Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent

Hayriye Aral

doi:10.53433/yyufbed.1315917

TR EN

Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent

Öz

The enrichment and simultaneous analysis of Cu2+, Cr3+, Co2+, and Ni2+ by solid-phase extraction method were performed using a stationary phase containing amide functional groups, an aromatic benzene ring, and aliphatic groups in a silica-based structure that we had synthesized for HPLC separations in our previous studies. Solid-phase extraction was performed using a column system and the results obtained were analysed by ICP-OES. Effects of pH, amount of sorbent, amount of eluting solvent, sample volume, flow rates of the eluent and the sample, and interfering ions were evaluated in recovery processes for the metals in the sample solutions. Linear range, detection limit, and relative standard deviation (% RSD) values were calculated for each metal. The linear range (ng/mL) was between 0.01 and 0.25 for all ions, while the limit of detection (ng/mL) was found to be 0.64, 1.7, 0.44, and 0.51 and % RSD was 2.8, 2.4, 2.6, and 2.9 for Cu2+, Cr3+, Co2+, ve Ni2+, respectively.

Anahtar Kelimeler

Chromium, Cobalt, Copper, Nickel, Solid-based stationary phase, Solid-phase extraction

Kaynakça

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Ayrıntılar

Birincil Dil

İngilizce

Konular

Enstrümantal Yöntemler, Separasyon Bilimi

Bölüm

Araştırma Makalesi

Yazarlar

Hayriye Aral ^*
0000-0001-7673-5108
Türkiye

Yayımlanma Tarihi

30 Nisan 2024

Gönderilme Tarihi

17 Haziran 2023

Kabul Tarihi

30 Ekim 2023

Yayımlandığı Sayı

Yıl 2024 Cilt: 29 Sayı: 1

DOI

https://doi.org/10.53433/yyufbed.1315917

IZ

https://izlik.org/JA85GY47CT

APA

Aral, H. (2024). Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 29(1), 109-118. https://doi.org/10.53433/yyufbed.1315917

AMA

1.Aral H. Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent. YYUFBED. 2024;29(1):109-118. doi:10.53433/yyufbed.1315917

Chicago

Aral, Hayriye. 2024. “Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent”. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi 29 (1): 109-18. https://doi.org/10.53433/yyufbed.1315917.

EndNote

Aral H (01 Nisan 2024) Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi 29 1 109–118.

IEEE

[1]H. Aral, “Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent”, YYUFBED, c. 29, sy 1, ss. 109–118, Nis. 2024, doi: 10.53433/yyufbed.1315917.

ISNAD

Aral, Hayriye. “Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent”. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi 29/1 (01 Nisan 2024): 109-118. https://doi.org/10.53433/yyufbed.1315917.

JAMA

1.Aral H. Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent. YYUFBED. 2024;29:109–118.

MLA

Aral, Hayriye. “Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent”. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi, c. 29, sy 1, Nisan 2024, ss. 109-18, doi:10.53433/yyufbed.1315917.

Vancouver

1.Hayriye Aral. Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent. YYUFBED. 01 Nisan 2024;29(1):109-18. doi:10.53433/yyufbed.1315917

Cited By

ZnO nanoparticles coated with EDTA and Ag nanoparticles (ZnO@EDTA-Ag NPs) for enhanced electrochemical detection of Cu2+ ions in food and environmental samples

Microchemical Journal

https://doi.org/10.1016/j.microc.2025.113562

Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent

Cu2+, Cr3+, Co2+, and Ni2+’nin Son Zamanlarda Geliştirilen Karma Mod Bir Sorbent Kullanılarak Katı Faz Ekstraksiyonu ile Zenginleştirilmesi

Öz

Anahtar Kelimeler

Preconcentration of Cu2+, Cr3+, Co2+, and Ni2+ by Solid-Phase Extraction Using a Recently Developed Mixed-Mode Sorbent

Öz

Anahtar Kelimeler

Kaynakça

Ayrıntılar

Birincil Dil

Konular

Bölüm

Yazarlar

Yayımlanma Tarihi

Gönderilme Tarihi

Kabul Tarihi

Yayımlandığı Sayı

DOI

IZ

Kaynak Göster

Cited By

ZnO nanoparticles coated with EDTA and Ag nanoparticles (ZnO@EDTA-Ag NPs) for enhanced electrochemical detection of Cu2+ ions in food and environmental samples