Co Katkılı SnO2 Numunelerinin Sentez ve Karakterizasyonu

Yıl 2020, , 152 - 160, 28.06.2020

Tankut Ateş , Omer Kaygili , Niyazi Bulut , Havva Esma Okur , Serhat Keser , İ.s. Yahıa , Süleyman Köytepe , Turgay Seçkin , İmren Özcan Turan Ince

https://doi.org/10.35193/bseufbd.712514

Öz

Yüksek kristalleşmeye sahip katkısız ve Co katkılı SnO₂ numuneleri başarılı bir biçimde hazırlandı. Co içeriğinin SnO₂’nin termal ve morfolojik özellikleri üzerine etkileri araştırıldı. Co ilavesiyle Kristal büyüklüğünde ve birim hücre parametrelerinde değişimler tespit edildi. Co ilavesiyle faz bileşimi değişmedi. Hem X-ışını kırınımı hem de Fourier dönüşümlü kızılötesi sonuçları her bir numune için SnO₂ fazının oluşumunu doğruladı. Üretilen numunelerin oda sıcaklığından 900 °C’ye kadar termal kararlılığı gözlendi. Morfoloji Co içeriğinden etkilendi ve enerji dağılımlı X-ışını sonuçları SnO₂ yapısı içerisine Co’ın nüfuz ettiğini doğruladı.

Anahtar Kelimeler

Kristal yapı, Elektron mikroskobu, IR, X-ışını difraksiyon

Proje Numarası

FF.18.20

Synthesis and Characterization of Co-Doped SnO2 Samples

Öz

The un-doped and Co-doped SnO₂ samples having high crystallinity were successfully prepared. The effects of Co content on the structural, thermal and morphological properties of SnO₂ were investigated. Changes in the crystallite size and unit cell parameters were detected with adding of Co. The phase composition did not alter with the addition of Co. Both X-ray diffraction and Fourier transform infrared results confirmed the formation of the SnO₂ structure for each sample. The thermal stability of the as-produced samples from room temperature to 900 °C was observed. The morphology was affected by Co content, and energy dispersive X-ray results verified the introduction of Co into the SnO₂ structure.

Anahtar Kelimeler

Crystal structure, Electron microscopy, IR, X-ray diffraction

Destekleyen Kurum

Fırat Üniversitesi Bilimsel Arastırma Projeleri (FÜBAP) Koordinasyon Birimi

Proje Numarası

FF.18.20

Teşekkür

The authors extend their appreciation to the Deanship of Scientific Research at King Khalid University for funding this work through research groups program under Grant No. R.G.P.2/65/40. This work was also supported by the Management Unit of Scientific Research projects of Firat University (FÜBAP) (Project Number: FF.18.20).

Kaynakça

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