TiO2 Nanopartikülü İle Fonksiyonelleştirilmiş Çok Duvarlı Karbon Nanotüpün Su Bazlı Sondaj Çamuruna Etkisinin Belirlenmesi: Deneysel Çalışma

Öz

Bu çalışmada, su bazlı sondaj çamuruna (Na-Bentonit bazlı) fonksiyonelleştirilmiş karbon nanotüpün etkisinin tespiti amaçlanmıştır. Bu kapsamda su bazlı sondaj çamurları hazırlanmış ve kimyasal buhar biriktirme (CVD) yöntemi ile üretilen TiO2 nanopartikülü ile fonksiyonelleştirilmiş çok duvarlı karbon nanotüp (TiO2NP/ÇDKNT) farklı oranlarda (0.001 – 0.01 % k/h) eklenmiştir. Hazırlanan sondaj çamurlarının plastik viskozitesi (PV), görünür viskozitesi (AV), kopma noktası (YP), jel mukavemeti değerleri (10 saniye ve 10 dakika) gibi reolojik özellikleri FANN viskozimetresi ile ayrıca su (filtrasyon) kaybı ve sondaj çamuru kek kalınlığı Amerikan Petrol Enstitüsü (API) sıvı kaybı test ekipmanları ile API standartlarına uygun olacak şekilde detaylı analiz edilmiştir. TiO2NP/ÇDKNT’ün eklenmesi ile hazırlanan sondaj çamurlarının reolojik ve filtrasyon özellikleri kendi içlerinde, daha sonra da katkısız sondaj çamuru ile karşılaştırılmıştır. Elde edilen sonuçlara göre; TiO2NP/ÇDKNT’ün su bazlı sondaj çamuruna eklenmesiyle; PV değerinin % 71.4; AV değerinin % 41.8; YP değerinin % 28; 10 saniye değerinin % 8.3; 10 dakika değerinin % 5.6 arttığı; filtrasyon kaybının % 8.6 azaldığı; aynı zamanda da kek kalınlığı değerinin de % 11 oranında arttığı görülmüştür. Yapılan bu çalışmayla; TiO2NP/ÇDKNT’ün sondaj çamurunun reolojik özellikleri ile filtrasyon kaybı değerlerine olumlu yönde katkı sağladığı tespit edilmiştir.

Anahtar Kelimeler

• Su bazlı sondaj çamuru,nanopartikül madde,fonksiyonelleştirilmiş çok katmanlı karbon nanotüp,kimyasal buhar biriktirme yöntemi

Effect of TiO2 Nanoparticle Functionalized Multi-Walled Carbon Nanotubes on the Water Based Drilling Fluid: Experimental Study

Öz

In this study, it is aimed to determine the effect of functionalized carbon nanotube on water-based drilling mud (Na-Bentonite based). In this context, water based drilling muds were prepared and multi-walled carbon nanotube (TiO2NP/MWCNTs) functionalized with TiO2 nanoparticle produced by chemical vapor deposition (CVD) method was added in different ratios (0.001 - 0.01% w/v). The rheological properties of the prepared drilling muds such as plastic viscosity (PV), apparent viscosity (AV), yield point (YP), gel strength values (10 seconds and 10 minutes) were determined with a FANN viscometer, as well as water (filtration) loss and drilling mud cake thickness have been analyzed using American Petroleum Institute liquid loss test equipment accordance API standards in detail. The rheological and filtration properties of the drilling muds prepared by adding TiO2NP/MWCNTs were compared with each other and then with pure drilling mud. According to the results obtained; 71.4% of PV, 41.8% of AV value, 28% of the YP value, 8.3% of 10 seconds, 5.6% of 10 minutes increased and 8.6% of the loss of filtration decreased by adding TiO2NP/MWCNTs to water based drilling mud. At the same time, cake thickness value increased by 11%. With this study; it was found that TiO2NP/MWCNTs contributed positively to the rheological properties and filtration loss values of the drilling mud.

Anahtar Kelimeler

• Water based drilling mud,nanoparticle substance,functionalized multi-walled carbon nanotube,chemical vapor deposition method

Kaynakça

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