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Dual optimization for instant soluble carob pod powder production by response surface method

Yıl 2023, Cilt: 12 Sayı: 2, 408 - 419, 15.04.2023

Mehmet Şükrü Karakuş Merve Akalan Melike Yücetepe Kamile Bayrak Akay Asliye Karaaslan Bülent Başyiğit Mehmet Karaaslan

https://doi.org/10.28948/ngumuh.1205063
Cited By: 1

Öz

In this study, bioactive compounds (phenolics) from carob pod were extracted by using microwave assisted extraction method. Spray drying technique was performed for the conversion of the resulting extract into powder form. Microwave assisted extraction and spray drying steps were optimized using response surface methodology. In the extraction stage, the effect of solvent temperature and extraction time on the total phenolic content was evaluated. Optimum extraction conditions (total phenolic content: 84.48 mg GAE/g) were determined as 55 °C and 26 min. For the final powder production, the maximum process yield (48.00%) was obtained at the point where the spray dryer inlet temperature was 184 °C and the flow rate was 8 mL/min. The presence of phenolic structures in final product was verified by FTIR spectroscopy. Total phenolic content (15.37 mg GAE/g) and antioxidative behavior (DPPH: 0.63 mmol TE/g, ABTS: 0.30 mmol TE/g, FRAP: 0.06 mmol TE/g, CUPRAC: 0.05 mmol TE)/g) of carob powders were evaluated.

Anahtar Kelimeler

Keçiboynuzu kabuğu Mikrodalga destekli ekstraksiyon Püskürtmeli kurutma Toplam fenolik madde Antioksidan aktivite

Kaynakça

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  • S. Naghmouchi, M.L. Khouja, A. Romero, J. Tous, M. Boussaid, Tunisian carob (Ceratonia siliqua L.) populations: Morphological variability of pods and kernel. Scientia Horticulturae, 121 (2), 125–130, 2009. https://doi.org/10.1016/j.scienta.2009.02.026
  • H.R. Oziyci, N. Tetik, I. Turhan, E. Yatmaz, K. Ucgun, H. Akgul, H. Gubbuk, M. Karhan, Mineral composition of pods and seeds of wild and grafted carob (Ceratonia siliqua L.) fruits. Scientia Horticulturae, 167 (6), 149–152, 2014. https://doi.org/10.1016/j.scienta.2014.01.005
  • L. Tounsi, S. Karra, H. Kechaou, N. Kechaou, Processing, physico-chemical and functional properties of carob molasses and powders. Journal of Food Measurement and Characterization, 11, 1440–1448, 2017. https://doi.org/10.1007/s11694-017-9523-4
  • M. Musa Özcan, D. Arslan, H. Gökçalik, Some compositional properties and mineral contents of carob (Ceratonia siliqua) fruit, flour and syrup. International Journal of Food Science and Nutrition, 58 (8), 652–658, 2007. https://doi.org/10.1080/09637480701395549
  • L. Tounsi, H. Kchaou, F. Chaker, S. Bredai, N. Kechaou, Effect of adding carob molasses on physical and nutritional quality parameters of sesame paste. Journal of Food Science and Technology, 56, 1502–1509, 2019. https://doi.org/10.1007/s13197-019-03640-w
  • M. Sengül, M. Fatih Ertugay, M. Sengül, Y. Yüksel, Rheological Characteristics of Carob Pekmez. International Journal of Food Properties, 10 (1), 39–46, 2007. https://doi.org/10.1080/10942910600627996
  • L.M. Hernandez, E.G. Xu, H.C.E. Larsson, R. Tahara, V.B. Maisuria, N. Tufenkji, Plastic Teabags Release Billions of Microparticles and Nanoparticles into Tea. Enviromental Science Technology, 53 (21), 12300–12310, 2019. https://doi.org/10.1021/acs.est.9b02540
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Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu

Yıl 2023, Cilt: 12 Sayı: 2, 408 - 419, 15.04.2023

Mehmet Şükrü Karakuş Merve Akalan Melike Yücetepe Kamile Bayrak Akay Asliye Karaaslan Bülent Başyiğit Mehmet Karaaslan

https://doi.org/10.28948/ngumuh.1205063
Cited By: 1

Öz

Bu çalışmada, mikrodalga destekli ekstraksiyon yöntemi kullanılarak keçiboynuzu kabuğundan elde edilen biyoaktif maddeler (fenolikler) püskürtmeli kurutma tekniği ile çözünür toz forma dönüştürülmüştür. Mikrodalga destekli ekstraksiyon ve püskürtmeli kurutma adımları yanıt yüzey metodolojisi kullanılarak optimize edilmiştir. Ekstraksiyon aşamasında, solvent sıcaklığının ve ekstraksiyon süresinin toplam fenolik madde miktarı üzerine etkisi değerlendirilmiştir. Optimum ekstraksiyon koşulları (toplam fenolik madde miktarı: 84.48 mg GAE/g), 55 °C ve 26 dk olarak belirlenmiştir. Nihai toz üretimi için ise maksimum işlem verimi (%48.00) püskürtmeli kurutucu giriş sıcaklığının 184 °C ve akış hızının 8 mL/dk olduğu noktada sağlanmıştır. Son üründeki fenolik maddelerin varlığı FTIR spektroskopisi ile doğrulanmıştır. Elde edilen tozların toplam fenolik madde miktarı (15.37 mg GAE/g) ve antioksidatif davranışı (DPPH: 0.63 mmol TE/g, ABTS: 0.30 mmol TE/g, FRAP: 0.06 mmol TE/g, CUPRAC: 0.05 mmol TE/g) araştırılmıştır.

Anahtar Kelimeler

Keçiboynuzu kabuğu Mikrodalga destekli ekstraksiyon Püskürtmeli kurutma Toplam fenolik madde Antioksidan aktivite

Kaynakça

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  • S. Naghmouchi, M.L. Khouja, A. Romero, J. Tous, M. Boussaid, Tunisian carob (Ceratonia siliqua L.) populations: Morphological variability of pods and kernel. Scientia Horticulturae, 121 (2), 125–130, 2009. https://doi.org/10.1016/j.scienta.2009.02.026
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  • L. Tounsi, S. Karra, H. Kechaou, N. Kechaou, Processing, physico-chemical and functional properties of carob molasses and powders. Journal of Food Measurement and Characterization, 11, 1440–1448, 2017. https://doi.org/10.1007/s11694-017-9523-4
  • M. Musa Özcan, D. Arslan, H. Gökçalik, Some compositional properties and mineral contents of carob (Ceratonia siliqua) fruit, flour and syrup. International Journal of Food Science and Nutrition, 58 (8), 652–658, 2007. https://doi.org/10.1080/09637480701395549
  • L. Tounsi, H. Kchaou, F. Chaker, S. Bredai, N. Kechaou, Effect of adding carob molasses on physical and nutritional quality parameters of sesame paste. Journal of Food Science and Technology, 56, 1502–1509, 2019. https://doi.org/10.1007/s13197-019-03640-w
  • M. Sengül, M. Fatih Ertugay, M. Sengül, Y. Yüksel, Rheological Characteristics of Carob Pekmez. International Journal of Food Properties, 10 (1), 39–46, 2007. https://doi.org/10.1080/10942910600627996
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  • S. Saikia, N.K. Mahnot, C.L. Mahanta, Effect of Spray Drying of Four Fruit Juices on Physicochemical, Phytochemical and Antioxidant Properties. Journal of Food Processing and Preservation, 39 (6), 1656–1664, 2015. https://doi.org/10.1111/jfpp.12395
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  • C. Turchiuli, Z. Eloualia, N. el Mansouri, E. Dumoulin, Fluidised bed agglomeration: Agglomerates shape and end-use properties. Powder Technology, 157 (1-3), 168–175, 2005. https://doi.org/10.1016/j.powtec.2005.05.024
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  • K. Duangmal, B. Saicheua, S. Sueeprasan, Colour evaluation of freeze-dried roselle extract as a natural food colorant in a model system of a drink. LWT - Food Science and Technology, 41 (8), 1437–1445, 2008. https://doi.org/10.1016/j.lwt.2007.08.014
  • V.L. Singleton, J.A. Rossi, Colorimetry of Total Phenolics with Phosphomolybdic-Phosphotungstic Acid Reagents. American of Journal Enology and Viticulture, 16, 144–158, 1965.
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  • R. Apak, K. Güçlü, M. Özyürek, S.E. Çelik, Mechanism of antioxidant capacity assays and the CUPRAC (cupric ion reducing antioxidant capacity) assay. Microchimica Acta., 160, 413–419, 2008. https://doi.org/10.1007/s00604-007-0777-0
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  • A. Christou, I.J. Stavrou, C.P. Kapnissi-Christodoulou, Continuous and pulsed ultrasound-assisted extraction of carob’s antioxidants: Processing parameters optimization and identification of polyphenolic composition. Ultrasonics Sonochemistry, 76, 105630, 2021. https://doi.org/10.1016/j.ultsonch.2021.105630
  • M. Almanasrah, L.B. Roseiro, R. Bogel-Lukasik, F. Carvalheiro, C. Brazinha, J. Crespo, M. Kallioinen, M. Mänttäri, L.C. Duarte, Selective recovery of phenolic compounds and carbohydrates from carob kibbles using water-based extraction. Industrial Crops and Products, 70, 443–450, 2015. https://doi.org/10.1016/j.indcrop.2015.02.051
  • C.-H. Chan, R. Yusoff, G.-C. Ngoh, F.W.-L. Kung, Microwave-assisted extractions of active ingredients from plants. Journal of Chromatography A., 1218 (37), 6213–6225, 2011. https://doi.org/10.1016/j.chroma.2011.07.040
  • F. Dahmoune, G. Spigno, K. Moussi, H. Remini, A. Cherbal, K. Madani, Pistacia lentiscus leaves as a source of phenolic compounds: Microwave-assisted extraction optimized and compared with ultrasound-assisted and conventional solvent extraction. Industrial Crops and Products, 61, 31–40, 2014. https://doi.org/10.1016/j.indcrop.2014.06.035
  • J. Song, D. Li, C. Liu, Y. Zhang, Optimized microwave-assisted extraction of total phenolics (TP) from Ipomoea batatas leaves and its antioxidant activity. Innovative Food Science & Emerging Technologies, 12 (3), 282–287, 2011. https://doi.org/10.1016/j.ifset.2011.03.001
  • E. Assadpour, S. Mahdi Jafari, A systematic review on nanoencapsulation of food bioactive ingredients and nutraceuticals by various nanocarriers. Critical Reviews Food Science and Nutrition, 59 (19), 3129–3151, 2019. https://doi.org/10.1080/10408398.2018.1484687
  • M.R.I. Shishir, L. Xie, C. Sun, X. Zheng, W. Chen, Advances in micro and nano-encapsulation of bioactive compounds using biopolymer and lipid-based transporters. Trends in Food Science and Technology, 78, 34–60, 2018. https://doi.org/10.1016/j.tifs.2018.05.018
  • C.S. Singh, V.K. Paswan, D.C. Rai, Process optimization of spray dried Jamun (Syzygium cumini L.) pulp powder. LWT, 109, 1–6, 2019. https://doi.org/10.1016/j.lwt.2019.04.011
  • L. Mahmoudi, H. Tavakoilpour, L. Roozbeh-Nasiraie, A. Kalbasi-Ashtari, Ultrasonication and encapsulation of Butcher broom (Ruscus Hyrcanus L.) extract and its bioactive effects on qualitative properties, oxidative stability and shelf life of cake. Sustainable Chemistry and Pharmacy, 17, 100295, 2020. https://doi.org/10.1016/j.scp.2020.100295
  • V. Sablania, S.J.D. Bosco, Optimization of spray drying parameters for Murraya koenigii (Linn) leaves extract using response surface methodology. Powder Technology, 335, 35–41, 2018. https://doi.org/10.1016/j.powtec.2018.05.009
  • A. Rezvankhah, Z. Emam-Djomeh, G. Askari, Encapsulation and delivery of bioactive compounds using spray and freeze-drying techniques: A review. Drying Technology, 38 (1-2), 235–258, 2020. https://doi.org/10.1080/07373937.2019.1653906
  • A.M. Naji, B. Başyiğit, H. Alaşalvar, P. Salum, S. Berktaş, Z. Erbay, M. Çam, Instant soluble roselle (Hibiscus sabdariffa L.) powder rich in bioactive compounds: Effect of the production process on volatile compounds. Journal of Food Measurement and Characterization, 1-13, 2022. https://doi.org/10.1007/s11694-022-01593-x
  • L. Medina-Torres, R. Santiago-Adame, F. Calderas, J.A. Gallegos-Infante, R.F. González-Laredo, N.E. Rocha-Guzmán, D.M. Núñez-Ramírez, M.J. Bernad-Bernad, O. Manero, Microencapsulation by spray drying of laurel infusions (Litsea glaucescens) with maltodextrin. Industrial Crops and Products, 90, 1–8, 2016. https://doi.org/10.1016/j.indcrop.2016.06.009
  • S. Thummajitsakul, P. Piyaphan, S. Khamthong, M. Unkam, K. Silprasit, Comparison of FTIR fingerprint, phenolic content, antioxidant and anti-glucosidase activities among Phaseolus vulgaris L., Arachis hypogaea L. and Plukenetia volubilis L. Electronic Journal of Biotechnology, 61, 14–23, 2023. https://doi.org/10.1016/j.ejbt.2022.10.003
  • O. Abbas, G. Compère, Y. Larondelle, D. Pompeu, H. Rogez, V. Baeten, Phenolic compound explorer: A mid-infrared spectroscopy database. Vibrational Spectroscopy, 92, 111–118, 2017. https://doi.org/10.1016/j.vibspec.2017.05.008
  • C. Christou, A. Agapiou, R. Kokkinofta, Use of FTIR spectroscopy and chemometrics for the classification of carobs origin. Journal of Advanced Research, 10, 1–8, 2018. https://doi.org/10.1016/j.jare.2017.12.001
  • A. Can Karaca, O. Guzel, M.M. Ak, Effects of processing conditions and formulation on spray drying of sour cherry juice concentrate. Journal of the Science of Food and Agriculture, 96 (2), 449–455, 2016. https://doi.org/10.1002/jsfa.7110
  • B.R. Bhandari, N. Datta, T. Howes, Problems Associated With Spray Drying Of Sugar-Rich Foods. Drying Technology, 15 (2), 671–684, 1997. https://doi.org/10.1080/07373939708917253
  • H. Ali, A.R. Al-khalifa, W. Aboelsood, G. Bareh, A. Farouk, Influence of spray-drying on improving the quality of dried carob juice. Quality Assurance and Safety of Crops & Foods, 11 (4), 391–399, 2019. https://doi.org/10.3920/QAS2018.1524
  • A.A. Santana, L.G.P. Martin, R.A. de Oliveira, L.E. Kurozawa, K.J. Park, Spray drying of babassu coconut milk using different carrier agents. Drying Technology, 35 (1), 76–87, 2017. https://doi.org/10.1080/07373937.2016.1160111
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  • B. Neirinck, J. van Deursen, O. van der Biest, J. Vleugels, Wettability Assessment of Submicrometer Alumina Powder Using a Modified Washburn Method. Journal of the American Ceramic Society, 93 (9), 2515–2518, 2010. https://doi.org/10.1111/j.1551-2916.2010.03854.x
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  • P.H.C. Felix, V.S. Birchal, D.A. Botrel, G.R. Marques, S.V. Borges, Physicochemical and Thermal Stability of Microcapsules of Cinnamon Essential Oil by Spray Drying. Journal of Food Processing and Preservation, 41 (3), e12919, 2017. https://doi.org/10.1111/jfpp.12919
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  • C.V. Bezerra, E.R. Amante, D.C. de Oliveira, A.M.C. Rodrigues, L.H.M. da Silva, Green banana (Musa cavendishii) flour obtained in spouted bed – Effect of drying on physico-chemical, functional and morphological characteristics of the starch. Industrial Crops and Products, 41, 241–249, 2013. https://doi.org/10.1016/j.indcrop.2012.04.035
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  • A. Richane, B.M. Rim, M. wided, K. Riadh, A. Khaoula, M. Nizar, B.I. Hanen, Variability of phenolic compounds and antioxidant activities of ten Ceratonia siliqua L. provenances. Biochemical Systematics and Ecology, 104, 104486, 2022. https://doi.org/10.1016/j.bse.2022.104486
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Toplam 65 adet kaynakça vardır.

Ayrıntılar

Birincil Dil Türkçe
Konular Gıda Mühendisliği
Bölüm Gıda Mühendisliği
Yazarlar

Mehmet Şükrü Karakuş 0000-0002-1805-8206

Merve Akalan 0000-0002-3926-245X

Melike Yücetepe 0000-0002-9581-225X

Kamile Bayrak Akay 0000-0001-7976-377X

Asliye Karaaslan 0000-0002-3834-0647

Bülent Başyiğit 0000-0002-6617-1836

Mehmet Karaaslan 0000-0001-8097-9535

Yayımlanma Tarihi 15 Nisan 2023
Gönderilme Tarihi 15 Kasım 2022
Kabul Tarihi 15 Şubat 2023
Yayımlandığı Sayı Yıl 2023 Cilt: 12 Sayı: 2

Kaynak Göster

APA Karakuş, M. Ş., Akalan, M., Yücetepe, M., Bayrak Akay, K., vd. (2023). Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, 12(2), 408-419. https://doi.org/10.28948/ngumuh.1205063
AMA Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M. Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. NÖHÜ Müh. Bilim. Derg. Nisan 2023;12(2):408-419. doi:10.28948/ngumuh.1205063
Chicago Karakuş, Mehmet Şükrü, Merve Akalan, Melike Yücetepe, Kamile Bayrak Akay, Asliye Karaaslan, Bülent Başyiğit, ve Mehmet Karaaslan. “Kullanıma hazır Suda çözünebilir keçiboynuzu kabuğu Tozu üretiminin yanıt yüzey yöntemi Ile çift aşamalı Optimizasyonu”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 12, sy. 2 (Nisan 2023): 408-19. https://doi.org/10.28948/ngumuh.1205063.
EndNote Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M (01 Nisan 2023) Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 12 2 408–419.
IEEE M. Ş. Karakuş, “Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu”, NÖHÜ Müh. Bilim. Derg., c. 12, sy. 2, ss. 408–419, 2023, doi: 10.28948/ngumuh.1205063.
ISNAD Karakuş, Mehmet Şükrü vd. “Kullanıma hazır Suda çözünebilir keçiboynuzu kabuğu Tozu üretiminin yanıt yüzey yöntemi Ile çift aşamalı Optimizasyonu”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 12/2 (Nisan 2023), 408-419. https://doi.org/10.28948/ngumuh.1205063.
JAMA Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M. Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. NÖHÜ Müh. Bilim. Derg. 2023;12:408–419.
MLA Karakuş, Mehmet Şükrü vd. “Kullanıma hazır Suda çözünebilir keçiboynuzu kabuğu Tozu üretiminin yanıt yüzey yöntemi Ile çift aşamalı Optimizasyonu”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, c. 12, sy. 2, 2023, ss. 408-19, doi:10.28948/ngumuh.1205063.
Vancouver Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M. Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. NÖHÜ Müh. Bilim. Derg. 2023;12(2):408-19.

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Journal of the Institute of Science and Technology
https://doi.org/10.21597/jist.1290953
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