KIRMIZI PUL BİBER ÖRNEKLERİNDE ELEMENT İÇERİĞİNİN BELİRLENMESİ

Yıl 2019, , 1000 - 1007, 06.10.2019

Serpil Kılıç , Murat Kılıç

https://doi.org/10.15237/gida.GD19101

Cited By: 1

Öz

Çevresel kirlilikler, tarım ürünlerini tehdit etmekte ve
dolayısıyla insan sağlığı için risk oluşturmaktadır. Bu tarım ürünleri
içerisinde yer alan, kırmızıbiber, üretiminde kimyasal ilaçların kullanımı ise
sağlık için tehlike oluşturan bazı elementlerin kontamine olmasına sebep
olabilmektedir. Gıda sanayinde yaygın olarak kullanılan bir baharat çeşidi olan
ve özellikle gıdaları çeşnilendirmek için en çok kullanılan baharatlar arasında
yer alan kırmızıbiber tüketiminde, bu kontaminasyon insan sağlığını tehdit
edici unsur oluşturmaktadır. Bu çalışmada, kırmızıbibere kontamine olabilen
bazı metal kirleticiler (krom (Cr), kobalt (Co), bakır (Cu), demir (Fe), nikel
(Ni), selenyum (Se), çinko (Zn)) indüktif eşleşmiş plazma kütle spektrometrisi
kullanılarak (ICP-MS) tespit edildi. 
Analitik performansları; doğrusallık, tespit sınırı, ölçüm sınırı ve
geri kazanım olarak değerlendirildi. Metot validasyonu için sertifikalı
referans madde olarak Tomato Leaves 1573a kullanıldı. Çalışılan elementler için
geri kazanım,%98 ile %103 arasında değişmektedir. Örneklerde tüm metallerin
konsantrasyonları uluslararası ve Türk Gıda Kodeksinde belirtilen sınırları
aşmadığı gözlemlenmiştir.

Anahtar Kelimeler

Kırmızı pul biber, ICP-MS, metal analizi

Destekleyen Kurum

Akdeniz Üniversitesi

Proje Numarası

FBA-2017-2494

Teşekkür

Çalışmamızı FBA-2017-2494 proje numarası ile maddi olarak destekleyen Akdeniz Üniversitesi Bilimsel Araştırma Projeleri Koordinasyon Birimi’ne çok teşekkür ediyoruz.

DETERMINATION OF ELEMENT CONTENTS IN RED PEPPER SAMPLES

Öz

Environmental pollution threatens the agricultural
products and therefore poses a risk for human health. In the production of red
pepper which is one of these agricultural products, the use of chemical drugs,
may cause some elements with health hazards to be contaminated. The
contamination threatens human health in consumption of red pepper, which is
used in the food industry and is one of the most widely used spices for
seasoning foods. In this study, was determined of some metallic contaminants
(chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), nickel (Ni), selenium
(Se), zinc (Zn)) in red pepper using inductive coupled plasma mass spectrometry
(ICP-MS). The validation procedure was applied for the evaluation of linearity,
repeatability, recovery, limit of detection, and quantification. Tomato Leaves
1573a was used as certified reference material for method validation. The
recovery ranged from 98% to 103% for studied elements. It is observed that the
concentrations of all metals in samples did not exceed the international and
Turkish codex values.

Anahtar Kelimeler

Red pepper, ICP-MS, metal analysis

Proje Numarası

FBA-2017-2494

Kaynakça

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