The Effect of Cu doping on Fatigue Properties of TiZrNbN Coatings

Yıl 2020, Cilt: 13 Sayı: 1, 181 - 189, 20.03.2020

Hossein Ahmad Aghdam Ayşenur Keleş , Ozlem Baran , Yaşar Totik , İhsan Efeoglu

Öz

The
fatigue properties are very important for cutting tools due to service life. To
improve fatigue properties of cutting tools, transition metal nitrides with
soft metal (Cu, Ni etc.) have been coated on cutting tool materials. To
investigate Cu effect on fatigue properties, TiZrNbN and Cu doped TiZrNbN
coatings were deposited on M2 high speed steel using reactive closed field
unbalanced magnetron sputtering (CFUBMS) in bias voltage of -80V, coating
pressure of 0.33 Pa and Cu target current of 0.6 A. Microstructure properties
of the coatings were determined by X-Ray Diffraction (XRD), Scanning Electron
Microscope (SEM) and Energy Dispersive Spectroscopy (EDS). Mechanical
properties of the coatings were examined with microhardness tester and scratch
tester. Fatigue properties of the coatings were examined using multi-pass
scratch tester. According to the results, the microhardness of Cu doped TiZrNbN
is better than TiZrNbN. On the other hand, the adhesion and fatigue properties
of TiZrNbN are the highest.

Anahtar Kelimeler

CFUBMS, multi-pass scratch, TiZrNbN, fatigue, Cu

Cu ilavesinin TiZrNbN Kaplamaların Yorulma Özelliklerine Etkisi

Öz

Yorulma
özellikleri, kullanım ömrü nedeniyle kesme aletleri için çok önemlidir. Kesici
takımların yorulma özelliklerini iyileştirmek için kesici takım malzemeleri
üzerine yumuşak metalle (Cu, Ni vb.) Geçiş metali nitrürleri kaplanmıştır.
Yorulma özellikleri üzerindeki Cu etkisini araştırmak için, TiZrNbN ve Cu
katkılı TiZrNbN kaplamalar, -80V'luk ön gerilim voltajında, 0.33 Pa'lık kaplama
basıncı ve Cu hedef akımında 0.6 A değerinde reaktif kapalı alan dengesiz manyetik
alanda sıçratma (CFUBMS) kullanılarak M2 yüksek hızlı çelik üzerinde
biriktirildi. Kaplamaların mikro yapı özellikleri X-Ray Difraktometri (XRD),
Taramalı Elektron Mikroskop (SEM) ve Enerji Dağıtıcı Spektroskopi (EDS) ile
belirlenmiştir. Kaplamaların mekanik özellikleri microhardness test cihazı ve çizik
test cihazı ile incelenmiştir. Kaplamaların yorulma özellikleri çok geçişli
çizik test cihazı kullanılarak incelenmiştir. Sonuçlara göre, Cu katkılı
TiZrNbN'nin mikro sertliği TiZrNbN'den daha iyidir. Öte yandan, TiZrNbN'nin
yapışma ve yorulma özellikleri en yüksektir

Anahtar Kelimeler

CFUBMS, çoklu geçişli çizik, TiZrNbN, yorulma, Cu

Kaynakça

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