Yıl 2019, Cilt 31 , Sayı 4, Sayfalar 295 - 304 2019-11-01

Hidroksiapatit / seryum oksit kompozitleri: Sinterleme, mikroyapısal, mekanik ve invitro biyoaktivite özellikleri
Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties

Süleyman Serdar PAZARLIOĞLU [1]


Effect of cerium oxide (CeO2) additive on the microstructure, mechanical and invitro bioactivity properties of a commercially synthetic hydroxyapatite (HA) was investigated. HA without CeO2 started to decompose at 1100 oC, but the decomposition temperature of the CeO2 added samples decreased up to 900 oC. Decomposition rate of the sintered samples increased as the sintering temperature reached to 1300 oC. It was about 5.8% for monolithic HA, and increased to 11.4% when the CeO2 additive to HA reached to 2.5 wt%. SEM images showed that an excessive grain growth as well as microcracks occured on the surface of monolithic HA when it was sintered at the temperatures than that of 1100 oC. The microcracks were also observed on the surface of HA-CeO2 composites, when they were sintered at 1300 oC. The composite of HA-0.5CeO2 sintered at 1100 oC possess the higher fracture toughness (Kıc) (2.510 ± 0.225 MPam1/2) and the higher compressive strength (152.73 ± 6.31 MPa) compared to other HA-CeO2 composites, and it's mechanical properties are higher than that of monolithic HA at about 2-3 times. In-vitro bioactivity test results showed that apatite layers on the surface of the samples were in the different morphologies. 

Effect of cerium oxide (CeO2) additive on the microstructure, mechanical and invitro bioactivity properties of a commercially synthetic hydroxyapatite (HA) was investigated. HA without CeO2 started to decompose at 1100 oC, but the decomposition temperature of the CeO2 added samples decreased up to 900 oC. Decomposition rate of the sintered samples increased as the sintering temperature reached to 1300 oC. It was about 5.8% for monolithic HA, and increased to 11.4% when the CeO2 additive to HA reached to 2.5 wt%. SEM images showed that an excessive grain growth as well as microcracks occured on the surface of monolithic HA when it was sintered at the temperatures than that of 1100 oC. The microcracks were also observed on the surface of HA-CeO2 composites, when they were sintered at 1300 oC. The composite of HA-0.5CeO2 sintered at 1100 oC possess the higher fracture toughness (Kıc) (2.510 ± 0.225 MPam1/2) and the higher compressive strength (152.73 ± 6.31 MPa) compared to other HA-CeO2 composites, and it's mechanical properties are higher than that of monolithic HA at about 2-3 times. In-vitro bioactivity test results showed that apatite layers on the surface of the samples were in the different morphologies. 

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Birincil Dil en
Konular Mühendislik
Yayımlanma Tarihi 2019
Bölüm Araştırma Makaleleri
Yazarlar

Orcid: 0000-0002-7870-8418
Yazar: Süleyman Serdar PAZARLIOĞLU (Sorumlu Yazar)
Kurum: MARMARA ÜNİVERSİTESİ
Ülke: Turkey


Tarihler

Yayımlanma Tarihi : 1 Kasım 2019

Bibtex @araştırma makalesi { jeps512240, journal = {International Journal of Advances in Engineering and Pure Sciences}, issn = {}, eissn = {2636-8277}, address = {fbedergi@marmara.edu.tr}, publisher = {Marmara Üniversitesi}, year = {2019}, pages = {295 - 304}, doi = {10.7240/jeps.512240}, title = {Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties}, key = {cite}, author = {PAZARLIOĞLU, Süleyman Serdar} }
APA PAZARLIOĞLU, S . (2019). Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties. International Journal of Advances in Engineering and Pure Sciences , 31 (4) , 295-304 . DOI: 10.7240/jeps.512240
MLA PAZARLIOĞLU, S . "Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties". International Journal of Advances in Engineering and Pure Sciences 31 (2019 ): 295-304 <https://dergipark.org.tr/tr/pub/jeps/article/512240>
Chicago PAZARLIOĞLU, S . "Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties". International Journal of Advances in Engineering and Pure Sciences 31 (2019 ): 295-304
RIS TY - JOUR T1 - Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties AU - Süleyman Serdar PAZARLIOĞLU Y1 - 2019 PY - 2019 N1 - doi: 10.7240/jeps.512240 DO - 10.7240/jeps.512240 T2 - International Journal of Advances in Engineering and Pure Sciences JF - Journal JO - JOR SP - 295 EP - 304 VL - 31 IS - 4 SN - -2636-8277 M3 - doi: 10.7240/jeps.512240 UR - https://doi.org/10.7240/jeps.512240 Y2 - 2019 ER -
EndNote %0 International Journal of Advances in Engineering and Pure Sciences Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties %A Süleyman Serdar PAZARLIOĞLU %T Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties %D 2019 %J International Journal of Advances in Engineering and Pure Sciences %P -2636-8277 %V 31 %N 4 %R doi: 10.7240/jeps.512240 %U 10.7240/jeps.512240
ISNAD PAZARLIOĞLU, Süleyman Serdar . "Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties". International Journal of Advances in Engineering and Pure Sciences 31 / 4 (Kasım 2019): 295-304 . https://doi.org/10.7240/jeps.512240
AMA PAZARLIOĞLU S . Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties. JEPS. 2019; 31(4): 295-304.
Vancouver PAZARLIOĞLU S . Hydroxyapatite/cerium oxide composites: Sintering, microstructural, mechanical and invitro bioactivity properties. International Journal of Advances in Engineering and Pure Sciences. 2019; 31(4): 304-295.