BibTex RIS Cite

PAN-Based Pd-doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A new Method for Chemical Activation and Characterization of Fibers

Year 2008, Volume: 36 Issue: 3, 247 - 253, 01.08.2008

Abstract

The preparation of ACFs from PAN fibers under various conditions and the method to load Pd on ACFs weredescribed. Chemical activation of the fibers increased the surface areas of the fibers from about 64 m2/g to 381 m2/g.SEM micrographs of Pd-loaded indicated the diameters of the fibers were in the range of 1.0-10.0 mm. Diameters ofmetallic Pd particles on the fibers changed between 80 nm and 100 nm. 4.5% by wt metallic palladium was depositedon the ACFs. This high percentage of palladium deposited on ACFs is useful for hydrogen storage, since Pd-H systemis established under a wide range of pressure and temperature

References

  • 1. A.C. Dillon, K.E.H. Gilbert, J.L. Alleman, T. Gennett, K.M. Jones, P. A. Parilla, M.J. Heben, in: Proceedings of the 2001 DOE Hydrogen Program Review, NREL/ CP-570-30535, 2001.
  • 2. E.David, J. Mater. Proc. Technol. 162/163 (2005) 169.
  • 3. G.G. Tibbetts, G.P. Meisner, C.H. Olk, Carbon 39 (2001) 292.
  • 4. H.M. Cheng, Q.H. Yang, C. Liu, Carbon 39 (2001) 1447.
  • 5. L. Zhou, Y. Zhou, Y. Sun, Int. J. Hydrogen Energy 29 (3) (2004) 319.
  • 6. R.K. Agarwal, J.S. Noh, J.A. Schwarz, P. Davini, Carbon 25 (1987) 219.
  • 7. J.A. Menendez, L.R. Radovic, B. Xia, J. Phillips, J. Phys. Chem. 100 (1996) 17243.
  • 8. P. Chen, X. Wu, J. Lin, K. L. Tan, Science 285 (1999) 91.
  • 9. Z.H. Zhu, G.Q. Lu, S.C. Smith, Carbon 42 (2004) 2509.
  • 10. S. Challet, P. Azais, R.J.M. Pellenq, O. Isnard, J. -L. Soubeyroux, L. Duclaux, J. Phys. Chem. Solids 65 (2004) 541.
  • 11. K. Kim, H. Lee, K. Han, J. Kim, M. Song, M. Park, J. Lee, J. Kang, J. Phys. Chem. B 109 (2005) 8983.
  • 12. S. Dag, Y. Ozturk, S. Ciraci, T. Yildirim, Phys. Rev. B 72 (2005) 155404.
  • 13. A. Lueking, R.T. Yang, J. Catal. 206 (2002) 165.
  • 14. F.H. Yang, A.J. Lachawiec, R.T. Yang, J. Phys. Chem. B 110 (2006) 6236.
  • 15. A. Anson, E. Lafuente, E. Urriolabeitia, R. Navarro, A.M. Benito, W.K. Maser, M.T. Martinez, J. Phys. Chem. B 110 (2006) 6643.
  • 16. H. Takagi, H. Hatori, Y. Yamada, S. Matsuo, M. Shiraishi, J. Alloy. Compd. 385 (2004) 257.
  • 17. J. Ozaki, W. Ohizumi, A. Oya, M. J. IllanGomez, M.C. Roman-Martinez, A. Linares-Solano, Carbon 38 (2000) 775.
  • 18. G. Shevla, G. Comprehensive Analytical Chemistry, Volume VI, Analytical Infrared Spectroscopy, Elsevier, Amsterdam, 1976, pp. 334.
  • 19. Y. Yürüm, N. Altuntas, Fuel Science and Technol. Int., 12 (1994) 1115.
  • 20. IUPAC Compendium of Chemical Terminology, second ed., vol. 46, 1997, p. 1976.
  • 21. D.A. Bulushev, I. Yuranov, E. I. Suvorova, P. A. Buffat, L. Kiwi-Minsker, J. Catalysis, 224 (2004) 8.
  • 22. G. Sandrock, Hydrogen-Metal Systems, in Hydrogen Energy System, Y. Yürüm (Ed.), NATO ASI Series E, Vol. 295, Kluwer Academic Publishers, Dordrecht, 1995, pp. 135.
There are 22 citations in total.

Details

Primary Language English
Journal Section Research Article
Authors

Serkan Baş This is me

Özgül Hakli This is me

Ahu Gümrah Dumanlı This is me

Yuda Yürüm This is me

Publication Date August 1, 2008
Published in Issue Year 2008 Volume: 36 Issue: 3

Cite

APA Baş, S., Hakli, Ö., Dumanlı, A. G., Yürüm, Y. (2008). PAN-Based Pd-doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A new Method for Chemical Activation and Characterization of Fibers. Hacettepe Journal of Biology and Chemistry, 36(3), 247-253.
AMA Baş S, Hakli Ö, Dumanlı AG, Yürüm Y. PAN-Based Pd-doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A new Method for Chemical Activation and Characterization of Fibers. HJBC. August 2008;36(3):247-253.
Chicago Baş, Serkan, Özgül Hakli, Ahu Gümrah Dumanlı, and Yuda Yürüm. “PAN-Based Pd-Doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A New Method for Chemical Activation and Characterization of Fibers”. Hacettepe Journal of Biology and Chemistry 36, no. 3 (August 2008): 247-53.
EndNote Baş S, Hakli Ö, Dumanlı AG, Yürüm Y (August 1, 2008) PAN-Based Pd-doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A new Method for Chemical Activation and Characterization of Fibers. Hacettepe Journal of Biology and Chemistry 36 3 247–253.
IEEE S. Baş, Ö. Hakli, A. G. Dumanlı, and Y. Yürüm, “PAN-Based Pd-doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A new Method for Chemical Activation and Characterization of Fibers”, HJBC, vol. 36, no. 3, pp. 247–253, 2008.
ISNAD Baş, Serkan et al. “PAN-Based Pd-Doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A New Method for Chemical Activation and Characterization of Fibers”. Hacettepe Journal of Biology and Chemistry 36/3 (August 2008), 247-253.
JAMA Baş S, Hakli Ö, Dumanlı AG, Yürüm Y. PAN-Based Pd-doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A new Method for Chemical Activation and Characterization of Fibers. HJBC. 2008;36:247–253.
MLA Baş, Serkan et al. “PAN-Based Pd-Doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A New Method for Chemical Activation and Characterization of Fibers”. Hacettepe Journal of Biology and Chemistry, vol. 36, no. 3, 2008, pp. 247-53.
Vancouver Baş S, Hakli Ö, Dumanlı AG, Yürüm Y. PAN-Based Pd-doped Activated Carbon Fibers for Hydrogen Storage: Preparation, A new Method for Chemical Activation and Characterization of Fibers. HJBC. 2008;36(3):247-53.

HACETTEPE JOURNAL OF BIOLOGY AND CHEMİSTRY

Copyright © Hacettepe University Faculty of Science

http://www.hjbc.hacettepe.edu.tr/

https://dergipark.org.tr/tr/pub/hjbc