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Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes

Yıl 2022, , 200 - 210, 20.08.2022

Sevi Öz , Pınar Acar Bozkurt , Şaziye Betül Sopacı , Nurcan Acar , Orhan Atakol

https://doi.org/10.19113/sdufenbed.996596
Cited By: 1

Öz

Five different Nickel (II) complexes were prepared using a ONNO type Schiff base bis-N;N’(salicylidene)-1,3-propanediamine (LH2) and an ONO type Schiff base N(2-hydroxy)salicylaldimine (SAPH2) in the presence of NH3 or amine and NiO nanoparticles were obtained with thermal decomposition of this complexes in air. The prepared complexes and Schiff bases have been characterized by element analysis, IR spectroscopy, Thermogravimetry (TG), 1HNMR and 13CNMR spectroscopy, Mass Spectrometry (MS), Atomic absorption spectrometry (AAS), and Scanning Electron Microscopy (SEM). The surface area of the obtained nanoparticle NiO material was measured by the Brunauer-Emmett-Teller (BET) method. The thermal decomposition products NiO nanoparticles were investigated with XRD, and SEM technics. SEM investigations showed that due to the very little solubility of the prepared two complexes and consequently they were precipitated in the form of nanoparticles. In addition, it observed that this very insoluble complexes are converted to NiO nanoparticles a result of thermal decomposition.

Anahtar Kelimeler

ONO type Schiff base ONNO type Schiff base Schiff base complexes Thermal decomposition NiO nanoparticles

Kaynakça

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Ni(II) – ONO ve ONNO Tipi Schiff Bazı Komplekslerinin Termal Bozunmalarını Kullanarak NiO Nanopartiküllerinin Sentezi ve Karakterizasyonu

Yıl 2022, , 200 - 210, 20.08.2022

Sevi Öz , Pınar Acar Bozkurt , Şaziye Betül Sopacı , Nurcan Acar , Orhan Atakol

https://doi.org/10.19113/sdufenbed.996596
Cited By: 1

Öz

Bir ONNO tipi Schiff bazı olan bis-N;N'(salisiliden)-1,3-propandiamin (LH2) ve ONO tipi Schiff bazı olan N(2-hidroksi)salisillaldimin (SAPH2) kullanılarak beş farklı Nikel (II) kompleksi NH3 veya amin varlığında hazırlandı ve bu komplekslerin havada termal bozunması ile NiO nanoparçacıkları elde edildi. Hazırlanan kompleksler ve Schiff bazları, element analizi, IR spektroskopisi, Termogravimetri (TG), 1HNMR ve 13CNMR spektroskopisi, Kütle Spektrometrisi (MS), Atomik absorpsiyon spektrometrisi (AAS), ve Taramalı Elektron Mikroskobu (SEM) ile karakterize edildi. Elde edilen nanoparçacık NiO malzemenin yüzey alanı Brunauer-Emmett-Teller (BET) yöntemi ile ölçüldü. NiO nanoparçacıklarının termal bozunma ürünleri XRD ve SEM teknikleri ile incelendi. SEM incelemeleri, hazırlanan iki kompleksin çözünürlüğünün çok az olması nedeniyle nanopartiküller halinde çöktüğünü gösterdi. Bu sebepten dolayı çözünmeyen komplekslerin termal bozunma sonucunda NiO nanoparçacıklarına dönüştüğü gözlemlendi.

Anahtar Kelimeler

ONO tipi Schiff bazı ONNO tipi Schiff bazı Schiff bazı kompleksleri Ttermal bozunma NiO nanoparçacıkları

Kaynakça

  • [1] Chen, Y. N., Ge, Y. Y., Zhou, W., Ye, L. F., Gu, Z. G., Ma, G. Z., Li, W. S., Li, H., Cai, Y. P. 2011. The First Mn-Zn Heterometallic Dinuclear Compound Based On Schiff Base Ligand N,N’-Bis(Salicylidene)-1,3-Propanediamine. Inorg Chem Comm., 14, 1228-1232.
  • [2] Aksu, M., Durmuş, S., Sarı, M., Emregül, K. C., Svoboda, I., Fuess, H., Atakol O. 2007. Investigation of Thermal Decomposition Some Heterodinuclear Niii-Mii Complexes Prepared from ONNO Type Reduced Schiff Base Compounds. J Therm Anal Cal., 90, 541-547.
  • [3] Chacraborty, P., Mohanta, S. 2015. Mononuclear and Heterometallic Dinuclear, Trinuclear and Dimer-of-Dinuclear Complexes Derived from Single- and Double-Compartment Schiff Base Ligands Having a Less Utilized Diamine. Polyhedron, 87, 98-108.
  • [4] Hazari, A, Das, A, Mahapatra, P, Ghosh, A. 2017. Mixed Valence Trinuclear Cobalt(II/III) Complexes. Polyhedron, 134, 99-106.
  • [5] Mahapatra, P., Ghosh, S., Koizumi, N., Kanetomo, T., Ishida, T., Drew, M.G.B., Ghosh, A. 2017. Structural Variations in (Cul)2ln Complexes of a Series of Lanthanide Ions with a Salen Type Unsymmetrical Schiff Base (H2L). Dalton Trans., 46, 12095-12105.
  • [6] Mahapatra, P., Ghosh, S., Giri, S., Rane, V., Kadam, R., Drew, M.G.B., Ghosh, A. 2017. Subtle Structural Changes in (CuIIL)2MnII Complexes to Induce Heterometallic Cooperative Catalytic Oxidase Activities of Phenolic Substrates (H2L=Salen Type Unsymmetrical Schiff Base). Inorg Chem., 56, 5105-5121.
  • [7] Zhou, H., Chen, C., Lu, J., Liu, Y., Shen, X. 2016. New Examples of Hetero-tri-Metallic Complexes CuII-LnIII-MIII (M=Cr,Fe; Ln=Gd,Dy,Er). Inorg Chim Acta, 453, 482-487.
  • [8] Ghosh, S., Ghosh, A. 2016. Coordination of Metalloligand [NiL] (H2L=Salen Type N2O2 Type Schiff Base Ligand to the f Block Elements. Inorg Chim Acta, 442, 64-69.
  • [9] Seth, P., Figuerola, A., Jover, J., Ruiz, E., Ghosh, A. 2016. Antiferro- to Ferromagnetic Crossover in Phenoxido Bridged NiII2MnII Complexes Derived from N2O2 Donor Schiff Base Ligands. Polyhedron, 117, 57-63.
  • [10] Hazari, A., Giri, S., Diaz, C., Ghosh, A. 2016. Unusual Site Electron of NCS- in Trinuclear Complexes of Cu(II) and Ni(II) with a Reduced N2O2 Donor Schiff Base. Polyhedron, 118, 70-80.
  • [11] Alexandru, M. G., Visinescu, D., Andruh, M., Marino, N., Armentano, D., Cano, J., Lloret, F., Julve, M. 2015. Heterotrimetallic Coordination Polymers. Chem Eur J., 21, 5429-5446.
  • [12] Saha, S., Sasmal, A., Choudhury, C. R., Gomez-Garcia, C. J., Garribba, E., Mitra, S. 2014. A New Double Phenoxide-Bridged Trinuclear Cu(II)-Schiff Base Complex. Polyhedron, 69, 262-269.
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  • [14] Biswas, S., Diaz, C., Ghosh, A. 2013. The First Triple Phenoxido-Bridged Triangular NIICuII2 Complexes with a N2O2 Donor di-Schiff Base and Pseudohalide (N(CN)2- or NCS-) Ligands. Polyhedron, 51, 96-101.
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  • [16] Fukuhara, C., Tsuneyoshi, K., Matsumoto, N., Kida, S., Mikuriya, M., Mori, M. 1990. Synthesis and Characterization of Trinuclear Schiff Base Complexes Containing Sulphure Dioxide or Hydrogensulphide Ions as Bridging Group. JCS Dalton Trans., 11, 3473-3479.
  • [17] Song, Y., Gamez, P., Roubeau, O., Mutikainen, I., Turpeinen, U., Reedijk, J. 2005. Structure and Magnetism of Two New Trinuclear Copper(II) Clusters Obtained from the Tetradentate N2O2 Ligand Bis(2-Hydroxybenzyl)-1,3-Diaminopropane. Inorg Chim Acta, 358, 109-115.
  • [18] Kurtaran, R., Yıldırım, L. T., Azaz, A. D., Namlı, H., Atakol, O. 2005. Synthesis, Characterization, Crystal Structure and Biological Activity of a Novel Heterotetranuclear Complex J Inorg Biochem., 99, 1937-1944.
  • [19] Uhlenbrock, S., Wegner, R., Krebs, B. 1996. Synthesis and Characterization of Novel Tri- and Hexanuclear Zinc Complexes with Biomimetic Chelate Ligands. JCS Dalton Trans., 18, 3731-3736.
  • [20] Atakol, O., Nazir, H., Arıcı, C., Durmuş, S., Svoboda, I., Fuess, H. 2003. Some New Ni-Zn Heterodinuclear Complexes: Square-Pyramidal Nickel(Ii) Coordination. Inorg Chim Acta 342, 295-300.
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  • [24] Maggio, F., Pizzino, T., Romano, V. 1974. Complexes of First Series Transition Metals Formally Tricoordinated. Inorg Nuclear Chem Lett., 10, 1005-1008.
  • [25] Maggio, F., Pizzino, T., Romano, V., Dia, G. 1976. Adduct Formation by Sub-Coordinated Metal Complexes. J Inorg Nucl Chem., 38, 599-601.
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  • [28] Haggag, S. M. S., Abdel-Hamid, I. A. M. 2015. A Tridentate (O,N,O) Donor Schiff Base Zinc(II) Nano Complex. J Therm Anal Cal., 119, 737-746.
  • [29] Mohammadikish, M. 2015. Green Synthesis and Growth Mechanism of New Nanomaterial: Zn(Salen) Nanocomplex. J Crystal Growth, 431, 39-48.
  • [30] Grivani, G., Vakili, M., Khalaji, A. D., Bruno, G., Rudbari, H. A., Taghavi, M., Tahmasebi, V. 2014. Synthesis, Characterization, Crystal Structure Determination, Computational Study and Thermal Decomposition into NiO Nanoparticles of a New NiIIL2 Schiff Base Complex. J Mol Struct., 1072, 77-83.
  • [31] Grivani, G., Eigner, V., Dusek, M., Sadeghi, B., Khalaji, A. D. 2015. New µ-OAC Bridged Dinuclear Copper(Ii) Complex with Tridentate Schiff Base Ligand. Russ J Coord Chem., 41, 456-461.
  • [32] Elseman, A. M., Rayan, D. A., Rashad, M. M. 2016. Structure, Optical and Magnetic Behaviour of Nanocrystalline CuO Nanopowders Synthesized via a New Technique Using Schiff Base Complex. J Mater Sci: Mater Electron, 27, 2652-2661.
  • [33] El-Mekharbel, S. M., Megahed, A. S., Refat, M. S. 2016. Preparation, Physical and Chemical Studies on Metal Complexes of Schiff Base as Nucleus Key to Prepare Nanometer Oxides Have Catalytic Applications. J Mol Liquids, 216, 608-614.
  • [34] Parsaee, Z., Mohammadi, K., Ghahramaninezhad, M., Hosseinzadeh, B. 2016. A Novel Nano-Sized Binuclear Nickel(II) Schiff Base Complex as a Precursor for NiO Nanoparticles. New J Chem., 40, 10569-10583.
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  • [36] El-samanoyedi El-Sayed, A., Emam, S.M., Emara, E.M. 2017. Synthesis, Characterization, Molecular Modelling and Biological Activity of Metal Complexes Derived from (E)-N’-(Furan-2-Ylmethylene)Morpholine-4-Carbothiohydrazide. J Mol Struct., 1146, 868-880.
  • [37] Kalam, A., Al-Sehemi, A. G., Al-Shihri, A. S., Du, G., Tokeer, A. 2012. Synthesis and Characterization of NiO Nanoparticles by Thermal Decomposition of Nickel Linoleat and Their Optical Properties. Material Characterization, 68, 77 -81.
  • [38] Saednia, S., Iranmanesh, P., Arkadani, M.H., Mohammeadi, M., Norouzi, G.H. 2016. Phenoxo Bridged Dinuclear Zn(Ii) Schiff Base Complex as New Precursor for Preparation Zinc Oxide Nanoparticles: Synthesis, Characterization, Crystal Structures and Photoluminescence Studies. Mater Res Bull., 78, 1-10.
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  • [41] Elerman, Y., Kabak, M., Svoboda, I., Fuess, H., Griesar, K., Haase, W. 1996. Structure and Magnetic Properties of a Triply Oxygen. Bridged Dinuclear Ni(II) Complex. Z Naturforsch B, 51, 1132-1136.
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  • [45] Greenwood, N. N., Earnshow, A. 1994. Chemistry of The Elements, Pergamon Press.
  • [46] Khalaji, A .D., Nikookar M., Das D. 2014. Co(III), Ni(II) and Cu(II) complex of bidentate N, O-donor Schiff base ligand derived from 4-methoxy-2-nitroaniline and salicylaldehyde. J Therm Anal Cal., 115, 409-417.
  • [47] Rashad M. M., Hassan A. M., Nassar A. M., Ibrahim N. M., Mourdata A. 2014. A new nano-strUctured Ni(II) Schiff base complex. Appl Phys A, 117, 877-890.
  • [48] Khalaji A. D., Grivani G., Izadi S., Ebadi M. 2018. Facile synthesis of Ni/NiO nanocomposites via thermal decomposition. J Nanoanalysis, 5, 115-120.
  • [49] Saghadforoush, L. A., Mehdizadeh R., Chalabian F. 2010. Hydrothermal and sonochemical synthesis of nano-sized nickel(II) Schiff base complex as a precursor for nansized nickel(II) oxide. Transtion Met Chem., 35, 903-910. [50] Barfeie, H., Grivani, G., Eigner, V., Dusek, M., Khalaji, A.D. 2018. Copper(II), nickel(II), zinc(II) and vanadium(IV) Schiff base complexes. Polyhedron, 146, 19-25.
  • [51] Refat, M. S., El-Sayed, M. Y., Adam, A. M. A. 2013. Cu(II), Co(II) and Ni(II) complexes of new Schiff base ligand. J Mol Struct., 1038, 62-72.
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  • [54] Khansari, A., Enhessari, M., Salavati-Niasari, M. 2013. Synthesis and Characterization of Nickel oxide Nanoparticles from Ni(salen)as Precursor. J Clust Sci., 24, 289-297.
  • [55] Moosavi, S., Zakariya, S., Chia, C. H., Gan, S., Azahari, N. A. 2017. Hydrothermal Synthesis, Magnetic Properties and Characterization of CoFe2O4 Nanocrystals. Ceramic Int., 43, 7889-7894.
Toplam 54 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Mühendislik
Bölüm Makaleler
Yazarlar

Sevi Öz 0000-0002-4628-0365

Pınar Acar Bozkurt 0000-0001-8743-9734

Şaziye Betül Sopacı 0000-0002-2840-4985

Nurcan Acar 0000-0003-3531-9073

Orhan Atakol 0000-0003-0977-6588

Yayımlanma Tarihi 20 Ağustos 2022
Yayımlandığı Sayı Yıl 2022

Kaynak Göster

APA Öz, S., Acar Bozkurt, P., Sopacı, Ş. B., Acar, N., vd. (2022). Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 26(2), 200-210. https://doi.org/10.19113/sdufenbed.996596
AMA Öz S, Acar Bozkurt P, Sopacı ŞB, Acar N, Atakol O. Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. Ağustos 2022;26(2):200-210. doi:10.19113/sdufenbed.996596
Chicago Öz, Sevi, Pınar Acar Bozkurt, Şaziye Betül Sopacı, Nurcan Acar, ve Orhan Atakol. “Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 26, sy. 2 (Ağustos 2022): 200-210. https://doi.org/10.19113/sdufenbed.996596.
EndNote Öz S, Acar Bozkurt P, Sopacı ŞB, Acar N, Atakol O (01 Ağustos 2022) Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 26 2 200–210.
IEEE S. Öz, P. Acar Bozkurt, Ş. B. Sopacı, N. Acar, ve O. Atakol, “Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes”, Süleyman Demirel Üniv. Fen Bilim. Enst. Derg., c. 26, sy. 2, ss. 200–210, 2022, doi: 10.19113/sdufenbed.996596.
ISNAD Öz, Sevi vd. “Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 26/2 (Ağustos 2022), 200-210. https://doi.org/10.19113/sdufenbed.996596.
JAMA Öz S, Acar Bozkurt P, Sopacı ŞB, Acar N, Atakol O. Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. 2022;26:200–210.
MLA Öz, Sevi vd. “Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, c. 26, sy. 2, 2022, ss. 200-1, doi:10.19113/sdufenbed.996596.
Vancouver Öz S, Acar Bozkurt P, Sopacı ŞB, Acar N, Atakol O. Synthesis and Characterization of NiO Nanoparticles by Using Thermal Decompositions of Ni(II) – ONO and ONNO Type Schiff Base Complexes. Süleyman Demirel Üniv. Fen Bilim. Enst. Derg. 2022;26(2):200-1.

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https://doi.org/10.1134/S1061933X22600610

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