandra, V. K. (2009) X-ray absorption spectroscopy, Photosynthesis Research, 102, 241–254. doi: 10.1007/s11120-009-9473-8

SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE

Yıl 2019, , 75 - 88, 31.12.2019
https://doi.org/10.17482/uumfd.534761

Öz

In the present study, a general overview covering the consecutive steps, starting with the
release of electrons from an electron source until the generation of synchrotron radiation, is presented. A
brief introduction regarding the main characteristics and fundamental components of third generation
light sources as well as the radiation characteristics of different Insertion Devices are discussed.
Following a concise description of a typical hard X-ray synchrotron beamline, synchrotron radiation
based X-ray Raman scattering spectroscopy, which is a non-resonant inelastic hard X-ray technique, is
explained. Finally, liquid water oxygen K-edge absorption spectrum recorded with a resolution of 0.8 eV
at 10 keV utilizing X-ray Raman spectrometer at PETRA III facility of DESY is presented and
compared to the spectrum from the literature measured by conventional X-ray absorption spectroscopy.

Kaynakça

  • Ascone, I. et al. (2004) PETRA III: A Low Emittance Synchrotron Radiation Source, Technical Design Report, EDMS ID: D00000000822371,A,1,1
  • Balerna, A. and Mobilio, S. (2015) Introduction to synchrotron radiation, Springer-Verlag Berlin Heidelberg. doi: 10.1007/978-3-642-55315-8_1
  • Basile, F. et al. (2010) Combined Use of Synchrotron‐Radiation‐Based Imaging Techniques for the Characterization of Structured Catalysts, Advanced Functional Materials, 20, 4117–4126. doi: 10.1002/ADFM.201001004
  • Bergmann, U. et al. (2002a) Bulk-sensitive XAS characterization of light elements: From X-ray Raman scattering to X-ray Raman spectroscopy, Microchemical Journal, 71, 221–230. doi: 10.1016/S0026-265X(02)00014-0
  • Bergmann, U. et al. (2002b) X-ray Raman spectroscopy at the oxygen K edge of water and ice: Implications on local structure models, Physical Review B, 66, 092107. doi: 10.1103/PhysRevB.66.092107
  • Braun, A. et al. (2015) Hard X-rays in–soft X-rays out: An operando piggyback view deep into a charging lithium ion battery with X-ray Raman spectroscopy. Journal of Electron Spectroscopy and Related Phenomena, 200, 257-263. doi: 10.1016/j.elspec.2015.03.005
  • Brown, G.E. and Sturchio, N.C. (2002) An Overview of Synchrotron Radiation Applications to Low Temperature Geochemistry and Environmental Science, Reviews in Mineralogy and Geochemistry, 49 (1) , 1-115. doi: 10.2138/gsrmg.49.1.1
  • Cai Y. Q. et al. (2005) Ordering of hydrogen bonds in high-pressure low-temperature H2O, Physical Reiew Letters, 94, 025502. doi: 10.1103/PhysRevLett.94.025502
  • Cotte, M. et al. (2010) Synchrotron-Based X-ray Absorption Spectroscopy for Art Conservation: Looking Back and Looking Forward, Accounts of Chemical Research, 43 (6),705–714. doi: 10.1021/ar900199m
  • Fukui, H. et al. (2007) Oxygen K-edge fine structures of water by x-ray Raman scattering spectroscopy under pressure conditions, Journal of Chemical Physics, 127, 134502. doi: 10.1063/1.2774988
  • Gomez, A. et al. (2018) The high-energy x-ray diffraction and scattering beamline at the Canadian Light Source, Review of Scientific Instruments, 89, 063301. doi: 10.1063/1.5017613
  • Gueriau, P. et al. (2017) Noninvasive Synchrotron-Based X-ray Raman Scattering Discriminates Carbonaceous Compounds in Ancient and Historical Materials. Analytical Chemistry, 89 (20), 10819-10826. doi: 10.1021/acs.analchem.7b02202
  • Hämäläinen, K. and Manninen, S. (2001) Resonant and non-resonant inelastic x-ray scattering, Journal of Physics-Condensed Matter, 13 (34), 7539–7555. doi: 10.1088/0953-8984/13/34/306
  • Huotari, S. et al. (2010) Direct tomography with chemical-bond contrast, Nature Materials, 10 (7), 489–493. doi: 10.1038/nmat3031
  • Iwamoto, H. (2018) Synchrotron Radiation X-ray Diffraction Techniques Applied to Insect Flight Muscle, International Journal of Molecular Sciences, 19 (6), 1748. doi: 10.3390/ijms19061748
  • Iitaka T. et al. (2015) Pressure-induced dissociation of water molecules in ice VII, Scientific Reports, 5, 12551. doi: 10.1038/srep12551
  • Jonas A. et al. (2014) Comparison of x-ray absorption spectra between water and ice: New ice data with low pre-edge absorption cross-section, Journal of Chemical Physics, 141, 034507. doi: 10.1063/1.4890035
  • Lee, S. K. et al. (2014) Probing of pressure-induced bonding transitions in crystalline and amorphous earth materials: insights from X-ray Raman scattering at high pressure, Reviews in Mineralogy and Geochemistry, 78 (1), 139-174. doi: 10.2138/rmg.2014.78.4
  • Lindegaard-Andersen, A. and Gerward, L. (1995) Röntgen centenary-100 years of X-rays, Radiation Physics and Chemistry, 46 (3), 299–302. doi: 10.1016/0969-806X(95)00063-4
  • Lutzenkirchen-Hecht, D. et al. (2014) The multi-purpose hard X-ay beamline BL10 at the DELTA storage ring, Journal of Synchrotron Radiation, 21, 819-826. doi: 10.1107/S1600577514006705
  • Mao W. L. et al. (2006) X-ray-induced dissociation of H2O and formation of an H2O2 alloy at high pressure, Science, 314, 636–638. doi: 10.1126/science.1132884
  • McCarthy, A. A. et al. (2018) ID30B–a versatile beamline for macromolecular crystallography experiments at the ESRF, Journal of Synchrotron Radiation, 25, 1249–1260 doi: 10.1107/S1600577518007166
  • Moffat, K. and Ren, Z. (1997) Synchrotron radiation applications to macromolecular crystallography, Current Opinion in Structural Biology, 7 (5), 689-696. doi: 10.1016/S0959-440X(97)80079-6
  • Myneni, S. et al. (2002) Spectroscopic probing of local hydrogen-bonding structures in liquid water, Journal of Physics Condensed Matter, 14 (8), L213. doi: 10.1088/0953-8984/14/8/106
  • Näslund, L. Å. et al. (2005) X-ray absorption spectroscopy measurements of liquid water, Journal of Physical Chemistry B, 109 (28), 13835-13839. doi: 10.1021/jp052046q
  • Nilsson, A. et al. (2010) X-ray absorption spectroscopy and x-ray Raman scattering of water and ice: an experimental view, Journal of Electron Spectroscopy and Related Phenomena, 177 (2-3), 99–129. doi: 10.1016/j.elspec.2010.02.005
  • Parent, P. et al. (2002) Structure of the water ice surface studied by x-ray absorption spectroscopy at the O K-edge, Journal of Chemical Physics, 117, 10842–10851. doi: 10.1063/1.1519256
  • Richard, F. et al. (2001) TESLA Technical Design Report Part I Executive Summary, ISBN: 3-935702-00-0, ISSN: 0418-9833
  • Sahle C. J. et al. (2013) Microscopic structure of water at elevated pressures and temperatures, Proceedings of the National Academy of Sciences, 110, 6301–6306. doi: 10.1073/pnas.1220301110
  • Sahle, C. J. et al. (2015) Planning, performing and analyzing X-ray Raman scattering experiments, Journal of Synchrotron Radiation, 22, 400-409. doi: 10.1107/S1600577514027581
  • Sahle, C. J. et al. (2016). In situ characterization of the decomposition behavior of Mg (BH4)2 by X-ray Raman scattering spectroscopy. Physical Chemistry Chemical Physics, 18 (7), 5397-5403. doi: 10.1039/C5CP06571B
  • Smith, J. D. et al. (2006) Probing the local structure of liquid water by x-ray absorption spectroscopy, Journal of Physical Chemistry B, 110 (40), 20038–20045. doi: 10.1021/jp063661c
  • Tse, J. S. et al. (2008) X-ray Raman spectroscopic study of water in the condensed phases, Physical Reiew Letters, 100, 095502. doi: 10.1103/PhysRevLett.100.095502
  • Yano, J. and Yachandra, V. K. (2009) X-ray absorption spectroscopy, Photosynthesis Research, 102, 241–254. doi: 10.1007/s11120-009-9473-8
Toplam 34 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Mühendislik
Bölüm Araştırma Makaleleri
Yazarlar

Didem Ketenoğlu 0000-0002-2382-1413

Yayımlanma Tarihi 31 Aralık 2019
Gönderilme Tarihi 2 Mart 2019
Kabul Tarihi 29 Nisan 2019
Yayımlandığı Sayı Yıl 2019

Kaynak Göster

APA Ketenoğlu, D. (2019). SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE. Uludağ Üniversitesi Mühendislik Fakültesi Dergisi, 24(3), 75-88. https://doi.org/10.17482/uumfd.534761
AMA Ketenoğlu D. SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE. UUJFE. Aralık 2019;24(3):75-88. doi:10.17482/uumfd.534761
Chicago Ketenoğlu, Didem. “SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE”. Uludağ Üniversitesi Mühendislik Fakültesi Dergisi 24, sy. 3 (Aralık 2019): 75-88. https://doi.org/10.17482/uumfd.534761.
EndNote Ketenoğlu D (01 Aralık 2019) SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE. Uludağ Üniversitesi Mühendislik Fakültesi Dergisi 24 3 75–88.
IEEE D. Ketenoğlu, “SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE”, UUJFE, c. 24, sy. 3, ss. 75–88, 2019, doi: 10.17482/uumfd.534761.
ISNAD Ketenoğlu, Didem. “SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE”. Uludağ Üniversitesi Mühendislik Fakültesi Dergisi 24/3 (Aralık 2019), 75-88. https://doi.org/10.17482/uumfd.534761.
JAMA Ketenoğlu D. SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE. UUJFE. 2019;24:75–88.
MLA Ketenoğlu, Didem. “SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE”. Uludağ Üniversitesi Mühendislik Fakültesi Dergisi, c. 24, sy. 3, 2019, ss. 75-88, doi:10.17482/uumfd.534761.
Vancouver Ketenoğlu D. SYNCHROTRON RADIATION: FROM STORAGE RING TO A HARD X-RAY BEAMLINE. UUJFE. 2019;24(3):75-88.

DUYURU:

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