Research Article

Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites

Volume: 16 Number: 2 June 10, 2026
Burak Hülagü *, Muhammed Ali Güven , Batuhan Öztürk , Emrihan Binici
EN TR

Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites

Abstract

In this study, the mechanical and dynamic properties of particle reinforced epoxy composites produced by incorporating agricultural waste derived microparticles into an epoxy resin matrix were investigated. Microparticles obtained from the roots of Brassica oleracea var. capitata cabbage and Beta vulgaris var. cicla chard were added to the epoxy matrix at 1, 2, and 3 percent by weight. The main aim of the study was to develop environmentally friendly and sustainable composite systems that contribute to the reuse of natural waste materials. The effect of reinforcement content on composite performance was evaluated by SEM imaging, three point bending tests, and vibration analyses. The results showed that the addition of natural microparticles generally improved the vibration damping behavior of epoxy composites, while causing a reduction in flexural strength. The first damping ratio increased by 43 percent in composites reinforced with 1 percent cabbage microparticles and by up to 91 percent in composites containing 1 percent chard microparticles. SEM observations indicated that cabbage microparticles had a rougher surface morphology, which promoted better interfacial bonding and provided superior mechanical performance compared with chard. However, at higher reinforcement contents, agglomeration, particle size variations, and microstructural discontinuities negatively affected the mechanical properties. These findings indicate that particle size, dispersion quality, and reinforcement content should be carefully optimized to achieve balanced performance.

Keywords

Agricultural waste, Epoxy composites, Cabbage microparticles, Chard microparticles, Flexural strength, Waste management

Ethical Statement

This study does not involve any human participants or animal subjects. The experimental procedures were conducted using agricultural waste materials and commercial epoxy systems only. Therefore, no ethical approval was required for this research.

Thanks

We would like to thank Volkan ACAR, Salih ÇAĞLAYAN and Muhammed Emin KULA for their support within the scope of this study.

References

  1. Akhavan, H. & Ribeiro, P. (2011). Natural modes of vibration of variable stiffness composite laminates with curvilinear fibers. Composite Structures, 93(11), 3040–3047. https://doi.org/10.1016/j.compstruct.2011.04.027
  2. Barczewski, M., Sałasińska, K. & Szulc, J. (2019). Application of sunflower husk, hazelnut shell and walnut shell as waste agricultural fillers for epoxy-based composites: A study into mechanical behavior related to structural and rheological properties. Polymer Testing, 75, 1–11. https://doi.org/10.1016/j.polymertesting.2019.01.017
  3. Chinnasamy, S., Kowsik, K. V., & Raviram, R. (2024). Mechanical and vibration properties of epoxy composites reinforced with sisal, areca, and hemp fibers, enhanced by sugarcane bagasse and coconut husk fillers. Materials Circular Economy, 6(1), 24. https://doi.org/10.1007/s42824-024-00118-9
  4. da Silva, J. M. F., da Silva, J. P. S. & Soares, B. G. (2022). Reinforced epoxy-based laminates containing agro-industrial waste fiber from peach palm tree: effect of the matrix modification. Polymer Bulletin, 79(9), 7679–7696. https://doi.org/10.1007/s00289-021-03869-6
  5. Ding, N., Wang, X., Tian, Y., Yang, L., Chen, H. & Wang, Z. (2014). A renewable agricultural waste material for the synthesis of the novel thermal stability epoxy resins. Polymer Engineering and Science, 54(12), 2777–2784. https://doi.org/10.1002/pen.23838
  6. Fuentes, C. A., Beckers, K., Pfeiffer, H., Tran, L. Q. N., Dupont-Gillain, C., Verpoest, I. & Van Vuure, A. W. (2014). Equilibrium contact angle measurements of natural fibers by an acoustic vibration technique. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 455(1), 164–173. https://doi.org/10.1016/j.colsurfa.2014.04.054
  7. Ghazi, I. F. (2022, July). Plant waste reinforced epoxy composite: A short review on tensile and flexural strength. In AIP Conference Proceedings (Vol. 2450, No. 1, p. 020014). AIP Publishing LLC. https://doi.org/10.1063/5.0093831
  8. Hsieh, Y. Y., Tsai, Y. C., He, J. R., Yang, P. F., Lin, H. P., Hsu, C. H. & Loganathan, A. (2017). Rice husk agricultural waste-derived low ionic content carbon–silica nanocomposite for green reinforced epoxy resin electronic packaging material. Journal of the Taiwan Institute of Chemical Engineers, 78, 493–499. https://doi.org/10.1016/j.jtice.2017.06.010
  9. Ianov, V. V., Zenitova, L. A., & Ivanova, M. A. (2022, February). Reducing environmental hazards in the elimination of oil spills through the use of sorption materials based on polyurethane foams containing waste from agricultural and polymer industries. In IOP Conference Series: Earth and Environmental Science (Vol. 990, No. 1, p. 012064). IOP Publishing. https://doi.org/10.1088/1755-1315/990/1/012064
  10. Kandpal, B. C., Johri, N. (2023). Industrial/agricultural waste utility study as reinforcement in metal matrix and fibre reinforced polymer matrix composites. Advances in Manufacturing Technologies and Application of Artificial Intelligence: AMTAAI 2021, 2521(1), 040022. https://doi.org/10.1063/5.0117226
APA
Hülagü, B., Güven, M. A., Öztürk, B., & Binici, E. (2026). Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites. Karadeniz Fen Bilimleri Dergisi, 16(2), 934-950. https://doi.org/10.31466/kfbd.1834719
AMA
1.Hülagü B, Güven MA, Öztürk B, Binici E. Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites. KFBD. 2026;16(2):934-950. doi:10.31466/kfbd.1834719
Chicago
Hülagü, Burak, Muhammed Ali Güven, Batuhan Öztürk, and Emrihan Binici. 2026. “Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites”. Karadeniz Fen Bilimleri Dergisi 16 (2): 934-50. https://doi.org/10.31466/kfbd.1834719.
EndNote
Hülagü B, Güven MA, Öztürk B, Binici E (June 1, 2026) Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites. Karadeniz Fen Bilimleri Dergisi 16 2 934–950.
IEEE
[1]B. Hülagü, M. A. Güven, B. Öztürk, and E. Binici, “Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites”, KFBD, vol. 16, no. 2, pp. 934–950, June 2026, doi: 10.31466/kfbd.1834719.
ISNAD
Hülagü, Burak - Güven, Muhammed Ali - Öztürk, Batuhan - Binici, Emrihan. “Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites”. Karadeniz Fen Bilimleri Dergisi 16/2 (June 1, 2026): 934-950. https://doi.org/10.31466/kfbd.1834719.
JAMA
1.Hülagü B, Güven MA, Öztürk B, Binici E. Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites. KFBD. 2026;16:934–950.
MLA
Hülagü, Burak, et al. “Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites”. Karadeniz Fen Bilimleri Dergisi, vol. 16, no. 2, June 2026, pp. 934-50, doi:10.31466/kfbd.1834719.
Vancouver
1.Burak Hülagü, Muhammed Ali Güven, Batuhan Öztürk, Emrihan Binici. Mechanical and Dynamic Characterization of Agricultural Waste Particle Reinforced Epoxy Composites. KFBD. 2026 Jun. 1;16(2):934-50. doi:10.31466/kfbd.1834719